The present disclosure relates to a method for forming a glass, ceramic or composite material. The method may involve initially forming a plurality of tubes and then performing a coating operation to coat the plurality of tubes with materials containing metal or metalloid elements, including inorganic compounds, organometallic compounds, or coordination complexes to form coated tubes. The method may further include performing at least one of a thermal operation or a thermochemical operation on the coated tubes to form a solid glass, ceramic, or composite structure with dimensions representing at least one of a rod or fiber.

The present application provides a process of fabrication of erbium and ytterbium-co-doped multielements silica glass based cladding-pumped fiber for use as a highly efficient high power optical amplifier.

Laser waveguides, methods and systems for forming a laser waveguide are provided. The waveguide includes an inner cladding layer surrounding a central axis and a glass core surrounding and located outside of the inner cladding layer. The glass core includes a laser-active material. The waveguide includes an outer cladding layer surrounding and located outside of the glass core. The inner cladding, outer cladding and/or core may surround a hollow central channel or bore and may be annular in shape.

A photodarkening-resistant ytterbium-doped quartz optical fiber and a method for preparing such a fiber are provided. Glass of a photodarkening-resistant ytterbium-doped quartz optical fiber core rod includes at least Yb.sub.2O.sub.3, Al.sub.2O.sub.3, P.sub.2O.sub.5, SiO.sub.2. The proportions of Yb.sub.2O.sub.3, Al.sub.2O.sub.3, and P.sub.2O.sub.5 in the entire substance are Yb.sub.2O.sub.3: 0.05-0.3 mol %, Al.sub.2O.sub.3: 1-3 mol %, and P.sub.2O.sub.5: 1-5 mol %, respectively. In the preparation method for the photodarkening-resistant ytterbium-doped quartz optical fiber, a sol-gel method and an improved chemical vapor deposition method are combined. By using the molecular-level doping uniformity and the low preparation loss thereof respectively, ytterbium ions, aluminum ions and phosphorus ions are effectively doped in a quartz matrix, thereby effectively solving the problems in the optical fiber of high loss, photodarkening caused by cluster or the like, and a central refractive index dip.

A manufacturing method for an optical fiber, includes: drawing, while heating in a heating furnace, a lower end of an optical fiber preform that is to be an optical fiber having a core consisting of silica glass containing a rare earth element compound. The heating furnace has a temperature profile in which a temperature of the heating furnace increases to a maximum temperature T.sub.max and then decreases from an upstream side of the heating furnace toward a downstream side of the heating furnace. The temperature profile has a changing point at which the temperature decreases more steeply on the downstream side from a position where the maximum temperature T.sub.max is reached. At the maximum temperature, a temperature of the silica glass is higher than or equal to a glass transition temperature and the silica glass is in a single phase.

A method for producing a component with portions of a rare earth metal-doped quartz glass, an intermediate product containing voids and consisting of a SiO.sub.2 raw material doped with rare earth metal is introduced into a sinter mold the interior of which is bordered by a carbonaceous mold wall, and is melted therein into the component by gas pressure sintering at a maximum temperature above 1500 C. A shield is arranged between the mold wall and the intermediate product. In order to indicate a modified gas pressure sintering method that ensures the production of rare earth metal-doped quartz glass with reproducible properties, a bulk material of amorphous SiO.sub.2 particles with a layer thickness of at least 2 mm is used as the shield, the softening temperature thereof being at least 20 C. higher than the softening temperature of the doped SiO.sub.2 raw material, and the bulk material being gas-permeable at the beginning of the melting of the intermediate product, and the bulk material sintering during melting into an outer layer that is gas-tight to a pressure gas.

In known methods for producing a glass component, a void-containing intermediate product containing doped or non-doped SiO.sub.2 is inserted into a sheath tube composed of glass, which has a longitudinal axis and an inner bore, and is thermally treated therein. In order to subject the intermediate product to a thermal and/or reactive treatment that is reproducible and uniform in its effect from this starting point, it is proposed in one embodiment that into the sheath tube's inner bore a first gas-permeable gas diffuser is inserted which is displaceable along the sheath tube's longitudinal axis and is pressed against the intermediate product during the thermal treatment.

The present invention provides a method for manufacturing an optical fiber base material and an optical fiber base material, the method including: arranging a rod containing SiO.sub.2 family glass for core, in a container; pouring a SiO.sub.2 glass raw material solution for cladding layer and a hardener into the container, the glass raw material solution containing a hardening resin; solidifying the glass raw material solution through a self-hardening reaction; and then drying the solidified material and heating the solidified material in chlorine gas, to manufacture an optical fiber base material in which a SiO.sub.2 cladding layer is formed in an outer periphery of the rod containing SiO.sub.2 family glass for core.

A method for preparing a doped optical fibre preform includes formulating, a rare earth material or a functional metal material and a co-doping agent into a doping solution, mixing a high-purity quartz powder with the doping solution, drying same at a temperature of 100 C.-150 C. for 12-48 hours, crushing and screening the same to obtain a doped quartz powder; depositing the doped quartz powder onto the surface of a target rod to form a doped core layer; replacing the doped quartz powder with the high-purity quartz powder, and depositing the high-purity quartz powder onto the surface of the doped core layer to form a quartz outer cladding; and removing the target rod, and gradually collapsing the entirety formed from the doped core layer and the quartz outer cladding at a high temperature to obtain the doped optical fibre preform.

A microheater comprises an optical fiber including a rare earth-doped glass core surrounded by a glass cladding. The rare earth-doped glass core comprises a rare earth dopant at a concentration sufficient for luminescence quenching such that, when the rare earth dopant is pumped with light at an absorption band wavelength, at least about 90% of absorbed pump light is converted into heat.