Patent classifications
C07C29/84
SYSTEMS AND METHODS FOR PRODUCING ULTRA-LOW CARBON INTENSITY ETHANOL
Processes and systems for producing cellulosic ethanol from byproducts of an ethanol production facility and methods and systems for more effectively integrating traditional ethanol production facilities with cellulosic ethanol production to reduce overall energy use and produce ethanol with lower carbon intensity scores.
SYSTEMS AND METHODS FOR PRODUCING ULTRA-LOW CARBON INTENSITY ETHANOL
Processes and systems for producing cellulosic ethanol from byproducts of an ethanol production facility and methods and systems for more effectively integrating traditional ethanol production facilities with cellulosic ethanol production to reduce overall energy use and produce ethanol with lower carbon intensity scores.
Nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol, preparation method thereof, and method of synthesizing terpinene-4-ol using the same
The present invention discloses a nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol as well as a preparation method and method of synthesizing terpinene-4-ol using the same. The preparation method includes the steps of catalyst preparation, terpinene-4-ol synthesis and the like are disclosed in the present invention. The preparation method includes the following steps: firstly, preparing a mixed colloid of TiO.sub.2 and SiO.sub.2 by using a sol-gel method, and then centrifuging, washing, drying and roasting is performed to prepare a TiO.sub.2—SiO.sub.2 binary oxide; then, preparing Ni/TiO2-SiO2 by dipping in a nickel nitrate solution, and preparing a supported catalyst by drying and roasting; and finally, adopting a terpinolene-4, 8-epoxide a raw material, carrying out isomerization under the dual catalytic action of TiO2-SiO2 and Ni of the supported catalyst, and carrying out hydrogenation to prepare terpinene-4-ol. The preparation method can combine isomerization and hydrogenation reaction on the same catalyst, has good selectivity on terpinene-4-ol, and is simple to operate and high in product yield.
Nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol, preparation method thereof, and method of synthesizing terpinene-4-ol using the same
The present invention discloses a nickel/titanium oxide-silicon oxide catalyst for synthesizing terpinene-4-ol as well as a preparation method and method of synthesizing terpinene-4-ol using the same. The preparation method includes the steps of catalyst preparation, terpinene-4-ol synthesis and the like are disclosed in the present invention. The preparation method includes the following steps: firstly, preparing a mixed colloid of TiO.sub.2 and SiO.sub.2 by using a sol-gel method, and then centrifuging, washing, drying and roasting is performed to prepare a TiO.sub.2—SiO.sub.2 binary oxide; then, preparing Ni/TiO2-SiO2 by dipping in a nickel nitrate solution, and preparing a supported catalyst by drying and roasting; and finally, adopting a terpinolene-4, 8-epoxide a raw material, carrying out isomerization under the dual catalytic action of TiO2-SiO2 and Ni of the supported catalyst, and carrying out hydrogenation to prepare terpinene-4-ol. The preparation method can combine isomerization and hydrogenation reaction on the same catalyst, has good selectivity on terpinene-4-ol, and is simple to operate and high in product yield.
Distillation vacuum technology
This disclosure describes energy efficient process to distill a process stream in a production facility. A process uses multiple effect evaporators, ranging from one evaporator to eight evaporators in each effect. The process arrangement shows an example of four effect evaporators, with a zero-effect evaporator having a single evaporator, a first-effect evaporator having a set of three evaporators, a second-effect evaporator having a set of three evaporators, and a third-effect evaporator having a set of evaporators to create condensed distillers solubles.
Distillation vacuum technology
This disclosure describes energy efficient process to distill a process stream in a production facility. A process uses multiple effect evaporators, ranging from one evaporator to eight evaporators in each effect. The process arrangement shows an example of four effect evaporators, with a zero-effect evaporator having a single evaporator, a first-effect evaporator having a set of three evaporators, a second-effect evaporator having a set of three evaporators, and a third-effect evaporator having a set of evaporators to create condensed distillers solubles.
Method of producing ethylene oxide and ethylene glycol
There is provided a method of producing ethylene oxide and ethylene glycol capable of reducing a concentration in discharged water of 1,4-dioxane contained generated in a step of producing ethylene oxide and ethylene glycol. A method of producing ethylene oxide and ethylene glycol includes a predetermined step of producing ethylene oxide, and a step of extracting a part of a column bottom liquid of an ethylene oxide stripping column in the step of producing ethylene oxide and supplying the extracted column bottom liquid to a by-produced ethylene glycol concentration column, concentrating ethylene glycol produced as a by-product in the step of producing ethylene oxide, and distilling and separating 1,4-dioxane produced as a by-product in the step of producing ethylene oxide, wherein the by-produced ethylene glycol concentration column is a divided wall distillation column.
Method of producing ethylene oxide and ethylene glycol
There is provided a method of producing ethylene oxide and ethylene glycol capable of reducing a concentration in discharged water of 1,4-dioxane contained generated in a step of producing ethylene oxide and ethylene glycol. A method of producing ethylene oxide and ethylene glycol includes a predetermined step of producing ethylene oxide, and a step of extracting a part of a column bottom liquid of an ethylene oxide stripping column in the step of producing ethylene oxide and supplying the extracted column bottom liquid to a by-produced ethylene glycol concentration column, concentrating ethylene glycol produced as a by-product in the step of producing ethylene oxide, and distilling and separating 1,4-dioxane produced as a by-product in the step of producing ethylene oxide, wherein the by-produced ethylene glycol concentration column is a divided wall distillation column.
Method of revamping of a plant for distillation of methanol
Method for revamping a refining section of a methanol distillation plant comprising a medium pressure (MP) column a low pressure (LP) column, wherein both said columns comprise at least one bottom boiler, a gaseous stream of distilled methanol withdrawn from the MP column is fed to at least one bottom boiler of the LP column and a liquid solution containing methanol withdrawn from the MP column is fed to the LP column, the method of revamping comprising the installation of a high pressure (HP) column; the installation of a line feeding a gaseous stream of distilled methanol from the HP column to at least one bottom boiler of the MP column and the installation of a bottom line for exporting from the HP column a liquid stream consisting essentially of water.
Method of revamping of a plant for distillation of methanol
Method for revamping a refining section of a methanol distillation plant comprising a medium pressure (MP) column a low pressure (LP) column, wherein both said columns comprise at least one bottom boiler, a gaseous stream of distilled methanol withdrawn from the MP column is fed to at least one bottom boiler of the LP column and a liquid solution containing methanol withdrawn from the MP column is fed to the LP column, the method of revamping comprising the installation of a high pressure (HP) column; the installation of a line feeding a gaseous stream of distilled methanol from the HP column to at least one bottom boiler of the MP column and the installation of a bottom line for exporting from the HP column a liquid stream consisting essentially of water.