Process and apparatus for the separation of a compressed feed air stream to produce an oxygen product using a distillation column having a lower-pressure column and a higher-pressure column, a higher-pressure heat exchanger and a lower-pressure heat exchanger where the gaseous nitrogen expander receives a nitrogen-enriched fraction from a position intermediate the warmer end and the colder end of the higher-pressure heat exchanger.

A hydrocarbon distribution system is provided. The hydrocarbon distribution system has a vessel shell. A vapor distribution tray is disposed within the vessel shell. A first spray header and a second spray header are disposed above the vapor distribution tray. A draw system is disposed above the first and second spray headers. The hydrocarbon distribution system reduces clogging of nozzles, and improves product quality.

A system for melting contaminant-laden solids that have been separated from a hydrocarbon-containing vapor stream in a hydrocarbon distillation tower, comprising at least one plate positioned where the solids form within the hydrocarbon distillation tower, hollow tubing forming an integral part of each of the at least one plate, and a heating medium disposed to flow through the hollow tubing at a higher temperature than a temperature of the solids to at least partially melt the solids.

In a process for the cryogenic separation of a feed mixture of at least carbon monoxide, hydrogen and methane, the feed mixture is separated in a methane wash column fed by a liquid methane stream at the top of the methane wash column to produce a gas enriched in hydrogen, a liquid stream from the bottom of the methane wash column is treated to produce a mixture of carbon monoxide and methane, the mixture of carbon monoxide and methane is separated in a separation column to produce a gas enriched in carbon monoxide and a liquid methane flow at least part of which forms a purge stream, the purge stream being varied to take account of load variations.

A system for melting contaminant-laden solids that have been separated from a hydrocarbon-containing vapor stream in a hydrocarbon distillation tower, comprising at least one plate positioned where the solids form within the hydrocarbon distillation tower, hollow tubing forming an integral part of each of the at least one plate, and a heating medium disposed to flow through the hollow tubing at a higher temperature than a temperature of the solids to at least partially melt the solids.

A system for removing acid gases from a raw gas stream is provided. The system includes a cryogenic distillation tower. The cryogenic distillation tower has a controlled freezing zone that receives a cold liquid spray comprised primarily of methane. The tower receives and then separates the raw gas stream into an overhead methane gas stream and a substantially solid material comprised on carbon dioxide. The system includes a collector tray below the controlled freezing zone. The collector tray receives the substantially solid material as it is precipitated in the controlled freezing zone. The system also has a filter. The filter receives the substantially solid material and then separates it into a solid material comprised primarily of carbon dioxide, and a liquid material comprising methane. The solid material may be warmed as a liquid and sold, while the liquid material is returned to the cryogenic distillation tower.

A batch process for producing a purified, pressurized liquid carbon dioxide stream, includes withdrawing a liquid carbon dioxide stream (A) from a liquid carbon dioxide supply (10); introducing the liquid carbon dioxide stream (A) into a distillation column (B) having packing (C) therein, and stripping volatile impurities from the liquid carbon dioxide stream with the packing; vaporizing the liquid carbon dioxide stream (A) in a sump (D) of the distillation column (B) for providing a carbon dioxide vapor; withdrawing from a vaporized portion (F) of carbon dioxide vapor in the sump (D) a first vapor stream (G) vented from the distillation column (B); withdrawing from the vaporized portion (F) of the carbon dioxide vapor in the sump (D) a second vapor portion (H) vented from the sump into a conduit (I); and introducing the second vapor portion (H) in the conduit (I) into a carbon dioxide vapor feed stream.

The present disclosure provides a distillation tower for separating a feed stream. The distillation tower includes a controlled freeze zone section having a controlled freeze zone upper section and a controlled freeze zone lower section below the controlled freeze zone upper section. The controlled freeze zone section includes: (a) a spray assembly in the controlled freeze zone upper section; (b) a melt tray assembly in the controlled freeze zone lower section; (c) a feed stream distribution mechanism between the spray assembly and the melt tray assembly. The feed stream distribution mechanism is constructed and arranged to uniformly distribute the feed stream in the controlled freeze zone section.

An apparatus is disclosed for maintaining constant fluid pressure and equalized fluid flow among a plurality of downcomer lines through which liquid from a tower is directed. A substantially annular fluid distribution belt is disposed at the circumference of the tower. The fluid distribution belt collects liquid from the tower. At least two outlets direct liquid from the fluid distribution belt out of the tower and into a corresponding number of downcomer lines disposed external to the tower.

A method and device are disclosed herein for distributing a gas into a vessel. The method comprises providing a gas distribution apparatus, wherein an exposed surface of the apparatus comprises a material that inhibits adsorption of the gas and deposition of the gas' solid form. The material chosen is chemically repulsive to the gas and the gas' solid form. In this manner, desublimation of the gas and deposition of the gas' solid form onto the exposed surface is prevented. The device disclosed herein is the gas distribution apparatus referenced above.