A process for producing bis(fluorosulfonyl) imide includes providing a solution comprising fluorosulfonic acid and urea, the solution maintained at a solution temperature from about 0° C. to about 70° C.; reacting the solution in the presence of a reaction medium at a reaction temperature from 80° C. to about 170° C. to produce a product stream including bis(fluorosulfonyl) imide, ammonium fluorosulfate and the reaction medium; separating the ammonium fluorosulfate from the product stream to produce an intermediate product stream; and separating the intermediate product stream into a concentrated product stream and a first recycle stream, the concentrated product stream including a higher concentration of bis(fluorosulfonyl) imide than the first recycle stream.

A process for producing bis(fluorosulfonyl) imide includes providing a solution comprising fluorosulfonic acid and urea, the solution maintained at a solution temperature from about 0° C. to about 70° C.; reacting the solution in the presence of a reaction medium at a reaction temperature from 80° C. to about 170° C. to produce a product stream including bis(fluorosulfonyl) imide, ammonium fluorosulfate and the reaction medium; separating the ammonium fluorosulfate from the product stream to produce an intermediate product stream; and separating the intermediate product stream into a concentrated product stream and a first recycle stream, the concentrated product stream including a higher concentration of bis(fluorosulfonyl) imide than the first recycle stream.

A tray assembly for improved gas/liquid contact in a chemical process tower includes a tray deck and a downcomer. A mixer is provided in the top of the downcomer and a distributor is attached to a floor of the downcomer. The mixer includes at least one mixing baffle parallel to an outlet weir on the tray. The distributor includes a plurality of spaced apart flow directing plates extending downwardly toward and spaced apart from the floor of the downcomer. In combination, the mixer and distributor effect even liquid flow across the surface of a subjacent tray deck.

The present disclosure provides an apparatus and method for producing a policosanol having a specific chromatographic fingerprint. The apparatus of the present disclosure has a feed tank and receiving tanks which are connected to a vacuum system. The method of the present disclosure is carried out by a high vacuum rectification process and includes: firstly, feeding a saponified crude alkanol into a melting tank in which the material is melted and then flows into the feed tank, and then injecting the material into a rectifying still using a delivery pump, followed by first rectification under vacuum condition and sequential collection of fractions at different phases from the tower top and stillage residue from the tower bottom; and after the completion of the rectification of the first batch crude product, carrying out second feeding on the basis of consistent vacuum in the feed tank and the rectifying tower.

The present disclosure relates to a pyrolysis bio-oil fractional condensation device and method capable of cooling medium self-circulation. The device includes a primary condensation system, a secondary condensation system and a cooling medium self-regulation heat exchange system. The primary condensation system uses the temperature-regulated cooling medium to condense the macromolecular tar by direct heat exchange with the pyrolysis volatiles. The condensed tar is heated, pushed and scraped with a rotary mechanism to prevent adhesion. The spray liquid in the secondary condensation system exchange heat with the uncondensed volatiles directly for secondary condensation. The cooling medium self-regulation heat exchange system realizes self-circulation and self-balance of the cooling medium mass flow and energy flow by integrating heat absorption during biomass raw material feeding and drying, heat release during volatiles condensation, and heat absorption during pyrolysis char cooling, and realized the independent operation of the condensation device in the mobile biomass pyrolysis system.

An impact test apparatus can be used to determine particle interfacial energies with varying relative air humidity. It was observed that capillary condensation increased the adhesive forces of hydrophilic materials. A systems humidity separation window was identified and the differences in interfacial energy for a hydrophilic surface and for a hydrophobic surface can be exploited in order to achieve the separation of particles. Separation and concentration of particles, particularly particles within a mineral ore body, can be obtained.

A process for the evaporation of a waste water stream having a mixture of inorganic and organic materials is provided. The process includes passing a waste water stream together with cleaning particles through a shell and tube heat exchanger of a forced circulation evaporator to mitigate scaling on the internal surface of the heat exchanger through which the stream of waste water flows. In another aspect, the invention concerns a forced circulation evaporator having a fluidized bed heat exchanger suitable for carrying out the method. The evaporator is located after a chemical process plant that produces a waste water containing a mixture of inorganic and organic materials, preferably after a dyestuff manufacturing plant.

A water processing and filling system includes a processing assembly configured to obtain and transport water; a filling assembly configured to receive water from the processing assembly; and a controller configured to: identify a presence of a container operatively adjacent to the filling assembly; determine whether an RFID tag on the container is valid; and if the RFID tag is valid, activate a flow of water from the filling assembly and into the container.

The present invention corresponds to a condensation device which in turn comprises said condensation device. The condensation device includes a first container (10), a heat exchanger (20) housed inside the first container, a condensing chamber (30) below the heat exchanger and a stirrer (40) housed inside the first container In an embodiment of the invention, the condensation device also comprises a second container, where both containers have a double wall. Moreover, the containers may include flanges for the inlet and outlet of substances into the containers and the heat exchanger, and for monitoring the substances inside the device.

An impact test apparatus can be used to determine particle interfacial energies with varying relative air humidity. It was observed that capillary condensation increased the adhesive forces of hydrophilic materials. A systems humidity separation window was identified and the differences in interfacial energy for a hydrophilic surface and for a hydrophobic surface can be exploited in order to achieve the separation of particles. Separation and concentration of particles, particularly particles within a mineral ore body, can be obtained.