C01P2004/84

Chemical-free production of hollow graphene balls
11603316 · 2023-03-14 · ·

Provided is a method of producing multiple isolated hollow graphene balls, comprising: (a) mixing multiple particles of a graphitic material and multiple particles of a solid polymer carrier material to form a mixture in an impacting chamber of an energy impacting apparatus; (b) operating the energy impacting apparatus to peel off graphene sheets from the graphitic material and transferring the graphene sheets to surfaces of solid polymer carrier material particles to produce graphene-coated polymer particles; (c) recovering the graphene-coated polymer particles from the impacting chamber; and (d) suspending the graphene-encapsulated polymer particles in a gaseous medium to keep the particles separated from each other while concurrently pyrolyzing the particles to thermally convert polymer into pores and carbon, wherein at least one of the graphene balls comprises a hollow core enclosed by a shell composed of graphene sheets bonded together by carbon.

LITHIUM COMPLEX OXIDE FOR LITHIUM SECONDARY BATTERY POSITIVE ACTIVE MATERIAL AND METHOD OF PREPARING THE SAME

A lithium complex oxide and method of manufacturing the same, more particularly, a lithium complex oxide effective in improving the characteristics of capacity, resistance, and lifetime with reduced residual lithium and with different interplanar distances of crystalline structure between a primary particle locating in an internal part of secondary particle and a primary particle locating on the surface part of the secondary particle, and a method of preparing the same.

LITHIUM-CONTAINING SILICON OXIDE COMPOSITE ANODE MATERIAL, METHOD FOR PREPARING SAME, AND LITHIUM ION BATTERY

A lithium-containing silicon oxide composite anode material has a core-shell structure which includes a core and a shell. The core includes nano-silicon, Li.sub.2SiO.sub.3 and Li.sub.2Si.sub.2O.sub.5, and the shell is a conductive carbon layer wrapping the core. The invention provides a lithium-containing silicon oxide composite anode material which is able to maximize the reversible capacity and has a long cycle life, and a lithium ion battery containing the lithium-containing silicon oxide composite anode material. The invention further provides a method for preparing a lithium-containing silicon oxide composite anode material, which is simple in process, environmentally friendly and free of pollution.

COMPOSITE PARTICLE AND METHOD OF PRODUCING COMPOSITE PARTICLE

The composite particle of the present invention includes an alumina particle having a card-house structure which is formed of three or more pieces of plate-like alumina and in which the pieces of plate-like alumina are fixed to each other; and an inorganic coating part provided on a surface of the plate-like alumina.

SECONDARY BATTERY, ELECTRONIC DEVICE, AND VEHICLE
20230129659 · 2023-04-27 ·

A positive electrode active material with high charge and discharge capacity is provided. A positive electrode active material with high charge and discharge voltage is provided. A power storage device that hardly deteriorates is provided. A highly safe power storage device is provided. A novel power storage device is provided. A positive electrode active material containing lithium, a plurality of transition metals, oxygen, and an impurity element. The positive electrode active material includes a first region including a surface portion and a second region provided inward from the first region, and the concentration of a transition metal is higher in the first region than in the second region. An impurity region is included between the first region and the second region.

Method for Producing Zirconia-Coated Titanium Oxide Fine Particles, Zirconia-Coated Titanium Oxide Fine Particles, and Use Thereof
20230128712 · 2023-04-27 ·

Provided is a method for producing a zirconia-coated titanium oxide fine particle dispersion which includes (1) a step of preparing a dispersion (1) of titanium oxide fine particles, (2) a step of adding, to the dispersion (1), 1 to 50 parts by mass of an aqueous peroxozirconic acid solution in terms of the mass of ZrO.sub.2 per 100 parts by mass of the titanium oxide fine particles, and then aging reaction fine particles (2a) obtained as a result of a reaction between the titanium oxide fine particles and the peroxozirconic acid to thereby obtain a dispersion (2) of a zirconia-coated titanium oxide fine particle precursor (2b), and (3) a step of adjusting the dispersion (2) to have a solid concentration of 0.01 to 10 mass % and then hydrothermally treating the resulting dispersion (2).

Lithium cobalt-based positive electrode active material, preparation method thereof, positive electrode and secondary battery including the same

A lithium cobalt-based positive electrode active material is provided. The lithium cobalt-based positive electrode active material includes a core portion including a lithium cobalt-based oxide represented by Formula 1 and a shell portion including a lithium cobalt-based oxide represented by Formula 2, wherein the lithium cobalt-based positive electrode active material includes 2500 ppm or more, preferably 3000 ppm or more of a doping element M based on the total weight of the positive electrode active material. An inflection point does not appear in a voltage profile measured during charging/discharging a secondary battery including the lithium cobalt-based positive electrode active material.

Coating composition and optical member

There are provided a coating composition being possible to form a cured film which has excellent transparency and weather resistance, and especially hardness. A coating composition obtained by which a silicon-containing substance as a component (M) and a silica colloidal particle having a primary particle diameter of 2 to 80 nm as a component (S) are mixed, and then the component (M) is hydrolyzed, and the resulting aqueous solution is subsequently mixed with a colloidal particle (C) wherein a component (F) is a modified metal oxide colloidal particle (C) having a primary particle diameter of 2 to 100 nm, which includes a metal oxide colloidal particle (A) having a primary particle diameter of 2 to 60 nm as a core, whose surface is coated with a coating (B) formed of an acidic oxide colloidal particle.

Particles with improved colour shielding

The present invention relates to particles comprising a core, in particular a magnetic core, and a first coating of a first shell material, wherein a second coating of a second shell material is applied to the surface of the first coating facing away from the core, the second shell material is different from the first shell material and has a higher refractive index than the first shell material.

Glitter pigment, pigment-containing composition, and pigment-containing painted product

The present invention provides a new glitter pigment suitable for providing high-brightness whitish reflected light. The glitter pigment according to the present invention includes: a flaky substrate 1; and a silicon oxide layer 2 and a titanium oxide layer 3 formed in this order on the flaky substrate 1, wherein in the case where the flaky substrate is the glass flake, the glass flake has a thickness of 284 to 322 nm, the silicon oxide layer has a thickness of 89 to 109 nm, and the titanium oxide layer has a thickness of 51 to 86 nm. In the case where the flaky substrate is the alumina flake, the alumina flake has a thickness of 260 to 280 nm, the silicon oxide layer has a thickness of 79 to 102 nm, and the titanium oxide layer has a thickness of 47 to 87 nm.