D21C3/00

METHOD FOR SEPARATING BIOMASS COMPONENTS BY TERNARY SYSTEM
20230323597 · 2023-10-12 ·

A method for separating biomass components by a ternary system, which relates to a technical field of biomass separation, and includes the following steps of: cooking and separating a biomass raw material by using a cooking liquor consisting of organic acid, small aromatic nucleophilic organic molecule and hydrogen peroxide to obtain solid residue and extracting solution, washing and screening the solid residue to obtain paper pulp, and separating and extracting lignin and/or hemicellulose from the extracting solution. This cooking system could effectively minimize the content of residual lignin and other compounds with chromophore groups in the obtained pulp, directly producing the high-whiteness pulp with excellent performance without additional bleaching process. In addition, the hemicellulose saccharides and high-activity lignin can be also obtained, so that the method has an important significance for realizing high value and industrialization of biomass resource utilization.

Cellulose filament-stabilized Pickering emulsions
11753770 · 2023-09-12 · ·

The present disclosure is directed to a Pickering emulsion comprising cellulose filaments. The heterogeneity of the cellulose filament material is critical and beneficial to the formation of stable emulsions. Emulsions with high stability can be prepared by controlling the CF surface properties. It is provided an emulsion comprising an internal phase dispersed in a continuous external phase and cellulose filaments located at the interface of the internal phase and the external phase, wherein the emulsion comprises 50% in volume or more of the internal phase and a method of producing same.

Strong and tough structural wood materials, and methods for fabricating and use thereof

A super strong and tough densified wood structure is formed by subjecting a cellulose-based natural wood material to a chemical treatment that partially removes lignin therefrom. The treated wood retains lumina of the natural wood, with cellulose nanofibers of cell walls being aligned. The treated wood is then pressed in a direction crossing the direction in which the lumina extend, such that the lumina collapse and any residual fluid within the wood is removed. As a result, the cell walls become entangled and hydrogen bonds are formed between adjacent cellulose nanofibers, thereby improving the strength and toughness of the wood among other mechanical properties. By further modifying, manipulating, or machining the densified wood, it can be adapted to various applications.

Multi-step process for the isolation of components from <i>Miscanthus</i>
11814790 · 2023-11-14 · ·

The invention relates to a process for the isolation of components from plant material of Miscanthus. The process comprises three subsequent extractions. The first extraction yields an extract comprising one or more compounds selected from the group of antioxidants, polyphenols, proteins, sterols, acids, alcohols, ketones, aldehydes and aromatic compounds. Thereafter, the plant material is subjected to two extractions with a metal hydroxide (e.g. NaOH), the first performed at a lower pH than the second. These steps yield a sugar fraction and a Iignin fraction, respectively. Finally, from the residue after the third extraction, cellulose is isolated.

MODIFIED SULFURIC ACID AND USES THEREOF

An aqueous composition comprising: sulfuric acid; a compound comprising an amine moiety; a compound comprising a sulfonic acid moiety; and a peroxide. Said composition being capable of delignifying biomass.

Method for extracting biomass
11377790 · 2022-07-05 · ·

Method for extraction of biomass with water in order to separate hemicelluloses from a fibrous structure. The biomass is impregnated under reduced pressure with the extraction fluid in order to prevent the degradation of the components to be extracted. During extraction the extract is circulated through the fiber matrix in order to remove unwanted components from the extract. The extract is reused for extracting untreated biomass in order to increase the consistency of the extract.

HYDROTHERMAL-MECHANICAL CONVERSION OF LIGNOCELLULOSIC BIOMASS TO ETHANOL OR OTHER FERMENTATION PRODUCTS

A low-cost process is provided to render lignocellulosic biomass accessible to cellulase enzymes, to produce fermentable sugars. Some variations provide a process to produce ethanol from lignocellulosic biomass (such as sugarcane bagasse or corn stover), comprising introducing a lignocellulosic biomass feedstock to a single-stage digestor; exposing the feedstock to a reaction solution comprising steam or liquid hot water within the digestor, to solubilize the hemicellulose in a liquid phase and to provide a cellulose-rich solid phase; refining the cellulose-rich solid phase, together with the liquid phase, in a mechanical refiner, thereby providing a mixture of refined cellulose-rich solids and the liquid phase; enzymatically hydrolyzing the mixture in a hydrolysis reactor with cellulase enzymes, to generate fermentable sugars; and fermenting the fermentable sugars to produce ethanol. Many alternative process configurations are described. The disclosed processes may be employed for other fermentation products.

HYDROTHERMAL-MECHANICAL CONVERSION OF LIGNOCELLULOSIC BIOMASS TO ETHANOL OR OTHER FERMENTATION PRODUCTS

A low-cost process is provided to render lignocellulosic biomass accessible to cellulase enzymes, to produce fermentable sugars. Some variations provide a process to produce ethanol from lignocellulosic biomass (such as sugarcane bagasse or corn stover), comprising introducing a lignocellulosic biomass feedstock to a single-stage digestor; exposing the feedstock to a reaction solution comprising steam or liquid hot water within the digestor, to solubilize the hemicellulose in a liquid phase and to provide a cellulose-rich solid phase; refining the cellulose-rich solid phase, together with the liquid phase, in a mechanical refiner, thereby providing a mixture of refined cellulose-rich solids and the liquid phase; enzymatically hydrolyzing the mixture in a hydrolysis reactor with cellulase enzymes, to generate fermentable sugars; and fermenting the fermentable sugars to produce ethanol. Many alternative process configurations are described. The disclosed processes may be employed for other fermentation products.

PROCESS FOR CONTINUOUSLY PREPARING A BROKEN-UP CELLULOSE-CONTAINING STARTING MATERIAL
20220243395 · 2022-08-04 ·

A method for continuously providing a treated cellulose-comprising starting material (110), in particular as starting material for manufacturing a cellulosic molded body (102), is provided. The method comprises: i) supplying (10) a cellulose-comprising starting material (101), which in particular is a solid matter, with a predefined composition to a reactor device (105), ii) continuously treating (20) the starting material (101) in the reactor device (105), to obtain the treated cellulose-comprising starting material (110), and iii) discharging (30) the treated cellulose-comprising starting material (110) from the reactor device (105).

COMMON PREPARATION OF LIGNOCELLULOSIC FEEDSTOCK AND A PRODUCT CONTAINING CELLULOSE BUT FREE FROM LIGNIN
20220243399 · 2022-08-04 ·

A method for providing a treated cellulose-comprising mixed starting material (110), in particular a mixed starting material (110) for forming a, in particular regenerated, cellulosic molded body (102) is described. The method comprises: i) providing (10) a first starting material (101a) which comprises a lignocellulosic raw material, ii) providing (1) a second starting material (101b) which comprises a cellulose-containing lignin-free product, iii) mixing (15) the first starting material (101a) and the second starting material (101b) to a mixed starting material (101), and iv) at least partially commonly treating (20) the first starting material (101a) and the second starting material (101b) for obtaining the treated mixed starting material (101), in particular a mixed pulp.