C04B2235/48

Porous carbon and method of manufacturing same

A porous carbon that has an extremely high specific surface area while being crystalline, and a method of manufacturing the porous carbon are provided. A porous carbon has mesopores 4 and a carbonaceous wall 3 constituting an outer wall of the mesopores 4, wherein the carbonaceous wall 3 has a portion forming a layered structure. The porous carbon is fabricated by mixing a polyamic acid resin 1 as a carbon precursor with magnesium oxide 2 as template particles; heat-treating the mixture in a nitrogen atmosphere at 1000° C. for 1 hour to cause the polyamic acid resin to undergo heat decomposition; washing the resultant sample with a sulfuric acid solution at a concentration of 1 mol/L to dissolve MgO away; and heat-treating the noncrystalline porous carbon in a nitrogen atmosphere at 2500° C.

HIGH PURITY POLYSILOCARB MATERIALS, APPLICATIONS AND PROCESSES

Organosilicon chemistry, polymer derived ceramic materials, and methods. Such materials and methods for making polysilocarb (SiOC) and Silicon Carbide (SiC) materials having 3-nines, 4-nines, 6-nines and greater purity. Processes and articles utilizing such high purity SiOC and SiC.

High Purity SiOC and SiC, Methods Compositions and Applications

Organosilicon chemistry, polymer derived ceramic materials, and methods. Such materials and methods for making polysilocarb (SiOC) and Silicon Carbide (SiC) materials having 3-nines, 4-nines, 6-nines and greater purity. Processes and articles utilizing such high purity SiOC and SiC.

HIGH-ENTROPY CARBIDE CERAMIC AND RARE EARTH-CONTAINING HIGH-ENTROPY CARBIDE CERAMIC, FIBERS AND PRECURSORS THEREOF, AND METHODS FOR PREPARING THE SAME
20230088418 · 2023-03-23 ·

Provided are a high-entropy carbide ceramic, a rare earth-containing high-entropy carbide ceramic, fibers thereof, precursors thereof, and preparation methods thereof. The precursor includes at least four elements selected from Ti, Zr, Hf, V, Nb, Ta, Mo, and W, with each metal element accounting for 5-35% of the total molar quantity of metal elements in the precursor. The rare earth-containing high-entropy carbide ceramic precursor includes at least four transition metal elements and at least one rare-earth metal element. The high-entropy ceramic is a single-crystal-phase high-performance ceramic prepared from the precursor, with each element being homogenously distributed at molecular level. The method for preparing the high-entropy ceramic fiber includes uniformly mixing high-entropy carbide ceramic precursor containing target metal elements with spinning aid and solvent to prepare a spinnable precursor solution, followed by spinning, pyrolyzation, and high-temperature solid solution to prepare the high-entropy carbide ceramic fiber.

POLYMER-DERIVED CERAMIC FIBERS AND METHODS OF PREPARING THE SAME
20220340494 · 2022-10-27 ·

Ceramic matrix composite (CMC) materials are a desired solution for lightweight and high temperature applications. CMC materials can be reinforced with polymer-derived ceramic (PDC) fibers, which advantageously possess intrinsic thermal stability and high mechanical strength. Carbon-rich SiOC and SiOCN fibers were synthesized via hand-drawing and electrospinning polymer pyrolysis of a hybrid precursor materials with the aid of a spinning reagent. The prepared fibers are crosslinked and pyrolyzed for polymer-to-ceramic conversion.

COMPOSITE MEMBER
20220340492 · 2022-10-27 ·

A composite member includes an inorganic matrix part made from an inorganic substance and a dispersed component present in a dispersed state within the inorganic matrix part and having elasticity, wherein a material making up the dispersed component has a modulus of elasticity in tension of 100 Pa or more and 3.5 GPa or less. The composite member has a porosity of 20% or less in a section of the inorganic matrix part.

Method for manufacturing sintered body, structure, and composite structure
11607728 · 2023-03-21 · ·

A method for manufacturing a sintered body, the method including heating a mixture that contains a plurality of particles of a metal oxide having a spinel-type structure, and a metal acetylacetonate under pressure at a temperature of from a melting point or higher of the metal acetylacetonate to 600° C. or lower, to form a sintered body that contains the metal oxide having the spinel-type structure.

BIOCARBON BLENDS WITH OPTIMIZED FIXED CARBON CONTENT, AND METHODS FOR MAKING AND USING THE SAME
20220340818 · 2022-10-27 ·

In some variations, the invention provides a biocarbon composition comprising a low fixed carbon material with a fixed carbon concentration from 20 wt % to 55 wt %; a high fixed carbon material with a fixed carbon concentration from 50 wt % to 100 wt % (and higher than the fixed carbon concentration of the low fixed carbon material; from 0 to 30 wt % moisture; from 0 to 15 wt % ash; and from 0 to 20 wt % of one or more additives (such as a binder). Some variations provide a process for producing a biocarbon composition, the process comprising: pyrolyzing a first biomass-containing feedstock to generate a low fixed carbon material; separately pyrolyzing a second biomass-containing feedstock to generate a high fixed carbon material; blending the low fixed carbon material with the high fixed carbon material, thereby generating an intermediate material; optionally, blending one or more additives into the intermediate material; optionally, drying the intermediate material; and recovering a biocarbon composition containing the intermediate material or a thermally treated form thereof.

METHOD FOR PRODUCING ARTICLE CONTAINING SILICON CARBIDE AS MAIN CONSTITUENT, AND RAW MATERIAL POWDER USED IN THE METHOD
20220324135 · 2022-10-13 ·

A method for producing an article containing silicon carbide as the main constituent includes a plurality of sets of steps of forming a layer of a raw material powder and irradiating the layer with laser light according to three-dimensional model data. The low material powder is a mixture of silicon carbide powder, metallic silicon powder, and carbon powder. The laser light used in the step of irradiation with laser light has a spatial laser power density of 11 J/mm.sup.3 to 50 J/mm.sup.3.

Graphite-containing refractory and method of producing graphite-containing refractory

A method of producing a graphite-containing refractory within which carbon fiber bundles are placed, the graphite constituting 1% to 80% by mass, the method including a bundling step of bundling carbon fibers to form the carbon fiber bundles; a mixing step of mixing a refractory raw material with graphite to prepare a graphite-containing refractory raw material; a pressing step of pressing the graphite-containing refractory raw material in which the carbon fiber bundles are placed to prepare a formed product; and a drying step of drying the pressed product, wherein the bundling step includes bundling 1000 to 300000 of the carbon fibers with a fiber diameter of 1 to 45 μm/fiber to form carbon fiber bundles 100 mm or more in length.