Disclosed are methods for forming boron nitride-containing aggregates that exhibit improved wear by attrition, and resulting filled polymers that exhibit significantly improved thermal conductivity. The boron nitride-containing aggregates are prepared according to a method that includes wet granulating boron nitride powder with a granulation solution to form wet boron nitride-containing granules; and drying the wet boron nitride-containing granules to cause evaporation of solvent in the granulation solution, thereby forming boron nitride-containing granules. Sintering achieves the desired boron nitride-containing aggregates.

The present invention relates to a mesoporous silica/ceria-silica composite and a method for preparing a mesoporous composite and, more specifically, to a mesoporous silica/ceria-silica composite which is composed of mesoporous silica having a hexagonal or cubic structure and ceria having a hexagonal structure provided on a surface and pores of the mesoporous silica, the oxidation state of the ceria being Ce.sup.4+ and Ce.sup.3+.

A method of preparing a lithium lanthanum zirconate (LLZO) cubic garnet material is provided which comprises the following steps: (a) milling a slurry comprising one or more precursor compounds in an aqueous medium, wherein the one or more precursor compounds comprise lithium, lanthanum, zirconium and optionally one or more dopant elements, to provide a milled slurry; (b) spray drying the milled slurry to provide a spray-dried powder; and (c) annealing the spray-dried powder. The resultant LLZO cubic garnet material may be used as a lithium ion conductive solid electrolyte in secondary lithium-ion batteries.

The present invention relates to a metal matrix composite (MMC). The MMC includes a preform formed from a composition having ceramic particles and ceramic fibers and defining a plurality of voids. The metal matrix composite also includes a support element, such as a metal, disposed within the voids of the preform. The MMC has a wear surface defined by both the preform and the support element.

Disclosed are methods for forming boron nitride-containing aggregates that exhibit improved wear by attrition, and resulting filled polymers that exhibit significantly improved thermal conductivity. The boron nitride-containing aggregates are prepared according to a method that includes wet granulating boron nitride powder with a granulation solution to form wet boron nitride-containing granules; and drying the wet boron nitride-containing granules to cause evaporation of solvent in the granulation solution, thereby forming boron nitride-containing granules. Sintering achieves the desired boron nitride-containing aggregates.

A process for fabricating pre-sintered zirconia blanks that are then computer machined and sintered to form dental appliances having highly advantageous features. The principal steps of a preferred embodiment of that process comprise; a) preparing a ceramic slurry of zirconia powder; b) subjecting the slurry to attrition milling down to about a 5-29 nm crystallite size; c) preparing a vacuum assisted and pressure assisted slip casting mold and pouring the milled slurry into the slip-casting mold; d) after casting, excess slurry is poured from the mold and a consolidated zirconia blank is removed; e) drying the blank and pre-sintering it to form solid blanks ready for CAD/CAM machining and sintering to net shape. The attrition is run with ball bearings that are of the sample material to prevent contamination. It also is run, up to 24 hours, to break down the crystallites to overcome the high density of zirconia.

A sintering-free inorganic ceramic brick-plate and its preparation method are disclosed. The sintering-free inorganic ceramic brick-plate includes following components by mass parts: 25-40 parts of magnesium oxide; 20-35 parts of magnesium chloride; 20-30 parts of fumed silica; 10-20 parts straw powders; 0.1-0.3 parts of graphene powders with a particle size of 2000 meshes; and 0.2-0.4 parts of airgel powders with a particle size of 100 nm. Compared with the prior art, the present invention utilizes a variety of raw natural non-toxic natural mineral raw materials, namely, the graphene powders with the particle size of 2000 meshes and the airgel powders with the particle size of 100 nm for mixing, and then the mixed raw materials can be solidified at room temperature and form sheets, and then the surface of the sheets is processed through printing or spraying glaze, so as to achieve the effect of high-grade tiles and natural marble.

The present disclosure relates to an orthophosphate thermal barrier coating material with high coefficient of thermal expansion and a preparation method thereof. ReM.sub.3P.sub.3O.sub.12 series ceramics with an eulytite crystal structure are prepared by a high-temperature solid-phase reaction for the first time. The ReM.sub.3P.sub.3O.sub.12 ceramic belongs to a −43 m space group of a cubic crystal system, which not only has a higher melting point and excellent high-temperature phase stability, but also has a lower thermal conductivity and a suitable coefficient of thermal expansion. It can effectively alleviate the stress caused by the mismatch of the coefficient of thermal expansion of the base material and the ceramic layer, so as to meet the requirements of thermal insulation and high-temperature oxidation and corrosion resistance of the hot end parts in long-term service, which has application prospects in the field of thermal barrier coatings.

A Li.sub.3Mg.sub.2SbO.sub.6-based microwave dielectric ceramic material easy to sinter and with high Q value, and a preparation method thereof are disclosed. A chemical formula of the material is Li.sub.3(Mg.sub.1-xZn.sub.x).sub.2SbO.sub.6, wherein 0.02≤x≤0.08. The preparation method includes: 1) mixing and ball-milling Sb.sub.2O.sub.3 and Li.sub.2CO.sub.3 according to a chemical ratio and then drying, and conducting pre-sintering to obtain a Li.sub.3SbO.sub.4 phase; and 2) mixing and ball-milling MgO, ZnO and Li.sub.3SbO.sub.4 powder according a chemical ratio of Li.sub.3(Mg.sub.1-xZn.sub.x).sub.2SbO.sub.6 and then drying, conducting granulation and sieving after adding an adhesive, pressing into a cylindrical body, and sintering the cylindrical body into ceramic in the air at 1325° C. and under normal pressure, wherein a dielectric constant is 7.2-8.5, a quality factor is 51844-97719 GHz, and a temperature coefficient of resonance frequency is −14-1 ppm/° C.

A foam formulation for preparing polymer-grafted nanoparticles stabilized foam, including nanoparticles, monomers of a polymer to be grafted on the nanoparticle surface, polymerization initiator, surfactant and water. The polymer-grafted nanoparticles may act together with the surfactant to form single-layer assembling at the boundary of bubbles, which in turn stabilizes the foam. The generated foam shows much better stability in long-term storage, high-temperature drying process and alkaline environments than conventional wet foams. A method of preparing solid porous materials with the foam is also provided.