C22B1/00

Steel for wind power gear with improved purity and reliability, and smelting method therefor

Provided is steel for a wind power gear with improved purity and reliability. The chemical components thereof comprise, in percentages by mass: 0.15-0.19% of C, ≤0.4% of Si, 0.5-0.7% of Mn, ≤0.012% of P, ≤0.006% of S, 1.5-1.8% of Cr, 0.28-0.35% of Mo, 1.4-1.7% of Ni, and 0.02-0.04% of Al, with the balance being Fe and inevitable impurities. A smelting method therefor comprises adding raw materials to a converter for primary melting, transferring same to a refining furnace for refining, carrying out continuous casting after vacuum degassing, and transferring same to a gas protection furnace for electroslag remelting. According to the present invention, a pure electroslag master batch is obtained by continuous casting, and the purity of the material is further improved by means of an electroslag remelting procedure; and the prepared steel material is used in a wind power gear, such that the flaw detection pass rate is significantly increased, large-particle inclusions in the steel material are significantly reduced, and the inclusions are fine and dispersed.

Microwave-mechanical fluidization mining system and mining method for metal mines

A microwave-mechanical fluidization mining system and a mining method for metal mines. The microwave-mechanical fluidization mining system comprises a microwave pre-splitting mechanical mining system, a microwave separation system, a high-power microwave focused melting system and a goaf, wherein ore-waste rock mixtures mined by the microwave pre-splitting mechanical mining system are transported to the microwave separation system through a conveyor and an elevator on the microwave pre-splitting mechanical mining system, separated ores are transported to the high-power microwave focused melting system, and separated waste rocks are transported through a conveyor to the goaf for filling. Microwave pre-splitting mechanical mining is adopted instead of a traditional blasting mining method to increase an excavation speed and avoid the influence of blasting on the stability of surrounding rocks.

COLLOCATING A LARGE-SCALE DISSOCIATING REACTOR NEAR A GEOTHERMAL ENERGY SOURCE FOR PRODUCING GREEN LITHIUM FROM BRINES
20230304129 · 2023-09-28 · ·

Techniques for refining valuable materials from aqueous sources, along with corresponding apparatuses, are disclosed. The disclosed techniques enable “green” and “conflict-free” acquisition of critical minerals. These advantages are impactful in applications including refinement of rare materials such as certain metals, especially metals necessary for production of energy storage devices required to advance environmental goals, such as in the Paris climate agreement. The inventive concepts include economically viable approaches to refinement, as well as economically viable apparatuses. In some approaches, valuable materials such as metals are refined from salts obtained from aqueous sources. Power required to refine materials is provided by renewable energy sources. Real world implementations involve co-locating a dissociative reactor with a geothermal energy plant near an aquifer with salt(s) therein. Refined minerals are produced on site. Practice of the disclosed techniques reduce or eliminate many negative environmental impacts such as those incurred by legacy mining based techniques.

Method of processing and treatment of alunite ores
11753697 · 2023-09-12 ·

The alunite ore processing method consists of crushing, grinding and flotation of raw alunite ore. The enriched alunite ore is roasted at 520 to 620° C., the roasting time is 1 to 3 hours. The roasted alunite is leached with 5 to 20% sodium carbonate solution, which is in 100 to 110% of the stoichiometric amount required to bond the SO.sub.3 aluminum sulfate in the alunite with leaching conditions of 70-100° C. for 0.5-2.0 hours. The obtained slurry contains all of the potassium sulfate from the alunite and all of the sodium sulfate obtained from sodium carbonate. In the insoluble residue remains all aluminium oxide and residual rock. The sulfate solution is separated from the insoluble residue and is converted with potassium chloride to potassium sulphate (fertilizer) and kitchen salt. The insoluble residue is treated by the Bayer method without the use of an autoclave and results in aluminium oxide (alumina) and quartz sand.

Reactor system for separation and enrichment of minerals from a slurry containing minerals and other materials

A reactor system has a number of stations arranged to recover mineral particles in a slurry. The system includes a hopper to receive the slurry and barren media having hydrophobic coating to attract the mineral particles. The hopper provides a mixture of barren media and slurry to a tumbler arranged to stir the mixture in order to increase the contact between the slurry and the barren media so as to allow the mineral particles to attach to the barren media to form mineral laden media. The mineral laden media are conveyed to a rinsing station where water jets are used to wash the gangue materials off the mineral laden media. The rinsed mineral laden media are mixed with a surfactant so that the mineral particles are released from the mineral laden media. High-pressure water and air jets are then used to remove remaining surfactant from the released media.

