C04B35/5618

Physical Forms of MXene Materials Exhibiting Novel Electrical And Optical Characteristics

The present invention(s) is directed to novel conductive M.sub.n+1X.sub.n(T.sub.s) compositions exhibiting high volumetric capacitances, and methods of making the same. The present invention(s) is also directed to novel conductive M.sub.n+1X.sub.n(T.sub.s) compositions, methods of preparing transparent conductors using these materials, and products derived from these methods.

Physical forms of MXene materials exhibiting novel electrical and optical characteristics

The present invention(s) is directed to novel conductive M.sub.n+1X.sub.n(T.sub.s) compositions exhibiting high volumetric capacitances, and methods of making the same. The present invention(s) is also directed to novel conductive M.sub.n+1X.sub.n(T.sub.s) compositions, methods of preparing transparent conductors using these materials, and products derived from these methods.

METHOD FOR PREPARING NANOMETER MAX PHASE CERAMIC POWDER OR SLURRY HAVING LAMINATED STRUCTURE BY MEANS OF BALL MILLING AND REGULATING OXYGEN CONTENT OF POWDER
20210322996 · 2021-10-21 ·

A method for preparing nanometer MAX phase ceramic powder or slurry having a laminated structure by means of ball milling and regulating the oxygen content of the powder. Micron-sized MAX phase ceramic coarse powder is adopted as a raw material, during ball milling, a gas or a liquid-state gas having a special effect is introduced into a ball milling tank, and by means of multi-dimensional functions and regulation such as ball milling parameters and gas reaction, the nanometer laminated MAX phase ceramic powder or the slurry containing the component is obtained. The surface components and the activated state of the powder are regulated while the particle size adjustment control of the powder is realized.

Short-Fiber-Reinforced Oriented MAX-Phase Ceramic-Based Composite and Preparation Method Therefor
20210323875 · 2021-10-21 ·

The present invention relates to the field of MAX-phase ceramic-based composites, specifically to a short-fiber-reinforced oriented MAX-phase ceramic-based composite and a preparation method therefor. By using a new process with a fiber, a nano lamellar MAX-phase ceramic powder, other additives, etc., for preparing a fiber-reinforced MAX-phase ceramic-based composite, a novel ternary composite is prepared, wherein a matrix is composed of a highly oriented lamellar MAX-phase ceramic, the fiber is distributed parallel to the lamellar MAX-phase ceramic in an axial direction, and a granulate ceramic phase enhancement phase is dispersed in the matrix. Thus, the problems of a MAX-phase ceramic-based composite matrix material prepared by an existing method, such as coarse grains, multiple internal defects and a low strength, and a poor fracture toughness; and a reaction sintering temperature being too high such that fibers are chemically and physically damaged in a substrate, resulting in performance degradation, are solved. Fibers prepared by the method are suitable for large-scale industrial preparation and have properties that are far superior to those of any existing known fiber MAX-phase composite.

HIGHLY ORIENTED NANOMETER MAX PHASE CERAMIC AND PREPARATION METHOD FOR MAX PHASE IN-SITU AUTOGENOUS OXIDE NANOCOMPOSITE CERAMIC
20210317045 · 2021-10-14 ·

A highly oriented nanometer MAX phase ceramic and a preparation method for a MAX phase in-situ autogenous oxide nanocomposite ceramic. The raw materials comprise a MAX phase ceramic nano-lamellar powder body or a blank body formed by the nano-lamellar powder body, wherein MAX phase ceramic nano-lamellar particles in the powder body or the blank meet the particle size being between 20-400 nm, and the oxygen content is between 0.0001%-20% by mass; MAX phase grains in the ceramic obtained after the raw materials are sintered are lamellar or spindle-shaped, the lamellar structure having a high degree of orientation. Utilizing special properties of the nano-lamellar MAX powder body, orientation occurs during compression and deformation to obtain a lamellar structure similar to that in a natural pearl shell, and such a structure has a high bearing capacity and resistance to external loads and crack propagation, just like a brick used in a building.

Hydrocarbon conversion

The invention relates to hydrocarbon conversion, to equipment and materials useful for hydrocarbon conversion, and to processes for carrying out hydrocarbon conversion, e.g., hydrocarbon pyrolysis processes. The hydrocarbon conversion is carried out in a reactor which includes at least one channeled member that comprises refractory and has an open frontal area≤55%. The refractory can include non-oxide ceramic.

OSMOTIC ENERGY CONVERSION WITH MXENE LAMELLAR MEMBRANE-BASED SYSTEM AND METHOD
20210175789 · 2021-06-10 ·

An osmotic energy conversion system includes a housing having a first inlet and a second inlet, an MXene lamellar membrane located inside the housing and configured to divide the housing into a first chamber and a second chamber, and first and second electrodes placed in the first and second chambers, respectively, and configured to collect electrical energy generated by a salinity-gradient formed by first and second liquids across the MXene lamellar membrane. The first chamber is configured to receive the first liquid at the first inlet and the second chamber is configured to receive the second liquid at the second inlet. The first liquid has a salinity lower than the second liquid, and the MXene lamellar membrane includes plural nanosheets of MXene stacked on top of each other.

Method for Producing Non-Oxide Ceramic Powders
20210147301 · 2021-05-20 ·

The invention relates to a method for producing a non-oxide ceramic powder comprising a nitride, a carbide, a boride or at least one MAX phase with the general composition Mn+1AXn, where M=at least one element from the group of transition elements (Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta), A=at least one A group element from the group (Si, Al, Ga, Ge, As, Cd, In, Sn, Tl and Pb), X=carbon (C) and/or nitrogen (N) and/or boron (B), and n=1, 2 or 3. According to the invention, corresponding quantities of elementary starting materials or other precursors are mixed with at least one metal halide salt (NZ), compressed (pellet), and heated for synthesis with a metal halide salt (NZ). The compressed pellet is first enveloped with another metal halide salt, compressed again, arranged in a salt bath and heated therewith until the melting temperature of the salt is exceeded. Optionally, melted silicate can be added, which prevents the salt from evaporating at high temperatures. Advantageously, the method can be carried out in the presence of air.

Osmotic energy conversion with MXene lamellar membrane-based system and method

An osmotic energy conversion system includes a housing having a first inlet and a second inlet, an MXene lamellar membrane located inside the housing and configured to divide the housing into a first chamber and a second chamber, and first and second electrodes placed in the first and second chambers, respectively, and configured to collect electrical energy generated by a salinity-gradient formed by first and second liquids across the MXene lamellar membrane. The first chamber is configured to receive the first liquid at the first inlet and the second chamber is configured to receive the second liquid at the second inlet. The first liquid has a salinity lower than the second liquid, and the MXene lamellar membrane includes plural nanosheets of MXene stacked on top of each other.

CERAMIC OXIDE COMPOSITES REINFORCED WITH 2D MX-ENES

The present disclosure is directed to nanocomposites comprising a co-sintered composition of a MXene crystal form composition and an inorganic oxide, or oxide-type ceramic and methods of making and using the same.