B01D9/00

SPIRAL-FLOW TYPE FLUIDIZED-BED COOLING CRYSTALLIZATION SYSTEM

The disclosure discloses a spiral-flow type fluidized-bed cooling crystallization system. The system comprises a first fluidized-bed crystallizer, a second fluidized-bed crystallizer, a crystal growing tank, a centrifuge, a circulating pump, a flow control valve, a densimeter and the like, wherein vertical heat transfer pipes are arranged in the first fluidized-bed crystallizer and the second fluidized-bed crystallizer, and scraping particles are contained in the heat transfer pipes. According to the invention, feed liquid exchanges heat with a cooling medium through the vertical heat transfer pipes; meanwhile, spiral spray heads at the bottoms of the heat transfer pipes are used for enabling the feed liquid in the pipes to form a spiral flow field, and the scraping particles are efficiently driven to continuously impact and crush crystals attached to heat transfer wall faces, so the effects of heat transfer enhancement, heat transfer wall face self-cleaning.

Natural crystalline colorant and process for production

A crystalline pigment or colorant composition having high color intensity and/or low sugar content, and methods and processes of preparation. The composition may comprise purified fruit and/or vegetable color juices.

Freeze concentration for urine-based fertilizer production

A system for generating a concentrated product from a feedstock includes a feedstock chamber to which the feedstock is provided, a heat exchanger assembly in thermal communication with the feedstock chamber, the heat exchanger assembly being configured to freeze the feedstock in the feedstock chamber, an output flow arrangement configured to carry liquid from the feedstock chamber as the feedstock thaws, the output flow arrangement comprising a flow controller, a sensor disposed along the output flow arrangement or the heat exchanger assembly, the sensor being configured to measure a characteristic of the liquid, the characteristic being indicative of a solute concentration level of the liquid or the heat exchanger assembly, and a processor responsive to the characteristic and configured to control the flow controller to, based on the solute concentration level, direct the liquid passing through the output flow arrangement to define a plurality of products at different concentration levels, the plurality of products comprising the concentrated product.

SYSTEM FOR PRODUCING MAGNESIUM HYDROXIDE

Disclosed is a system for producing magnesium hydroxide including: a generation unit; and a recovery unit connected to the generation unit, wherein the generation unit has a reaction tank in which a calcium hydroxide slurry is added to water to be treated containing magnesium ions to crystallize magnesium hydroxide and to obtain a reaction slurry containing particles of magnesium hydroxide, and a sedimentation tank in which the reaction slurry is reserved to sediment the particles and to separate the reaction slurry into a separation slurry containing the particles at a high concentration and a separation liquid containing the particles at a low concentration, and wherein, in the recovery unit, an alkaline aqueous solution is added to the separation liquid to crystallize magnesium hydroxide and to obtain the reaction slurry and then the reaction slurry is reserved to sediment the particles and to recover the sedimented particles.

Production of lithium hydroxide and lithium carbonate
11708278 · 2023-07-25 · ·

Methods and systems for production of lithium hydroxide and lithium carbonate are described. One or more embodiments of the method include producing lithium hydroxide from potassium chloride, lithium chloride, and water. One or more embodiments of the method include producing lithium carbonate from potassium chloride, lithium chloride, water, and a carbon dioxide source. One or more embodiments of the method include producing lithium carbonate from sodium chloride, lithium chloride, water, and a carbon dioxide source.

Production of lithium hydroxide and lithium carbonate
11708278 · 2023-07-25 · ·

Methods and systems for production of lithium hydroxide and lithium carbonate are described. One or more embodiments of the method include producing lithium hydroxide from potassium chloride, lithium chloride, and water. One or more embodiments of the method include producing lithium carbonate from potassium chloride, lithium chloride, water, and a carbon dioxide source. One or more embodiments of the method include producing lithium carbonate from sodium chloride, lithium chloride, water, and a carbon dioxide source.

PROCESS FOR THE REMOVAL AND RECOVERY OF HESPERALOE EXTRACTIVES

Disclosed are soluble extractives prepared from non-woody plants of the genus Hesperaloe and processes for preparing the same. The extracts preferably comprise at least one saponin. In certain instances, the process includes providing biomass derived from non-woody plants of the genus Hesperaloe, milling the biomass, washing the biomass with a solvent to yield a crude extract and optionally further purifying the crude extract by filtration to remove water insoluble compositions such as fibers, fines, epidermal debris and lipids. Preferably, the composition extracted from Hesperaloe comprises 25(27)-dehydrofucreastatin, 5(6),25(27)-disdehydroyuccaloiside C, 5(6)-disdehydroyuccaloiside, C, furcreastatin, yuccaloiside, or a mixture thereof.

A METHOD OF OPERATING A CRYSTALLIZING VESSEL ASSEMBLY, AS WELL AS A CRYSTALLIZING VESSEL ASSEMBLY
20230001325 · 2023-01-05 · ·

A method of operating a crystallizing vessel assembly, said vessel assembly having a crystallizing vessel, and a rotor comprising a rotor shaft, said rotor including a plurality of rotor arms, said rotor arms having arms attached to the rotor shaft and scrapers attached at the arms. The crystals are grown on the inside of the vessel and the rotor is rotated to scrape said crystals off. To improve liquid flow inside the crystallizing vessel, a plurality of arms of the rotor arms are hollow arms, each arm of the plurality of arms including an inlet opening that is relatively close to the shaft and an outlet opening that is relatively far from the shaft.

ADDITIVE USED IN METHIONINE PREPARATION PROCESS, AND METHIONINE PREPARATION METHOD

The present disclosure relates to an additive used in a methionine preparation process, and a methionine preparation method. The additive provided by the present disclosure is a mixture containing components A, B, and C; component A has a structure represented by the following general formula (1); component B has a structure represented by the following general formula (2); component C is silicone oil; RCON(CH.sub.3)CH.sub.2CH.sub.2SO.sub.3Na (1). The methionine preparation method provided in the present invention comprises subjecting methionine to crystallization and/or recrystallization in the presence of the additive provided by the present disclosure. The additive provided by the present disclosure results in uniform emulsification, has good stability, can be used stably for a long time, and is suitable for a continuous crystallization process. The prepared methionine crystal has a good crystal form, a large bulk density, and good flowability. In addition, according to the methionine preparation method of the present disclosure, a crystallization system can operate continuously and stably for a long time without obvious foaming, and the crystallization process of the methionine product can proceed smoothly.

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PROCESS FOR SULFONATION OF 2-AMINOETHANOL HYDROGEN SULFATE ESTER TO PRODUCE TAURINE
20230227403 · 2023-07-20 ·

A process comprises continuously adding a first stream and a second stream to a sulfonation vessel, wherein the first stream comprises aminoethanol sulfate ester (AES) and the second stream comprises an aqueous solution of sodium sulfite (Na.sub.2SO.sub.3). The process comprises continuously mixing the AES and the aqueous solution of Na.sub.2SO.sub.3 in the sulfonation vessel, thus producing a mixture. The process comprises continuously subjecting the mixture to heat in the presence of an inert gas, thus converting the AES to the taurine via sulfonation. In an aspect, the AES has a residence time of no more than four hours in the sulfonation vessel. In an aspect the heating step is conducted at a temperature of at least 115° C. and a pressure of at least 200 psi.