C04B35/62635

TUNGSTATE- AND MOLYBDATE-BASED CERAMIC COATING FOR PROTECTION OF METAL SURFACES, PREPARATION PROCEDURE AND USE THEREOF

The present invention relates to different inorganic ceramic coatings whose chemical compositions comprise silicates, acids, metallic oxysalts such as tungstates and molybdates, water, and non-metallic oxides such as silicon oxide. Said water-based inorganic ceramic coatings improve the ceramic, anti-corrosive and resistance properties of the metal substrates that are coated with same. Likewise, the present invention relates to a sol-gel process for synthesizing said coatings in which the non-metallic oxide, before being mixed with the rest of the components of the chemical compositions as claimed, can be pre-treated with hydrochloric acid and ammonium hydroxide, or can be sonicated to achieve a particle size in the range from approximately 160 to approximately 180 nm. Finally, the present invention also relates to a method for coating the metal parts with the inorganic ceramic coatings as claimed in the present invention.

Antimicrobial Ceramic Tile and Manufacturing Method Thereof
20230091820 · 2023-03-23 ·

The present invention provides an antimicrobial ceramic tile and manufacturing method thereof. A manufacturing method of an antimicrobial ceramic tile comprises: grinding soils into slurries; drying the slurries into powders by hot air; pressing the powders into a green body through a molding machine; dotting or spraying or showering a glaze slurry on the surface of the green body to form an engobe; dotting the glaze slurry on the engobe to form a ground glaze; mixing a surface glaze and an antimicrobial material into an antimicrobial glaze in a weight ratio of 100:5˜10; grinding water and the antimicrobial glaze into the antimicrobial glaze in a weight ratio of 5˜6:4˜5; and dotting antimicrobial glaze on the ground glaze; finally, rapidly firing the ceramic tile and the antimicrobial glaze into an antimicrobial ceramic tile.

PREPREG FOR CERAMIC MATRIX COMPOSITE

A prepreg including a support with, for more than 90% of the weight thereof, of ceramic fibers, and a thermoreversible liquefiable gel covering, at least in part, at least one portion of the ceramic fibers. The liquefiable gel including: 20% to 60% of ceramic particles and 0% to 10% of metal particles, both as percentage by volume based on the volume of the liquefiable gel; 0.2% to 10% of a thermoreversible hydrocolloid and 0% to 7% of one or more other constituents, both as a percentage by weight on the basis of the total weight of the ceramic particles and metal particles; the balance to 100% being water. It being possible for the ceramic particles and the metal particles to be replaced, partially or completely, by precursors of ceramic particles and of metal particles, respectively, capable of forming, by heat treatment above 200° C., ceramic particles and metal particles, respectively.

Method of producing alumina ceramics reinforced with oil fly ash

A method for making ceramic composites via sintering a mixture of alumina and oil fly ash. The alumina is in the form of nanoparticles and/or microparticles. The oil fly ash may be treated with an acid prior to the sintering. The composite may comprise graphite carbon derived from oil fly ash dispersed in an alumina matrix. The density, mechanical performance (e.g. Vickers hardness, fracture toughness), and thermal properties (e.g. thermal expansion, thermal conductivity) of the ceramic composites prepared by the method are also specified.

LOW TEMPERATURE CARBON/BN/ALUMINUM OXIDE COATING
20230118131 · 2023-04-20 ·

A method of forming an activated coating composition is disclosed. The method includes providing (a) boron nitride, (b) carbon, (c) aluminum oxide and (d) a liquid carrier. Each of the boron nitride, carbon and aluminum oxide are in particulate form. The coating composition is activated to form an activated coating composition. The activated coating composition includes active components having from about 60.0 wt% to about 90.0 wt% boron nitride, from about 16 wt% to about 24 wt% carbon and from about 4 wt% to about 6 wt% aluminum oxide. A coating method, coated substrate and activated coating composition are also disclosed.

TWO-STAGE SINTERING METHOD FOR PREPARING POROUS BIPHASIC CALCIUM PHOSPHATE CERAMIC FROM CALCIUM-CONTAINING BIOLOGICAL WASTE

The present invention relates to a two-stage sintering method for preparing a porous biphasic calcium phosphate ceramic from calcium-containing biological waste, wherein hydroxyapatite prepared from calcium-containing waste is mixed with a foaming agent to prepare a bone graft material having medicinal use through two-stage sintering.

