C04B35/62884

ELECTROSTATIC FILAMENT DISPERSAL FOR CMC APPLICATIONS

A method of preparing a woven fabric material for use in a ceramic matrix composite includes passing a desized woven fabric tape having a first inter-filament spacing through a dispersal module configured to transform the desized woven fabric tape into a dispersed woven fabric tape having a second inter-filament spacing greater than the first inter-filament spacing. The dispersal module includes a first charging element with a charged surface and disposed to apply an electric charge to the desized woven fabric tape. The method further includes applying a polymer binder to the dispersed woven fabric tape to create a stabilized woven fabric tape having the second inter-filament spacing.

HOMOGENEOUS COMPOSITE MICROSTRUCTURE
20230019485 · 2023-01-19 ·

A method of preparing a woven ceramic fabric for use in a ceramic matrix composite includes transforming a woven fabric sheet having a first tow architecture into a separated woven fabric sheet having a second tow architecture, the first tow architecture including a plurality of warp tows and a plurality of weft tows, and the second tow architecture including a plurality of warp subtows and/or a plurality of weft subtows. Transforming the woven fabric sheet includes separating at least some of the plurality of warp tows and/or the plurality of weft tows into a greater number of corresponding warp subtows and/or weft subtows, respectively, such that second tow architecture includes more warp subtows and/or weft subtows than the first tow architecture comprises warp tows and weft tows, and wherein each of the warp subtows and/or weft subtows includes fewer filaments than corresponding warp tow and/or weft tow. Each of the plurality of warp subtows and/or weft subtows is spaced apart from the closest adjacent warp subtow and/or weft subtow, respectively, a distance of 25 to 230 microns.

METHOD OF FABRIC PROCESSING FOR IMPROVED CMC INFILTRATION
20230013205 · 2023-01-19 ·

A method of preparing a woven fabric material for use in a ceramic matrix composite includes securing a woven fabric tape in tension across a roller, the roller having an outer surface with a plurality of spiked protrusions extending radially therefrom, each of the plurality of spiked protrusions having a diameter between 10 microns and 500 microns. The method further includes passing the woven fabric along the roller, such that the roller rotates with the passing of the woven fabric tape, thereby impinging the spiked protrusions into the woven fabric tape, and separating filaments within tows of the woven fabric tape by penetration of at least one of the spiked protrusions into the woven fabric tape, such that filaments within various tows of the woven fabric tape are pushed apart to form a separated woven fabric tape with a greater number of tows per unit area than the woven fabric tape.

CALCIUM LANTHANUM SULFIDE NANO-POWDERS, METHOD OF MAKING, AND OPTICALLY TRANSMISSIVE BODY FORMED THEREFROM
20230219824 · 2023-07-13 ·

A method for producing calcium lanthanum sulfide (CLS) nano powder and optical ceramics formed therefrom. The method includes the steps of mixing a lanthanum precursor and calcium precursor in water to obtain a solution and adding a sulfide precursor to the solution. Upon adding the sulfide precursor, stirring the solution for 5-25 minutes at 55-95° C. to obtain a mixture. The mixture is then introduced into a muffle furnace, preheated at 400-600° C., and the mixture is kept for 15-50 minutes to obtain nano powder. The nano powder can be annealed and subjected to spark plasma sintering to obtain the optical ceramics.

Continuous multiple tow coating reactor

A tow coating reactor system includes a reactor for receiving fiber tow, a wedge situated adjacent the reactor and configured to receive the tow at a tip end, such that as the tow moves across the wedge, the wedge spreads the tow into a plurality of sub-tows.

Ceramic matrix composite and method of manufacturing the same

A ceramic matrix composite includes a substrate which contains a fibrous body made of silicon carbide fiber, and a matrix which is formed in the substrate, and which contains silicon carbide and a silicon material made of silicon or a binary silicon alloy.

CVI matrix densification process

Disclosed herein is a chemical vapor infiltration method including flowing ceramic precursors through a preform and depositing a matrix material on the preform at a first gas infiltration pressure, increasing the gas filtration pressure to a second gas infiltration pressure, and lowering the gas infiltration pressure to a third gas infiltration pressure which is intermediate to the first and second gas infiltration pressures.

Fiber having integral weak interface coating, method of making and composite incorporating the fiber

Disclosed is a method of coating a high temperature fiber including depositing a base material on the high temperature fiber using atomic layer deposition, depositing an intermediate material precursor on the base material using molecular layer deposition, depositing a top material on the intermediate material precursor or the intermediate layer using atomic layer deposition, and heat treating the intermediate precursor. The intermediate material in the final coating includes a structural defect, has lower density than the top material or a combination thereof. Also disclosed are the coated high temperature fiber and a composite including the high temperature fiber.

Method of producing core-shell particles and multilayer ceramic electronic component including core-shell particles

A method of producing a core-shell particle includes introducing a barium titanate-based base powder and an additive to a reactor, and exposing the barium titanate-based base powder and the additive to a thermal plasma torch to obtain core-shell particles including a core portion having barium titanate (BaTiO.sub.3) and a shell portion including the additive and formed on a surface of the core portion.

SHAPE FORMING OPF PREFORM

A method for manufacturing a C/C part includes fabricating an oxidized PAN fiber preform comprising a stack of sheets of multi-axial, non-crimp, OPF fabric. The method includes positioning the oxidized PAN fiber preform with a female forming tool, the female forming tool comprising a die recess, and forming the oxidized PAN fiber preform into a shaped body. The shaped body is removed from the female forming tool and moved into a graphite fixture for carbonization. The carbonized shaped body may also be densified into the final C/C part. The carbonized shaped body can also be placed in a perforated graphite fixture for densification and removed from the perforated graphite fixture between densification processes for machining and for facilitating further densification.