C03B37/01807

Method for manufacturing silicon dioxide preforms employed in the production of optical fibers

The present invention relates to a method for manufacturing a preform of silica for optical fiber production, as well as to a method for the production of optical fibers comprising a step of drawing the optical fiber from such a preform of silica, the method comprising a step of vaporization of a siloxane feedstock added with a compound having the following formula (I): wherein R, R′ and R″, equal or different each other, are an alkyl group having from 1 to 5 carbon atoms, and A is a saturated or unsaturated chain of atoms selected from the group consisting of carbon atom, nitrogen atom, and oxygen atom, said chain A forming with the nitrogen atom linked thereto a saturated, unsaturated or aromatic heterocyclic moiety. ##STR00001##

GLASS BODY MANUFACTURING APPARATUS, GLASS BODY MANUFACTURING METHOD, SOOT CONVEYING MECHANISM, AND SOOT HEATING MECHANISM

A glass body manufacturing apparatus includes: a first heating furnace including a furnace core tube accommodating the soot and a first heater, to supply a dehydration gas into the furnace core tube and heat the soot at a first treatment temperature lower than a softening point of the porous portion by the first heater; a second heating furnace including a structural body accommodating the soot and a second heater, to heat the soot at a second treatment temperature equal to or higher than the softening point by the second heater; and a conveyance container, connectable to each of the first and second heating furnaces while keeping airtightness with respect to the atmosphere, to accommodate and hold the soot, and convey the soot between the first and second heating furnaces.

Method for the defined separation of a glass layer on an inner wall of a preform and preform and communication system
10604440 · 2020-03-31 · ·

A method for a defined deposition of a glass layer on an inner wall of a preform for an optical fiber and/or for setting a refractive index profile of the preform for a multi-mode fiber. The method includes providing the preform having a cavity and an inner wall which defines an inner diameter of the preform, and spreading a deposition gas at a flow speed (v) in the cavity of the preform so as to provide the defined deposition of the glass layer. The defined deposition is performed at a reduced change in the flow speed a*v, where a<1. Based on the defined deposition, a change in the flow speed (v): v = 4 Q .Math. ( 1 d i 2 - 1 d i + 1 2 )
forms at a volume flow (Q), a first diameter (d.sub.i), and a second diameter (d.sub.i+1).

Rotary feed-through for mounting a rotating substrate tube in a lathe, a CVD lathe and a corresponding method using the CVD lathe

A rotary feed-through for mounting a rotating substrate tube in a lathe and providing a flow of process gas into the tube, said feed-through including a process gas supply line for providing a process gas into said substrate tube, a rotatable holder arranged for receiving and holding said substrate tube for rotating said substrate tube with respect to said process gas supply line, a rotary union provided between said rotatable holder and said process gas supply line for rotatably connecting said rotatable holder to said process gas supply line, a stationary housing connected to said process gas supply line and to said rotatable holder, therewith forming a closed cavity surrounding said rotary union, wherein said stationary housing further includes an auxiliary gas supply line for providing said closed cavity with an auxiliary gas.

Optical fiber

Provided is an optical fiber containing an alkali metal element or the like having a smaller diffusion coefficient than K and having a low Rayleigh scattering loss. An optical fiber is composed of silica glass and includes a core and a cladding arranged to surround the core which has a lower refractive index than the core. The core includes a first core including a central axis and a second core arranged to surround the first core. The average concentration of an alkali metal element or alkaline-earth metal element in the first core is 10 mol ppm or less. The average concentration of chlorine in the first core is 2000 mol ppm or more. The average concentration of an alkali metal element or alkaline-earth metal element in the second core is 10 mol ppm or more. The average concentration of chlorine in the second core is 10 to 600 mol ppm.

METHOD FOR MANUFACTURING SILICON DIOXIDE PREFORMS EMPLOYED IN THE PRODUCTION OF OPTICAL FIBERS

The present invention relates to a method for manufacturing a preform of silica for optical fiber production, as well as to a method for the production of optical fibers comprising a step of drawing the optical fiber from such a preform of silica, the method comprising a step of vaporization of a siloxane feedstock added with a compound having the following formula (I): wherein R, R and R, equal or different each other, are an alkyl group having from 1 to 5 carbon atoms, and A is a saturated or unsaturated chain of atoms selected from the group consisting of carbon atom, nitrogen atom, and oxygen atom, said chain A forming with the nitrogen atom linked thereto a saturated, unsaturated or aromatic heterocyclic moiety.

##STR00001##

OPTICAL FIBER BASE MATERIAL MANUFACTURING METHOD, OPTICAL FIBER BASE MATERIAL, AND OPTICAL FIBER

The present embodiment relates to an optical fiber preform manufacturing method in which two or more kinds of alkali metal elements are diffused and doped to an inner surface of a glass pipe. The manufacturing method includes: a first drying step performed at a temperature equal to or lower than a lowest temperature among melting point temperatures of the alkali metal salt raw materials; and a second drying step performed at a temperature which is equal to or higher than a highest temperature among the melting point temperatures of the alkali metal salt raw materials and at which vapor pressures of the alkali metal salt raw materials are 2 mmHg or lower.

METHOD OF MANUFACTURING OPTICAL FIBER PREFORM AND OPTICAL FIBER PREFORM

The present invention relates to a method of manufacturing an optical fiber preform for obtaining an optical fiber with low transmission loss. A core preform included in the optical fiber preform comprises three or more core portions, which are each produced by a rod-in-collapse method, and in which both their alkali metal element concentration and chlorine concentration are independently controlled. In two or more manufacturing steps of the manufacturing steps for each of the three or more core portions, an alkali metal element is added. As a result, the mean alkali metal element concentration in the whole core preform is controlled to 7 atomic ppm or more and 70 atomic ppm or less.

OPTICAL FIBER PREFORM PRODUCTION METHOD AND OPTICAL FIBER PRODUCTION METHOD

The present embodiment relates to a production method for matching a shape of a refractive index profile of a core preform with an ideal curve with high precision and in a short time. Prior to a glass synthesis step of stacking a plurality of glass layers including a refractive index adjusting agent of a predetermined amount on an inner peripheral surface or on an outer peripheral surface of a glass deposition substrate, glass synthesis actual-result data is created from production condition data of a glass preform produced in the past and refractive index profile data of a core preform obtained from the glass preform. In each glass synthesis section where the glass synthesis step is executed, a doping amount of the refractive index adjusting agent is adjusted on the basis of the glass synthesis actual-result data.

OPTICAL FIBER PREFORMS WITH HALOGEN DOPING

Preparation of halogen-doped silica is described. The preparation includes doping silica with high halogen concentration, sintering halogen-doped silica to a closed-pore state, and subjecting the closed-pore silica body to a thermal treatment process and/or a pressure treatment process. The temperature of thermal treatment is sufficiently high to facilitate reaction of unreacted doping precursor trapped in voids or interstices of the glass structure, but is below temperatures conducive to foaming. Core canes or fibers drawn from halogen-doped silica subjected to the thermal treatment and/or pressure treatment show improved optical quality and possess fewer defects. The thermal treatment and/or pressure treatment is particularly advantageous when used for silica doped with high concentrations of halogen.