C01F17/00

Method of preparing cerium boride powder

A method of preparing cerium boride powder, according to the present invention, includes a first step for generating mixed powder by mixing at least one selected from among cerium chloride (CeCl.sub.3) powder and cerium oxide (CeO.sub.2) powder, at least one selected from among magnesium hydride (MgH.sub.2) powder and magnesium (Mg) powder, and boron oxide (B.sub.2O.sub.3) powder, a second step for generating composite powder including cerium boride (Ce.sub.xB.sub.y) and at least one selected from among magnesium oxide (MgO) and magnesium chloride (MgCl.sub.2), by causing reaction in the mixed powder at room temperature based on a ball milling process, and a third step for selectively depositing cerium boride powder by dispersing the composite powder in a solution.

Method of preparing cerium boride powder

A method of preparing cerium boride powder, according to the present invention, includes a first step for generating mixed powder by mixing at least one selected from among cerium chloride (CeCl.sub.3) powder and cerium oxide (CeO.sub.2) powder, at least one selected from among magnesium hydride (MgH.sub.2) powder and magnesium (Mg) powder, and boron oxide (B.sub.2O.sub.3) powder, a second step for generating composite powder including cerium boride (Ce.sub.xB.sub.y) and at least one selected from among magnesium oxide (MgO) and magnesium chloride (MgCl.sub.2), by causing reaction in the mixed powder at room temperature based on a ball milling process, and a third step for selectively depositing cerium boride powder by dispersing the composite powder in a solution.

CA-Y-CARBONATE NANOSHEETS, THEIR USE, AND SYNTHESIS

Nanosheets of Ca.sup.2+ and Y.sup.3+, with CO.sub.3.sup.2 in the interlayer with a uniform diameter and lengths of several tens of microns have been successfully synthesized in a hydrotalcite layer structure (a layered double hydroxide), using a hydrothermal method. The formation mechanism of lamellar CaYCO.sub.3.sup.2 layered double hydroxides (LDHs) depends on the molar ratio of Ca and Y and the reaction time and temperature. The resulting LDH materials exhibit excellent affinity and selectivity for heavy transition metal and metalloid ions.

Fluoride ion battery and method for producing fluoride ion battery
10790539 · 2020-09-29 · ·

An object of the present disclosure is to provide a fluoride ion battery of which power generating elements (a cathode active material layer, a solid electrolyte layer, and an anode active material layer) may be formed by two kinds of members: an electrode layer and a solid electrolyte layer. The present disclosure achieves the object by providing a fluoride ion battery comprising: an electrode layer that includes a first metal element or a carbon element and has capability of fluorination and defluorination; a solid electrolyte layer containing a solid electrolyte material, the solid electrolyte material including a second metal element with lower fluorination potential and defluorination potential than the potentials of the first metal element or the carbon element; and an anode current collector, in this order; and an anode active material layer being not present between the solid electrolyte layer and the anode current collector.

Rare earth silicate coatings solvothermally grown over high temperature ceramic components
10773999 · 2020-09-15 · ·

Methods are provided for forming high temperature coating over ceramic components, such as ceramic turbomachine components. In various embodiments, the method includes the step or process of at least partially filling a reactor vessel with a reaction solution containing a solution-borne rare earth cation source. A silicon-containing surface region of a ceramic component is submerged in the reaction solution, and a solvothermal growth process is carried-out. During the solvothermal growth process, the reaction solution is subject to elevated temperature and pressure conditions within the reactor vessel in the presence of a silicate anion source, which reacts with the solution-borne rare earth cation source to grow a rare earth silicate layer over the silicon-containing surface region of the ceramic component.

Method of manufacturing semiconductor material from mayenite
10766784 · 2020-09-08 · ·

A method of preparation of semiconductor material. The method includes: adding an organic substance containing a benzene ring and dodecacalcium hepta-aluminate (12CaO.7Al.sub.2O.sub.3 or C12A7) to a test tube, and sealing the test tube; heating the test tube to a temperature of 200-300 C., and holding the temperature for 1 to 3 hours; and continuously heating the test tube to a temperature of 900-1300 C., and holding the temperature for 10-120 hours.

Fluoride ion battery and method for producing fluoride ion battery
10727533 · 2020-07-28 · ·

A fluoride ion battery in which an occurrence of a short circuit is suppressed achieves the object by providing a fluoride ion battery including: an electrode layer that includes a first metal element or a carbon element and has capability of fluorination and defluorination; a solid electrolyte layer containing a solid electrolyte material, the solid electrolyte material including a second metal element with lower fluorination potential and defluorination potential than the potentials of the first metal element or the carbon element; and an anode current collector, in this order; and an anode active material layer being not present between the solid electrolyte layer and the anode current collector; and at least one of the solid electrolyte layer and the anode current collector includes a simple substance of Pb, Sn, In, Bi, or Sb, or an alloy containing one or more of these metal elements.

Phosphor containing Ce

A phosphor contains a crystal phase having a chemical composition Ce.sub.xM.sub.3-x-y.sub.6.sub.11-z. M is one or more elements selected from the group consisting of Sc, Y, La, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu. contains Si in an amount of 50 mol % or more of a total mol of . further contains Al. contains N in an amount of 80 mol % or more N of a total mol of . x satisfies 0<x0.6. y satisfies 0y1.0. z satisfies 0z1.0.

Cerium-based abrasive material and process for producing same
10717909 · 2020-07-21 · ·

A cerium-based abrasive that achieves a high polishing rate and suppresses the occurrence of surface defects such as scratches and pits and the deposition of the abrasive particles on the polished surface in surface polishing of glass substrates or the like, at low cost with a high production efficiency. The cerium-based abrasive includes a cubic composite rare earth oxide and a composite rare earth oxyfluoride, containing 95.0 to 99.5 mass % of total rare earth elements in terms of oxides, containing 54.5 to 95.0 mass % of cerium in terms of oxide, 4.5 to 45.0 mass % of lanthanum in terms of oxide, and 0.5 to 2.0 mass % of neodymium in terms of oxide relative to the total rare earth elements in terms of oxides, containing 0.5 to 4.0 mass % of fluorine atoms, and containing 0.001 to 0.50 mass % of sodium atoms relative to the total rare earth elements in terms of oxides.

Upgrade of yttrium in a mixed rare earth stream using iminodiacetic acid functionalized resin
10696562 · 2020-06-30 ·

Disclosed herein are methods, techniques, and processes for enhancing the purity of a mixed rare earth solution. In one embodiment the rare earth mixture may include Lanthanum, Cerium, Praseodymium, Neodymium, Promethium, Samarium, Europium, Gadolinium, Terbium, Dysprosium, Holmium, Erbium, Thulium, Ytterbium, Lutetium, Scandium, and/or Yttrium. In one embodiment, the resin is a chelating resin that interacts poorly with one or more rare earth elements. In one embodiment a rare earth is selectively excluded for example, Lanthanum (sometimes considered a transition metal), Cerium, Praseodymium, Neodymium, Promethium, Samarium, Europium, Gadolinium, Terbium, Dysprosium, Holmium, Erbium, Thulium, Ytterbium, Lutetium, Scandium, and/or Yttrium. In one embodiment, yttrium is selectively excluded from the column.