Li3Mg2SbO6-based microwave dielectric ceramic material easy to sinter and with high q value, and preparation method therefor

A Li.sub.3Mg.sub.2SbO.sub.6-based microwave dielectric ceramic material easy to sinter and with high Q value, and a preparation method thereof are disclosed. A chemical formula of the material is Li.sub.3(Mg.sub.1-xZn.sub.x).sub.2SbO.sub.6, wherein 0.02≤x≤0.08. The preparation method includes: 1) mixing and ball-milling Sb.sub.2O.sub.3 and Li.sub.2CO.sub.3 according to a chemical ratio and then drying, and conducting pre-sintering to obtain a Li.sub.3SbO.sub.4 phase; and 2) mixing and ball-milling MgO, ZnO and Li.sub.3SbO.sub.4 powder according a chemical ratio of Li.sub.3(Mg.sub.1-xZn.sub.x).sub.2SbO.sub.6 and then drying, conducting granulation and sieving after adding an adhesive, pressing into a cylindrical body, and sintering the cylindrical body into ceramic in the air at 1325° C. and under normal pressure, wherein a dielectric constant is 7.2-8.5, a quality factor is 51844-97719 GHz, and a temperature coefficient of resonance frequency is −14-1 ppm/° C.

METHOD FOR THE PREPARATION OF A LEAD-FREE PIEZOELECTRIC MATERIAL AND PRECURSOR SOLUTION

The present disclosure relates to a method for the preparation of a precursor solution for a ceramic of the BZT-aBXT type wherein X is selected from Ca, Sn, Mn and Nb and a is a molar fraction selected in the range between 0.10 and 0.90 comprising the steps of: a) dissolving at least one barium precursor compound and at least one precursor compound selected from the group consisting of a calcium precursor compound, a tin precursor compound, a manganese precursor compound and a niobium precursor compound in a linear or branched anhydrous alkyl alcohol containing from 2 to 6 carbon atoms and, after dissolution, dehydrating by stripping, to obtain a first solution; b) dissolving at least one zirconium precursor compound and at least one titanium precursor compound in a linear or branched anhydrous alkyl alcohol containing from 2 to 6 carbon atoms in the presence of an anhydrous chelating agent to obtain a second solution; c) joining said first and second solutions in an anhydrous environment and dehydrating by stripping to obtain said precursor solution. It also relates to a precursor solution, to a method for the preparation of a film of a piezoelectric material, to a piezoelectric material and to an electronic device comprising this piezoelectric material.

BISMUTH TUNGSTATE/BISMUTH SULFIDE/MOLYBDENUM DISULFIDE HETEROJUNCTION TERNARY COMPOSITE MATERIAL AND PREPARATION METHOD AND APPLICATION THEREOF

The present invention relates to a bismuth tungstate/bismuth sulfide/molybdenum disulfide heterojunction ternary composite material and a preparation method and application thereof. The composite material is composed of bismuth tungstate, bismuth sulfide and molybdenum disulfide in an ordered layered way, Bi.sub.2WO.sub.6 is an orthorhombic system, Bi.sub.2S.sub.3 is a p-type semiconductor located on a (130) crystal face, MoS.sub.2 is a layered transition metal sulfide located on a (002) crystal face, the whole composite material is of a spherical structure with an unsmooth surface, and a layer of nanosheets uniformly grow on an outer layer. The average particle size of composite materials is in the range of 2.4-2.6 μm. The spherical Bi.sub.2WO.sub.6/Bi.sub.2S.sub.3/MoS.sub.2 heterojunction ternary composite material prepared in the present invention has good adsorption of Cr(VI) and high catalytic reduction ability under visible light.

Facile synthesis of solid sodium ion-conductive electrolytes

Disclosed is a rapid, reproducible solution-based method to synthesize solid sodium ion-conductive materials. The method includes: (a) forming an aqueous mixture of (i) at least one sodium salt, and (ii) at least one metal oxide; (b) adding at least one phosphorous precursor as a neutralizing agent into the mixture; (c) concentrating the mixture to form a paste; (d) calcining or removing liquid from the paste to form a solid; and (e) sintering the solid at a high temperature to form a dense, non-porous, sodium ion-conductive material. Solid sodium ion-conductive materials have electrochemical applications, including use as solid electrolytes for batteries.