C07C45/512

PROCESS FOR PREPARING CYCLODODECANONE
20190345101 · 2019-11-14 ·

The invention relates to a method for producing cyclododecanone (CDON). During the production, contaminated cyclododecane (CDAN) is produced. This can be separated from CDON by distillation (CDAN-containing fraction). The separation of CDAN and impurities such as 13-oxabicyclo [7.3.1]tridacane occurs by crystallizing out CDAN from the CDAN-containing fraction.

Production of farnesol

The present invention relates to an improved way for the production of farnesol.

Production of farnesol

The present invention relates to an improved way for the production of farnesol.

OXY-COPE REARRANGEMENT FOR THE MANUFACTURE OF INSECTICIDAL CYCLOPENTENE COMPOUNDS

Compounds of formula I

##STR00001##

a process for preparation of compounds of formula I; precursor compounds of formula II

##STR00002##

a process for preparation of precursor compounds of formula II; compounds of formula III

##STR00003##

a process for the preparation of compounds of formula IV from compounds of formula III

##STR00004##

and the use of compounds of formula I for the preparation of compounds of formula IV.

OXY-COPE REARRANGEMENT FOR THE MANUFACTURE OF INSECTICIDAL CYCLOPENTENE COMPOUNDS

Compounds of formula I

##STR00001##

a process for preparation of compounds of formula I; precursor compounds of formula II

##STR00002##

a process for preparation of precursor compounds of formula II; compounds of formula III

##STR00003##

a process for the preparation of compounds of formula IV from compounds of formula III

##STR00004##

and the use of compounds of formula I for the preparation of compounds of formula IV.

Reaction sequence for the synthesis of nootkatone, dihydronootkatone, and tetrahydronootkatone

An inexpensive, stereoselective synthesis for nootkatone, tetrahydronootkatone, and their derivatives is disclosed utilizing ozonolysis. The starting materials used in the synthesis are inexpensive and the reactions are commercially feasible and amenable to scaling up. The principal starting material, ()--Pinene, is on the GRAS list (generally recognized as safe).

Reaction sequence for the synthesis of nootkatone, dihydronootkatone, and tetrahydronootkatone

An inexpensive, stereoselective synthesis for nootkatone, tetrahydronootkatone, and their derivatives is disclosed utilizing ozonolysis. The starting materials used in the synthesis are inexpensive and the reactions are commercially feasible and amenable to scaling up. The principal starting material, ()--Pinene, is on the GRAS list (generally recognized as safe).

Method for producing acrolein and/or acrylic acid from glycerol

The invention relates to the production of acrolein and/or acrylic acid from glycerol, and more particularly to a method for continuous production of a stream comprising acrolein by dehydration of glycerol, comprising cycles of reaction and regeneration of a dehydration catalyst.

Method for recovering phenol and acetone from cracking reaction product of bisphenol-A residue

Disclosed is a method for recovering phenol and acetone from the cracking reaction product of bisphenol-A residue, by which economic feasibility and efficiency may be improved by utilizing a phenol/acetone purification process used for preparing bisphenol-A.

Method for recovering phenol and acetone from cracking reaction product of bisphenol-A residue

Disclosed is a method for recovering phenol and acetone from the cracking reaction product of bisphenol-A residue, by which economic feasibility and efficiency may be improved by utilizing a phenol/acetone purification process used for preparing bisphenol-A.