D01F13/00

Carbon fiber recycling system and method of operation

A method and apparatus for obtaining carbon fiber from carbon fiber waste (e.g., pre-preg and CFP waste). The method and apparatus selects, or is controlled to select, between using an oxygen free pyrolytic process to volatilize the epoxy resin or other matrix in which the fibers are held to liberate the fibers therefrom and, depending upon the type of pre-preg waste, using a reactor environment where the reactor atmosphere has about 1% to about 2% oxygen by volume. The reactor has a counterflow such that the carbon fibers are moved in one direction and the off gasses are moved in the opposite direction. A combination of steam at the reactor outlet and vacuum pressure at the reactor inlet create the counter flow.

METHODS AND SYSTEMS FOR PROCESSING MIXED TEXTILE FEEDSTOCK, ISOLATING CONSTITUENT MOLECULES, AND REGENERATING CELLULOSIC AND POLYESTER FIBERS
20230124761 · 2023-04-20 ·

Methods and systems of the present invention use mixed textile feedstock, which may include post-consumer waste garments, scrap fabric and/or other textile materials as a raw feed material to produce isolated cellulose and other isolated molecules having desirable properties that can be used and be used in the textile and apparel industries, and in other industries. A multi-stage process is provided, in which mixed textile feed material is subjected to one or more pretreatment stages, followed by at least two pulping treatments for isolating cellulose molecules and other molecular constituents, such as polyester. The isolated cellulose and polyester molecules may be used in a variety of downstream applications. In one application, isolated cellulose and polyester molecules are extruded to provide regenerated cellulose fibers and regenerated polyester fibers having desirable (and selectable) properties that are usable in various industrial applications, including textile production.

PREPARATION METHOD AND DEVICE FOR PRODUCING RECYCLED FIBER SPINNING SOLUTION USING SOLVENT METHOD

The invention discloses a preparation method and a production device for producing a recycled fiber spinning solution with using a solvent, which comprises two or more vertical wiped film evaporators (3, 4, . . . ) connected with a single horizontal cylindrical kneading reactor. The aqueous mixture of cellulose and solvent and auxiliary agent is prepared into a spinnable cellulose spinning dope, which is characterized by injecting the material mixture into two or more vertical wiped film evaporators and a horizontal cylindrical kneading reactor, each unit is preferably equipped with a separate condensing system, and the vacuum system can be separately configured to share a vacuum system.

PREPARATION METHOD AND DEVICE FOR PRODUCING RECYCLED FIBER SPINNING SOLUTION USING SOLVENT METHOD

The invention discloses a preparation method and a production device for producing a recycled fiber spinning solution with using a solvent, which comprises two or more vertical wiped film evaporators (3, 4, . . . ) connected with a single horizontal cylindrical kneading reactor. The aqueous mixture of cellulose and solvent and auxiliary agent is prepared into a spinnable cellulose spinning dope, which is characterized by injecting the material mixture into two or more vertical wiped film evaporators and a horizontal cylindrical kneading reactor, each unit is preferably equipped with a separate condensing system, and the vacuum system can be separately configured to share a vacuum system.

Recycling of acid-superbase conjugate ionic liquids by water removal in the lyocell spinning process

According to an example aspect of the present invention, there is provided A process for the production of a cellulose filaments or films, comprising the steps of dissolving a cellulose substrate in an ionic liquid consisting of the superbase cation 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-enium [mTBDH]+ and an anion to produce a solution forming a spinning dope, said anion being derived from an acid which is present at a stoichiometric excess to the superbase, extruding the spinning dope through a spinneret in a coagulation bath containing water to form filaments or films from the solution, withdrawing ionic liquid in an aqueous mixture with water from the coagulation bath, recovering the ionic liquid [mTBDH][OAc] from the aqueous mixture by removing water and optionally recycling the recovered ionic liquid to the dissolution step.

Recycling of acid-superbase conjugate ionic liquids by water removal in the lyocell spinning process

According to an example aspect of the present invention, there is provided A process for the production of a cellulose filaments or films, comprising the steps of dissolving a cellulose substrate in an ionic liquid consisting of the superbase cation 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-enium [mTBDH]+ and an anion to produce a solution forming a spinning dope, said anion being derived from an acid which is present at a stoichiometric excess to the superbase, extruding the spinning dope through a spinneret in a coagulation bath containing water to form filaments or films from the solution, withdrawing ionic liquid in an aqueous mixture with water from the coagulation bath, recovering the ionic liquid [mTBDH][OAc] from the aqueous mixture by removing water and optionally recycling the recovered ionic liquid to the dissolution step.

METHOD OF PRODUCING MYCELIUM TEXTILE FABRIC AND FABRICS AND PRODUCTS MADE THEREBY
20210403857 · 2021-12-30 · ·

A system and method for creating mycelium textile materials is disclosed, in which leftover, cutoff, and other materials used to create the textile materials that would otherwise be discarded are further used in a second process to create bonded mycelium boards. The system and method further reuse or recycle materials throughout the process of creating the mycelium textile fabric and bonded mycelium boards, thus keeping waste to a minimum.

Method for separating unreacted monomer from mixture solution including unreacted monomer

The present invention relates to an energy saving method for separating an unreacted monomer, by which an unreacted monomer may be easily recovered from a mixture solution including an unreacted monomer, and a separation system which is capable of performing the method.

Method for separating unreacted monomer from mixture solution including unreacted monomer

The present invention relates to an energy saving method for separating an unreacted monomer, by which an unreacted monomer may be easily recovered from a mixture solution including an unreacted monomer, and a separation system which is capable of performing the method.

SYSTEM AND METHOD OF PRODUCING CARBON NANOTUBES
20220144642 · 2022-05-12 ·

Method of producing short carbon nanotube fibers from a carbonaceous gas.