A technique is provided, in which impure metal is efficiently separated and removed from titanium-containing raw material such as titanium slag or ilmenite and high titanium-containing raw material is produced. The method for improving quality of titanium-containing raw material containing slag, including steps of: oxidizing the titanium-containing raw material, selectively chlorinating impurities in the titanium-containing raw material, and separating and removing the impure chlorides to obtain high titanium-containing raw material. Alternatively, in this method, the oxidizing treatment and the selective chlorinating treatment are performed simultaneously.

The invention relates to a method for preparing high-melting-point metal powder through multi-stage deep reduction, and belongs to the technical field of preparation of powder. The method includes the following steps of mixing dried high-melting-point metal oxide powder with magnesium powder and performing a self-propagating reaction, placing an intermediate product into a closed reaction kettle, leaching the intermediate product with hydrochloric acid as a leaching solution so as to obtain a low-valence oxide Me.sub.xO precursor of the low-valence high-melting-point metal; uniformly mixing the precursor with calcium powder, pressing the mixture, placing the pressed mixture into a vacuum reduction furnace, heating the vacuum reduction furnace to 700-1200° C., performing deep reduction for 1-6 h, leaching a deep reduction product with hydrochloric acid as a leaching solution and performing treatment, so as to obtain the high-melting-point metal powder.

The invention relates to a method for preparing high-melting-point metal powder through multi-stage deep reduction, and belongs to the technical field of preparation of powder. The method includes the following steps of mixing dried high-melting-point metal oxide powder with magnesium powder and performing a self-propagating reaction, placing an intermediate product into a closed reaction kettle, leaching the intermediate product with hydrochloric acid as a leaching solution so as to obtain a low-valence oxide Me.sub.xO precursor of the low-valence high-melting-point metal; uniformly mixing the precursor with calcium powder, pressing the mixture, placing the pressed mixture into a vacuum reduction furnace, heating the vacuum reduction furnace to 700-1200° C., performing deep reduction for 1-6 h, leaching a deep reduction product with hydrochloric acid as a leaching solution and performing treatment, so as to obtain the high-melting-point metal powder.

The present disclosure broadly relates to a process for recovering scandium and/or vanadium values from various feedstocks. More specifically, but not exclusively, the present disclosure relates to a process for the selective recovery of scandium and/or vanadium values from a feedstock, the process comprising: leaching the feedstock in a sulfuric acid solution while simultaneously sonicating the sulfuric acid solution thereby producing a pregnant solution; and selectively removing scandium and vanadium compounds from the pregnant solution using a solvent extraction process.

A method includes forming a solution comprising a solvent and at least two elements selected from: scandium (Sc), yttrium (Y), one or more lanthanides, and one or more actinides. The method includes adding an effective amount of at least one polyoxometalate for forming complexes with at least one of the elements and adding an effective amount of a cation for causing precipitation of at least some of the complexes of one of the elements. Substantially all of another of the elements remains in solution during the precipitation of the at least some of the complexes of the one of the elements. A kit includes a polyoxometalate, a cation, and instructions for adding effective amounts of the polyoxometalate and the cation for separating at least two elements selected from the group consisting of: scandium (Sc), yttrium (Y), one or more lanthanides, and one or more actinides via a precipitation reaction.

A method includes forming a solution comprising a solvent and at least two elements selected from: scandium (Sc), yttrium (Y), one or more lanthanides, and one or more actinides. The method includes adding an effective amount of at least one polyoxometalate for forming complexes with at least one of the elements and adding an effective amount of a cation for causing precipitation of at least some of the complexes of one of the elements. Substantially all of another of the elements remains in solution during the precipitation of the at least some of the complexes of the one of the elements. A kit includes a polyoxometalate, a cation, and instructions for adding effective amounts of the polyoxometalate and the cation for separating at least two elements selected from the group consisting of: scandium (Sc), yttrium (Y), one or more lanthanides, and one or more actinides via a precipitation reaction.

The invention relates to a method for starting up a fluidized bed boiler, such as a circulating fluidized bed (CFB) or a bubbling fluidized bed (BFB) boiler, for operation with a predetermined concentration of ilmenite particles in the bed material. The invention also relates to a method for pre-oxidizing ilmenite, to pre-oxidized ilmenite and to the use of pre-oxidized ilmenite in a fluidized bed boiler.

The invention relates to a method for starting up a fluidized bed boiler, such as a circulating fluidized bed (CFB) or a bubbling fluidized bed (BFB) boiler, for operation with a predetermined concentration of ilmenite particles in the bed material. The invention also relates to a method for pre-oxidizing ilmenite, to pre-oxidized ilmenite and to the use of pre-oxidized ilmenite in a fluidized bed boiler.

The present invention is characterized by comprising: an acid leaching step for obtaining a leach liquid by causing leaching of, by means of an acid, a metal mixture at least containing vanadium and at least one type of a divalent or trivalent metal selected from nickel, cobalt, manganese, palladium, platinum, copper, and zinc; a complex generation step for adding an ammoniacal alkaline aqueous solution to the leach liquid for adjusting the pH to 10-12 and generating, in the alkaline aqueous solution, an ammine complex of a divalent or trivalent metal ion and an anion complex of a tetravalent and/or pentavalent vanadium ion; a divalent or trivalent metal recovery step for adding a carrier having a carboxyl group to the alkaline aqueous solution in which the ammine complex and the anion complex are generated, causing the divalent or trivalent metal ion in the ammine complex to be selectively adsorbed onto the carrier, and recovering the divalent or trivalent metal ion; and a vanadium recovery step for recovering vanadium from the anion complex contained in the alkaline aqueous solution after the divalent or trivalent metal ion is recovered.

The invention relates to a method for preparing high-melting-point metal powder through multi-stage deep reduction, and belongs to the technical field of preparation of powder. The method includes the following steps of mixing dried high-melting-point metal oxide powder with magnesium powder and performing a self-propagating reaction, placing an intermediate product into a closed reaction kettle, leaching the intermediate product with hydrochloric acid as a leaching solution so as to obtain a low-valence oxide Me.sub.xO precursor of the low-valence high-melting-point metal; uniformly mixing the precursor with calcium powder, pressing the mixture, placing the pressed mixture into a vacuum reduction furnace, heating the vacuum reduction furnace to 700-1200 C., performing deep reduction for 1-6 h, leaching a deep reduction product with hydrochloric acid as a leaching solution and performing treatment, so as to obtain the high-melting-point metal powder.