D21C3/00

PROCESS FOR PRODUCING REFINED COTTON WITH HIGH POLYMERIZATION DEGREE

A process for producing refined cotton with a high polymerization degree includes: a. selection of material; b. impurity removal; c. impregnation; d. pretreatment: compounding triethanolamine, sodium carbonate, copper sulfate and magnesium oxide in equal proportion to form a cooking compound adjuvant with a mass concentration of 0.2-0.5%, putting the cookingcompound adjuvant into a spherical digester together with the cotton linter subjected to the impregnation treatment, heating to 70 C, stopping heating, and subjecting to idling pretreatment for 40-60 min; e. cooking; f. cooling of the spherical digester; g. formulating a chlorine dioxide bleaching stabilization solution; h. a first stage of bleaching; I. alkali treatment; J. a second stage of bleaching; K. dechlorination; and 1. rolling and drying by baking.

METHOD AND PLANT FOR OBTAINING CELLULOSE FIBRES

The invention relates to a method for obtaining cellulose fibres from fibrous biomass, in which: the biomass is first subjected to thermo-pressure hydrolysis, preferably with steam explosion, in a thermo-pressure hydrolysis plant, and then separation of the fibrous sludge obtained from the thermo-pressure hydrolysis plant is carried out in at least one separation plant, wherein a press cake of cellulose fibres, preferably with a dry material content of over 20%, preferably of over 25%, and a filtrate of flowable, solids-rich thin sludge are obtained, and wherein the thin sludge is fed to a biogas plant as a fermentation substrate to obtain biogas. The invention also relates to a plant for carrying out this method.

TEMPERATURE-CONTROLLED DELIGNIFICATION OF BIOMASS
20220412001 · 2022-12-29 ·

A process to delignify biomass, said process comprising the steps of: providing a vessel; providing biomass comprising lignin, hemicellulose and cellulose fibers into said vessel; providing a aqueous acidic composition comprising a sulfuric acid component; providing a peroxide component; exposing said biomass to said sulfuric acid component and peroxide component, creating a reaction mass; allowing said sulfuric acid component and peroxide component to come into contact with said biomass for a period of time sufficient to a delignification reaction to occur and remove over 90 wt % of said lignin and hemicellulose from said biomass; and controlling the temperature of the delignification reaction to maintain it below 55° C.

Polysulfide Compositions and Processes for Making Same

An aqueous polysulfide composition comprises one or more inorganic polysulfides, wherein the amount of polysulfides in the composition is at least 30% by weight, preferably at least 35% by weight, more preferably at least 40% by weight, and wherein the amount of thiosulfate anions in the composition is at most 5% by weight, relative to the total weight of the composition. In one embodiment the weight ratio of polysulfides to thiosulfates in the aqueous composition is from 55/1 to 1.5/1. In another embodiment, the aqueous polysulfide composition has a pH of at least 10. A process for preparing an aqueous polysulfide composition comprises reacting a sulfide salt (c) with elemental sulfur to form one or more polysulfide salts. The compositions have many uses and are in particular useful in metal capturing, cyanide scavenging, soil remediation, water treatment, petroleum processing, leather processing, and making of paper pulp.

SYSTEM FOR THE PROCESSING AND RESUPPLY OF PULP AS WELL AS A METHOD FOR THE CONSTRUCTION THEREOF
20220389656 · 2022-12-08 ·

The present disclosure relates to a system for pulp processing and resupply of production-quality pulp to at least one fiber molding system, where the system is constructed in scalable modular form. For this, the system includes at least one supply module (110) and one or more process modules (120). The supply module (110) and the process modules (120) are equipped with a plurality of interfaces (150), matched to one another in each case, in order to connect supply and process modules (110, 120) to one another. This may guarantee the infrastructure supply of the process modules (120). The pulp or the constituents and starting materials may be received via at least one inlet (130) and transported between the process modules (120) to provide the production-quality pulp (160) via an outlet (140) for use by at least one fiber molding system.

Process for the treatment of lignocellulosic biomass

Lignocellulosic biomass can be fractionated for the purpose of increasing cellulose purity in the pulp, increasing native lignin content of the isolated lignin, and improving cellulose hydrolysis, by performing the steps of: (a) extracting the biomass with an extracting liquid comprising at least 20 wt % of a first organic solvent at a temperature below 100° C.; (b) treating the extracted biomass with a treatment liquid comprising a second organic solvent selected from lower alcohols, ethers and ketones, optionally water and optionally an acid, at a temperature between 120° C. and 280° C., and, optionally: (c) subjecting a cellulose-enriched product stream resulting from step (b) to enzymatic hydrolysis. The first and second organic solvent may be different or the same; in particular they comprise ethanol or acetone.

Process for the treatment of lignocellulosic biomass

Lignocellulosic biomass can be fractionated for the purpose of increasing cellulose purity in the pulp, increasing native lignin content of the isolated lignin, and improving cellulose hydrolysis, by performing the steps of: (a) extracting the biomass with an extracting liquid comprising at least 20 wt % of a first organic solvent at a temperature below 100° C.; (b) treating the extracted biomass with a treatment liquid comprising a second organic solvent selected from lower alcohols, ethers and ketones, optionally water and optionally an acid, at a temperature between 120° C. and 280° C., and, optionally: (c) subjecting a cellulose-enriched product stream resulting from step (b) to enzymatic hydrolysis. The first and second organic solvent may be different or the same; in particular they comprise ethanol or acetone.

Method to convert mechanical pulp derived waste material into value added cellulose products

According to an example aspect of the present invention, there is provided a process for the conversion of cellulosic waste material into a recycled cellulose product comprising the steps of cooking the waste material in a cooking liquor to remove lignin from the waste material and provide a delignified pulp, dissolving the delignified pulp in an ionic liquid to provide a spinning dope suitable for dry jet-wet spinning in an ionic liquid solution, and subjecting the spinning dope to a further processing step to provide a recycled cellulose product, said further step selected from the group of spinning cellulose fibers for use in textiles from the solution, extruding a film product for use in packaging, regenerating the dope as a hydrogel and regenerating the dope as an aerogel.

Method of producing chemical pulp
11473241 · 2022-10-18 · ·

A method of producing chemical pulp including at least the following steps: a) wood chips or other comminuted ligno-cellulosic fibrous material is treated with a polysulfide-containing cooking liquor in an impregnation stage at a temperature of 90-145° C., and b) slurry of fibrous material from step a) is heated into cooking temperature and cooked for producing pulp having a desired kappa number. After step a) mercaptide ions are added into the slurry of fibrous material and the fibrous material is treated at cooking temperature in step b).

EXTRACTION OF DELIGNIFIED, CELLULOSE-BASED FIBERS FROM NATURAL PLANT MATERIAL, AND MATERIALS INCORPORATING SUCH FIBERS
20230160141 · 2023-05-25 ·

A piece of natural plant material is subjected to one or more chemical treatments to remove substantially all lignin therefrom, thereby allowing the extraction of delignified, cellulose-based fibers. For example, the natural plant material can be a grass, such as bamboo or gladiolus. Subsequent drying of the extracted fiber densifies the structure, yielding improved mechanical properties. In some embodiments, the extracted fibers can be used, either alone or in combination with other materials, as a structural material. For example, the extracted fibers can be embedded within, infiltrated with, coated by, or otherwise combined with a polymer or concrete to form a composite material.