Reactor system for separation and enrichment of minerals from a slurry containing minerals and other materials

A reactor system has a number of stations arranged to recover mineral particles in a slurry. The system includes a hopper to receive the slurry and barren media having hydrophobic coating to attract the mineral particles. The hopper provides a mixture of barren media and slurry to a tumbler arranged to stir the mixture in order to increase the contact between the slurry and the barren media so as to allow the mineral particles to attach to the barren media to form mineral laden media. The mineral laden media are conveyed to a rinsing station where water jets are used to wash the gangue materials off the mineral laden media. The rinsed mineral laden media are mixed with a surfactant so that the mineral particles are released from the mineral laden media. High-pressure water and air jets are then used to remove remaining surfactant from the released media.

Method for separating and extracting rare-earth and regenerating rare-earth polishing powder from rare-earth polishing powder waste

The invention relates to a method of separating and extracting rare-earths from rare-earth polishing powder waste and regenerating rare-earth polishing powder, which is characterized by: firstly, process the waste powder with first acid leaching, alkali roasting, and second acid leaching to separate and extract rare-earths from rare-earth polishing powder waste to obtain the leaching solution of rare-earth chloride; secondly, precipitate from the leaching solution with ammonia to remove impurities and hydrochloric acid solution to obtain the purified solution of rare-earth chloride; thirdly, co-precipitate from the solution acquired in the second step with hydrofluoric acid, ammonium bicarbonate, and dispersant to obtain the lanthanum cerium fluoro-carbonate; and finally, after drying, two-stage high-temperature calcination, and ball milling, the regenerated rare-earth polishing powder with decent polishing performance can be obtained. The total leaching efficiency of rare-earths in the rare-earth polishing powder waste of the present invention reaches more than 95%, and the total recovery efficiency of rare-earths reaches more than 93%, which realizes the efficient separation, extraction, and regeneration of rare-earths in the rare-earth polishing powder waste.

Bio-reduction of metal ores integrated with biomass pyrolysis

Some variations provide a composition for reducing a metal ore, the composition comprising a carbon-metal ore particulate, wherein the carbon-metal ore particulate comprises at least about 0.1 wt % to at most about 50 wt % fixed carbon on a moisture-free and ash-free basis, and wherein the carbon is at least 50% renewable carbon as determined from a measurement of the .sup.14C/.sup.12C isotopic ratio. Some variations provide a process for reducing a metal ore, comprising: providing a biomass feedstock; pyrolyzing the feedstock to generate a biogenic reagent comprising carbon and a pyrolysis off-gas comprising hydrogen or carbon monoxide; obtaining a metal ore comprising a metal oxide; combining the carbon with the metal ore, to generate a carbon-metal ore particulate; optionally pelletizing the carbon-metal ore particulate; and utilizing the pyrolysis off-gas to chemically reduce the metal oxide to elemental metal, such as iron. The disclosed technologies are environmentally superior to conventional processes based on coal.

BATTERY RECYCLING BY REDUCTION AND CARBONYLATION

The present invention relates to a process for the recovery of transition metals from battery materials comprising (0.1) providing a battery material which comprises oxidic nickel and/or cobalt compounds, (1.1) heating the battery material above 350° C. to yield a reduced material which contains nickel and/or cobalt in elemental form, (2.1) carbonylating the reduced material with carbon monoxide optionally in the presence of a reactive gas to yield a solid carbonylation residue and a volatile carbonyl which comprises nickel and/or cobalt carbonyl containing compounds, and (3.1) separating the volatile carbonyl from the solid carbonylation residue by evaporation.

Methods for simultaneous leaching and extraction of precious metals

The present application relates to methods for the simultaneous leaching and extraction of precious metals. For example, the present application relates to methods of leaching and extracting gold and/or palladium from a substance comprising gold and/or palladium such as a gold and/or palladium-containing ore in one step using a compound of Formula I: (I).