A method is disclosed for preparing and dispensing a mixture obtained by mixing at least one first chemically reactive component and at least one second chemically reactive component containing a dispersed solid material i.e. a filler, by a high pressure mixing device comprising a head provided with injectors and one or more interception and supply devices defined by respective nozzles for narrowing the passage of the flows and with correlated plug members that are movable axially and settable for controlling said narrowing. The injectors and the interception and supply device transform the pressure energy of the fluids into kinematic energy of the jets that clash in the mixing chamber to mix the components for turbulence induced by the jets, in which a valve member is slidable, in particular a slide-valve, provided with longitudinal slots for recirculating the components to respective storage tanks. The method provides: removing from at least one tank, by pumping arrangement connected to a respective hydraulic delivery line to the head, a dosed quantity of the at least second chemically reactive second component to with filler material is added; preventing, once said quantity is removed, that the second component flows back from the pumping arrangement to the tank; dosing the component with a controlled flowrate B to the delivery line to the mixing head; keeping the slide-valve closed in a recirculating position and preventing the entry of the at least second component to the head and to the respective recirculating slot and pressurizing, by a dosed quantity Vot, the delivery line to subject the at least second polymeric component to a pressure increase along the delivery line until a value is reached that is near that reached by the passage through the nozzle of the respective interception and supply device; subsequently enabling the entry of the second component into the head to make the second component recirculate to the slots of the slide-valve for a period of time that is comparatively very reduced until it is reduced virtually to zero with respect to a recirculating step of the at least first component through the slide-valve, and subsequently opening by retracting the slide-valve to permit mixing by high pressure collision of the first and at least one second components to dispense the resulting mixture through the mixing chamber and the dispensing conduit for pouring the mixture into a cavity or into a shape to make an object by reaction of the aforesaid first and second chemically reactive components. An apparatus for preparing and dispensing the mixture is also disclosed.

Additives such as colourants may be incorporated into polymeric materials such as polyesters, such as in polyester fibre production, by use of a liquid formulation comprising colourant and a vehicle. The vehicle may comprise a functionalised pentaerythritol, trimethylolpropane or trimellitate. The liquid formulation is suitably contacted with the polymeric material in a melt processing apparatus.

A process for continuously preparing a polyolefin composition made from or containing a polyolefin and carbon black in an extruder device. The process includes the steps of supplying polyolefin in form of a polyolefin powder and carbon black to a mixing device; alternatively, (a) measuring the flow rate of the polyolefin powder supplied to the mixing device or (b) measuring the flow rate of the polyolefin pellets prepared in the extruder device; adjusting the flow rate of the carbon black to the mixing device in response to the measured flow rate of the polyolefin powder or adjusting the flow rate of the polyolefin powder to the mixing device in response to the measured flow rate of the polyolefin pellets; melting and homogenizing the mixture within the extruder device; and pelletizing the polyolefin composition into the polyolefin pellets.

In one aspect, the invention provides a substantially exfoliated nanocomposite material including starch and hydrophobically modified layered silicate clay. In another aspect, the invention provides packaging made from material including the substantially exfoliated nanocomposite material described above. The nanocomposite material has improved mechanical and rheological properties and reduced sensitivity to moisture in that the rates of moisture update and/or loss are reduced. In another aspect, the invention provides a process for preparing the substantially exfoliated nanocomposite material described above, including a step of mixing the starch in the form of an aqueous gel with the hydrophobic clay in a melt mixing device. In a further aspect, the invention provides a process for preparing the substantially exfoliated nanocomposite material, including the steps of mixing the starch with the hydrophobic clay to form a masterbatch (hereinafter “the masterbatch process”) and mixing the masterbatch with further starch.

A method for manufacturing a liquid formulation for reaction injection molding for polymerizing a norbornene-based monomer in the presence of a metathesis polymerization catalyst comprising tungsten as a center metal, the liquid formulation comprising a norbornene-based monomer, provided that in case where the norbornene-based monomer includes exo-dicyclopentadiene, a content of exo-dicyclopentadiene is from 0 to 2% by mass of the norbornene-based monomer, an activator of the catalyst, and a specific ether compound.

A method for producing a rubber member according to the present invention includes the steps of: supplying a rubber composition to a cylinder provided in an extruder; extruding the rubber composition to a downstream side of the cylinder while kneading the rubber composition in an internal space of the cylinder that includes a plurality of protruding members protruding from an inner wall surface of the cylinder; compressing the rubber composition at least once in the step of extruding the rubber composition to the downstream side; discharging a gas generated from the compressed rubber composition to outside of the cylinder; discharging, through a discharge outlet of the cylinder, the rubber composition after the gas has been generated; and molding the rubber composition that has been discharged through the discharge outlet into a predetermined rubber member shape.

Method for obtaining biodegradable polyesteretheramide that has a stage of esterification and/or transesterification and amidation reaction, a stage of prepolycondensation, a stage of polycondensation, an optional stage of extraction, a stage of drying and a final stage of extrusion with additives. The method of obtaining PEEA enables better satisfaction of the needs of each client as regards viscosity, composition and additives. It enables reducing the amount of interface product that has lower commercial value and improves the colour of the product, while at the same time provides a more efficient process, ecologically cleaner and safer for all the operatives.

For the production of polymers in which there are fillers with particle sizes below 10 μm incorporated and homogeneously distributed, a polymer starting material is input into a twin-screw extruder and is melted there to give a melt. In a conveying and mixing section, a suspension, which is formed of the fillers and of a carrier liquid, is injected into the melt. The melt viscosity is reduced by injection of the carrier liquid in the conveying and mixing section in that a cleavable polycondensate is used as polymer and low-molecular-weight cleavage product arising during the polycondensation is used as carrier liquid, and therefore the molten polymer is at least to some extent depolymerized within the conveying and mixing section. That the mixture, which is formed of the melt whose viscosity is reduced by cleavage, of the remainder of the carrier liquid and of the fillers, is homogenized.

A method of producing an adhesive resin includes: a heating and kneading step of kneading a mixture containing a ring structure-containing hydrocarbon resin, an adhesive functional group-containing compound, and a peroxide while heating the mixture to obtain a heated and kneaded product; and a cooling and kneading step, performed in succession to the heating and kneading step, of kneading the heated and kneaded product while cooling the heated and kneaded product to obtain a cooled and kneaded product. The adhesive resin has a yellowness index (Yi) of 3.0 or less when 0.8 parts by mass of 2-(5-chloro-2-benzotriazolyl)-6-tert-butyl-p-cresol is added to 100 parts by mass of the adhesive resin.

An earth plant-based compostable biodegradable composition for the formation of a bioplastic and method of producing said resin, the composition comprising: about 17.5 to 45% ethanol-based green polyethylene by weight, about 20 to 25% calcium carbonate by weight, about 2 to 12% hemp hurd or soy protein by weight, about 32 to 45% starch by weight, and about 0.5 to 1% biodegradation additive by weight to enable biodegradation and composting of the bioplastic; wherein the composition is produced by first mill grinding the ethanol-based green polyethylene, calcium carbonate, hemp hurd or soy protein, starch and the biodegradation additive into fine powders, then mechanically mixing the fine powders one by one into a final mixture for about 5-25 minutes at a time, dry and without heat, and then heating the final mixture to about 220 to 430 degrees Fahrenheit.