The present invention provides a method for producing a solution of nanosheets, comprising the step of contacting an intercalated layered material with a polar aprotic solvent to produce a solution of nanosheets, wherein the intercalated layered material is prepared from a layered material selected from the group consisting of a transition metal dichalcogenide, a transition metal monochalcogenide, a transition metal trichalcogenide, a transition metal oxide, a metal halide, an oxychalcogenide, an oxypnictide, an oxyhalide of a transition metal, a trioxide, a perovskite, a niobate, a ruthenate, a layered III-VI semiconductor, black phosphorous and a V-VI layered compound. The invention also provides a solution of nanosheets and a plated material formed from nanosheets.

The present application provides a negative thermal expansion material having excellent dispersibility and packing properties in a positive thermal expansion material. The negative thermal expansion material of the present invention comprises spherical zirconium tungsten phosphate having a BET specific surface area, of 2 m.sup.2/g or smaller. The degree of sphericity is preferably 0.90 or more and 1 or less. Also preferably, the negative thermal expansion material further contains at least Mg and/or V as a subcomponent element. Also preferably, the content of the subcomponent element is 0.1% by mass or more and 3% by mass or less. Also preferably, the average particle size is 1 m or larger and 50 m smaller.

Halogen-doped phosphorous nanoparticles and a manufacturing method thereof are provided. The manufacturing method includes a mixing process and a centrifugation or filtration process. The mixing process has the step of mixing a precursor with a reducing agent solution to form a mixed solution, the precursor is a halogen-based phosphide. Then, the mixed solution is centrifuged or filtrated to obtain the halogen-doped phosphorous nanoparticles.

A scalable approach for the synthesis of black phosphorus (BP) material thin films over large areas is described. A red phosphorus (RP) material thin film may be deposited on a substrate followed by conversion to a BP material thin film using high-pressure alone or high pressure and high temperature. A thin-film of dielectric material such as hexagonal boron nitride (hBN) can be formed on a RP material film before the conversion is performed to improve the crystalline quality and stability of the converted BP material. Surprisingly, an atomically sharp and defect-free interface can be formed between the converted BP material and hBN. The BP material has high crystalline uniformity and can be used to fabricate thin-film transistors and optoelectronic devices such as infrared photodetectors.

The invention relates to a device for sterilization of the interior surface of packaging containers with electron beam, comprising an emitter provided with an electron exit window. The emitter is adapted to emit charge carriers, such as electrons, through the electron exit window, said electrons forming an electron cloud. The device comprises at least one outlet adapted to provide a flow of sterile gaseous medium adapted to maintain a local aseptic zone around at least an emitter portion including the electron exit window, thus preventing any flow of medium from outside the local aseptic zone from coming into the local aseptic zone. The invention also relates to a method.

A composition of matter and method of forming a radiation shielding member at ambient temperatures in which the composition of matter includes a cold-fired chemically bonded oxide-phosphate ceramic cement matrix; with one or more suitably prepared and distributed radiation shielding materials dispersed in the cold-fired chemically bonded oxide-phosphate ceramic cement matrix.

The present application provides a method for preparing a lithium iron phosphate material coated with carbon nanoribbon, including the steps of: 1) fully and uniformly dispersing carbon nanoribbons in an aqueous solution by means of stirring and ultrasonic dispersion, and obtaining a mixture; 2) adding a lithium source, an iron source and a phosphorous source at a molar ratio of Li:Fe:P=1:1:1 into the mixture of step 1) under the protection of inert gas, adding water and stirring to form a slurry, and refluxing the slurry; 3) washing and drying the slurry to obtain a primary lithium iron phosphate material coated with carbon nanoribbon; and 4) annealing the primary lithium iron phosphate material coated with carbon nanoribbon of step 3) at high-temperature in a protective atmosphere of argon containing 5-10% v/v of hydrogen, and obtaining the lithium iron phosphate material coated with carbon nanoribbon.

A system for extracting uranium from wet-process phosphoric acid (WPA), includes an ion exchange resin or solvent extractor for separating uranium from WPA to produce a loaded uranium solution stream and a uranium depleted WPA stream. An ion exchange resin is positioned to receive the loaded uranium solution stream and bind uranium species thereto. An anion solution stream is positioned to feed a solution comprising anions onto the ion exchange resin to form a loaded uranium eluant stream. The loaded uranium eluant stream may then be treated to provide a uranium containing product.

The present invention relates to a new and simple purification process of phosphorus decasulfide (P.sub.4S.sub.10), also called phosphorus pentasulfide (P.sub.2S.sub.5), which is used as thionating agent for the syntheses of various organic compounds, particularly the organic compounds having sulfur heteroatom(s).

Methods for the preparation of few-layer phosphorene, compositions thereof and related devices fabricated therefrom.