The present invention provides a paper ball-like graphene microsphere, a composite material thereof, and a preparation method therefor. Such paper ball-like graphene microspheres are obtained by chemically reducing graphene oxide microspheres to slowly remove oxygen-containing functional groups on the surface of the graphene oxide to avoid the volume expansion caused by rapid removal of the groups, thereby maintaining a tight bond between graphene sheets without separation; and removing the remaining small number of oxygen-containing functional groups and repairing defect structures in the graphene oxide sheets by means of high temperature treatment, such that the graphene structure becomes perfect at an ultrahigh temperature (2500 to 3000° C.), thereby further improving the bonding ability between the graphene sheets in the microspheres and achieving a dense structure.

A hierarchical porous honeycombed nickel oxide microsphere and a preparation method thereof are disclosed. The method includes mixing nickel sulfate hexahydrate, urea, water and glycerol, to obtain a mixed solution; subjecting the mixed solution to a hydrothermal reaction, to obtain a precursor; and calcining the precursor, to obtain the hierarchical porous honeycombed nickel oxide microspheres.

Described are composite photonic materials that incorporate magnetic nanoparticles inside hollow or solvent-filled nano-scale or micro-scale shells and methods of making and using such composite photonic materials. When these photonic materials are present in a magnetic field, they exhibit a change in reflected, scattered, and/or transmitted light as compared to when the materials are not in the presence of the magnetic field. This results in the materials appearing to have a different color, such as when observed by the human eye or a light detecting device, such as a camera.

Provided is a hollow inorganic particle having excellent strength despite having high porosity. Provided is a hollow inorganic particle including an outer shell, the thinnest part of the outer shell/the thickest part of the outer shell being 0.80 or more. The hollow inorganic particle according to the present technology can be produced by a production method including: a coating step of coating core particles made of an organic polymer with a silicone-based compound; and a core particle removal step of removing the core particles. The coating step includes: a dispersant addition step of adding a dispersant to a core particle dispersion; and, after the dispersant addition step, a surfactant addition step of adding a cationic surfactant.

The present disclosure relates to a carbon-based nanomaterial composition that may be formed from a gas mixture and a nitrogen powder. The gas mixture may include a carbon-based gas, an oxygen gas, and a hydrogen gas. The carbon-based nanomaterial composition may include nitrogen doped nanospheres.

The present invention provides zeolite hollow spheres in which zeolite crystals grow to form a framework of macropore through a hydrothermal crystallization process using the hydrophilic surface of a carbon sphere as a hard template, wherein the zeolite framework is an ordered, porous crystalline zeolite material with a number of channels or pores interconnected, which has two independent pore structures including mesopores and micropores. The zeolite hollow spheres of the present invention can be used for various purposes such as catalysts and adsorbents.

Particulate material comprising rough mesoporous hollow nanoparticles. The rough mesoporous hollow nanoparticles may comprise a mesoporous shell, the external surface of which has projections thereon, the projections having smaller sizes than the particle size. The particulate material may be used to deliver active agents, such as insecticides and pesticides. The active agents can enter into the hollow core of the particles and be protected from degradation by sunlight. The rough surface of the particles retains the particles on plant leaves or animal hair. Methods for forming the particles are also described. Carbon particles and methods for forming carbon particles are also described.

Methods for producing porous graphic carbon microspheres having improved separation properties over conventional porous graphitic carbons. The methods include dispersing a monovinyl aromatic monomer, a polyvinyl aromatic monomer, and an initiator in a solvent, contacting porous silica microspheres with the monomer dispersion for a time sufficient for the monomers to coat the porous silica microspheres, polymerizing the monomers to form copolymer coated microspheres, sulfonating the copolymer, pyrolyzing the sulfonated copolymer, digesting the carbon microspheres to dissolve the silica leaving porous carbon microspheres, pyrolyzing the porous carbon microspheres, and graphitizing the porous carbon microspheres to form porous graphitic carbon microspheres. Further provided are improved porous graphitic carbon microspheres and chromatography columns including the improved porous graphitic carbon microspheres described herein.

A system for post-processing carbon powders includes a fluidized-bed reactor having an interior containing a fluidized-bed region. The system may include a gas feed source, a gas inlet value, a gas-solid separator, and an energy source coupled to the fluidized-bed reactor. Carbon nano-particulates may be loaded, in powder form, into the fluidized-bed region prior to operation. The gas feed source may output a gas-phase mixture into the interior of the fluidized-bed reactor, and the energy source may electromagnetically excite the gas-phase mixture and generate a plasma-phase mixture formed in a plasma region positioned adjacent to or within the interior of the fluidized-bed reactor. The energy source may be positioned at one or more positions relative to the gas inlet valve.

The present invention relates to hollow calcium phosphate particles comprising a respective shell comprising calcium, phosphate, water, magnesium, and strontium. The particles have a mean diameter ranging from 400 nm to 1.5 μm. The invention also relates to methods of producing such particles and compositions comprising such particles.