C01B33/00

Surface functionalization of inorganic nanocrystals for nanocomposite additive manufacturing

An aqueous or organic solvent medium for additive manufacturing technologies comprising a nanocrystal comprising a functional group. The nanocrystal material is selected from a metal oxide, fluoride, metallic, carbon-based, semiconducting quantum dot or combinations thereof. The functional group comprises primary amine, carboxylic acid, lactam ring, polyamide polymer chain or group used to attach a similar functional group.

Porous halloysite powder and method for producing halloysite powder

Provided are a halloysite powder and a method for producing the halloysite powder. The halloysite powder contains granules in which halloysite including halloysite nanotubes is aggregated. The granules have first pores derived from the tube holes in the halloysite nanotubes and second pores that are different from the first pores.

3D REDUCED GRAPHENE OXIDE/SIO 2 COMPOSITE FOR ICE NUCLEATION
20220002159 · 2022-01-06 ·

The present invention provides for an ice-nucleating particle for cloud seeding and other applications, which can initiate ice nucleation at a temperature of−8° C. Further, the ice nucleation particle number increased continuously and rapidly with the reducing of temperature. The ice nucleating particle in the present invention is a nanostructured porous composite of 3-dimensional reduced graphene oxide and silica dioxide nanoparticles (PrGO-SN). The present invention also provides for a process for synthesizing the PrGO-SN.

Solid State Catholyte or Electrolyte for Battery Using LiaMPbSc (M=Si, Ge, and/or Sn)

The present invention provides an energy storage device comprising a cathode region or other element. The device has a major active region comprising a plurality of first active regions spatially disposed within the cathode region. The major active region expands or contracts from a first volume to a second volume during a period of a charge and discharge. The device has a catholyte material spatially confined within a spatial region of the cathode region and spatially disposed within spatial regions not occupied by the first active regions. In an example, the catholyte material comprises a lithium, germanium, phosphorous, and sulfur (“LGPS”) containing material configured in a polycrystalline state. The device has an oxygen species configured within the LGPS containing material, the oxygen species having a ratio to the sulfur species of 1:2 and less to form a LGPSO material. The device has a protective material formed overlying exposed regions of the cathode material to substantially maintain the sulfur species within the catholyte material. Also included is a novel dopant configuration of the Li.sub.aMP.sub.bS.sub.c (LMPS) [M=Si,Ge, and/or Sn] containing material.

Solid State Catholyte or Electrolyte for Battery Using LiaMPbSc (M=Si, Ge, and/or Sn)

The present invention provides an energy storage device comprising a cathode region or other element. The device has a major active region comprising a plurality of first active regions spatially disposed within the cathode region. The major active region expands or contracts from a first volume to a second volume during a period of a charge and discharge. The device has a catholyte material spatially confined within a spatial region of the cathode region and spatially disposed within spatial regions not occupied by the first active regions. In an example, the catholyte material comprises a lithium, germanium, phosphorous, and sulfur (“LGPS”) containing material configured in a polycrystalline state. The device has an oxygen species configured within the LGPS containing material, the oxygen species having a ratio to the sulfur species of 1:2 and less to form a LGPSO material. The device has a protective material formed overlying exposed regions of the cathode material to substantially maintain the sulfur species within the catholyte material. Also included is a novel dopant configuration of the Li.sub.aMP.sub.bS.sub.c (LMPS) [M=Si,Ge, and/or Sn] containing material.

Active material, anode layer, battery, and methods for producing these

A main object of the present disclosure is to provide an active material wherein a volume variation due to charge/discharge is small. The present disclosure achieves the object by providing an active material comprising a silicon clathrate II type crystal phase, including a void inside a primary particle, and a void amount of the void with a fine pore diameter of 100 nm or less is 0.05 cc/g or more and 0.15 cc/g or less.

Polysilocarb based silicon carbide materials, applications and devices

Organosilicon chemistry, polymer derived ceramic materials, and methods. Such materials and methods for making polysilocarb (SiOC) and Silicon Carbide (SiC) materials having 3-nines, 4-nines, 6-nines and greater purity. Processes and articles utilizing such high purity SiOC and SiC.

Phosphor and light-emitting device

A phosphor which has a main crystal phase having the same crystal structure as that of CaAlSiN.sub.3, wherein the phosphor satisfies conditions of a span value (d90−d10)/d50 of 1.70 or less and a d50 of 10.0 μm or less, as represented with d10, d50, and d90 on a volume frequency measured according to a laser diffraction method; wherein the d10, d50, and d90 on a volume frequency in a particle distribution measured are each a measured by loading 0.5 g of a phosphor into 100 ml of a solution of 0.05% by weight of sodium hexametaphosphate mixed in ion exchange water, and subjecting the resultant to a dispersing treatment for 3 minutes with an ultrasonic homogenizer at an oscillation frequency of 19.5±1 kHz, a chip size of 20φ, and an amplitude of vibration of 32±2 μm, with a chip placed at a central portion.

Thermoelectric conversion material and method of obtaining electrical power using thermoelectric conversion material

A thermoelectric conversion material has a composition represented by the chemical formula Li.sub.3-aBi.sub.1-bSi.sub.b, in which the range of values a and b is: 0≤a≤0.0001, and −a+0.0003≤b≤0.023; 0.0001≤a<0.0003, and −a+0.0003≤b≤exp[−0.046×(ln(a)).sup.2−1.03×ln(a)−9.51]; or 0.0003≤a≤0.085, and 0<b≤exp[−0.046×(ln(a)).sup.2−1.03×ln(a)−9.51], and in which the thermoelectric conversion material has a BiF.sub.3-type crystal structure and has a p-type polarity.

METHOD FOR REFINING CRUDE SILICON MELTS USING A PARTICULATE MEDIATOR
20220219994 · 2022-07-14 · ·

A process for refining crude molten silicon. The process includes oxidatively refining the crude molten silicon in the production of technical silicon. The crude molten silicon is admixed during the refining with a particulate mediator which has a minimum amount of metallic silicon of 8% by mass and also at least one or more of the elements H, C, O, F, Cl, Ca, Fe and Al. The particulate mediator is described by a characteristic number K which has a value of 0.03 to 6 mm.sup.−1 and is calculated using the formula

[00001] K = 6 .Math. ( 1 - .Math. m , M ) d 50 , M

where d.sub.50,M is the particle size (diameter) at 50% of the mass undersize of the grading curve of the particulate mediator [mm] and the ε.sub.m,M is the mean effective porosity of the particulate mediator.