A method and system for controlling the nitrogen concentration in an LNG product and fuel from flash gas within preferred ranges. A cooled LNG stream is separated into a nitrogen-enriched vapor stream, a fuel stream, and an LNG product stream using a plurality of phase separating devices, such as flash drum or rectifying column. A portion of the vapor stream is recycled to the rectifying column as reflux. A portion of a stream having a higher concentration of nitrogen is combined with the fuel stream to maintain the fuel stream within a desired nitrogen concentration range.

Carbon dioxide is recovered from an exhaust gas in the form of liquid carbon dioxide or supercritical carbon dioxide utilizing a rotary separator. Nitrogen gas recovered from the rotary separator can be expanded to provide cooling for carbon dioxide in a closed-loop CO2 power cycle that is used to cool the exhaust gas upstream of the rotary separator. The recovery can power itself and can produce excess electricity from waste heat.

An apparatus for producing product nitrogen gas and product argon, comprising: a first rectification column into which raw air is introduced; a second rectification column from which product nitrogen gas is drawn; a third rectification column from which product argon gas is drawn; and a first condenser configured to perform heat exchange between a gas accumulated in a column top portion of the first rectification column, and a liquid accumulated in a column bottom portion of the second rectification column, wherein an intermediate portion gas containing nitrogen is drawn from an intermediate portion of the second rectification column and merged with a condenser gas drawn from the first condenser. The merged gases are expanded and cooled by means of an expansion turbine whereby the cold thereof is utilized.

A method for separating a mixture containing at least nitrogen and methane by cryogenic distillation in a first column operating in a first pressure and a second column operating at a second pressure lower than the first pressure, the mixture being separated in the first column to form a gas enriched in nitrogen and a liquid enriched in methane, at least a portion of the gas enriched in nitrogen being at least partially condensed in a heat exchanger and returned to the first column, the gas enriched in nitrogen is sent into the heat exchanger by the bottom, ascends in a first series of passages of the exchanger and condenses therein at least partially, the liquid formed descending in these passages of the first series and exiting by the bottom of the exchanger.

A method for processing a gas mixture containing nitrogen and methane, the gas mixture being at least partly liquefied using a mixed refrigerant circuit and is expanded in a storage tank, wherein: formed in the storage tank are a liquid phase, which is depleted in nitrogen and enriched with methane relative to the gas mixture, and a vapour phase, which is enriched with nitrogen and depleted in methane relative to the gas mixture; at least some of the vapour phase is compressed, at least partly liquefied, and subjected to low-temperature rectification; and formed in the low-temperature rectification are a top gas rich in nitrogen and lean in methane, and a bottom liquid lean in nitrogen and rich in methane. The invention provides that the partial liquefaction of the vapour phase is caused by cooling by means of heat exchange using the mixed refrigerant circuit.

A system and method for removing nitrogen from natural gas using two fractionating columns, that may be stacked, and a plurality of separators and heat exchangers, with horsepower requirements that are 50-80% of requirements for prior art systems. The fractionating columns operate at different pressures. A feed stream is separated with a vapor portion feeding the first column to produce a first column bottoms stream that is split into multiple portions at different pressures and first column overhead stream that is split or separated into two portions at least one of which is subcooled prior to feeding the top of the second column. Optional heat exchange between first column and second column streams provides first column reflux and reboil heat for a second column ascending vapor stream. Three sales gas streams are produced, each at a different pressure.

A system for the removal of nitrogen from a liquid natural gas (LNG) stream. The system. comprises a feed heat changer and a stripper column. The heat receives the LNG stream and cools the LNG stream via heat exchange with a stripper column side-draw stream to yield a cooled LNG stream and a heated side-draw stream. The stripper column receives the cooled LNG stream at a first tray and the heated side-draw stream. The stripper column produces the stripper column side-draw stream, a stripper column overhead stream, and a stripper column bottom stream. The stripper column side-draw stream is taken from the stripper column at a second tray. The second tray is at least about 15 feet higher than the feed heat exchanger.

A system for removing nitrogen from a natural gas fluid feed stream includes a main heat exchanger that receives the natural gas fluid feed stream. A distillation column receives a cooled fluid stream from the main heat exchanger and features a return vapor outlet and a side vapor outlet port. The return vapor outlet provides nitrogen vapor to the main heat exchanger which is warmed therein. The side vapor outlet port provides vapor to the main heat exchanger and a reflux compressor receives and compresses the resulting fluid from the main heat exchanger. A reflux aftercooler receives and cools fluid from the reflux compressor, directs cooled fluid to the main heat exchanger and the resulting fluid is directed to a reflux separation device. The reflux separation device has a vapor outlet and a liquid outlet. The vapor outlet of the reflux separation device directs fluid to the main heat exchanger so that fluid is directed to the first reflux inlet port of the distillation column. The liquid outlet of the reflux separation device directs fluid to a second reflux inlet port of the distillation column.

A gas recovery system for a compressor, said gas recovery system being equipped with: a distillation column that brings a supply gas in a liquid state into contact with a mixed gas, thereby cooling and liquefying a process gas in the mixed gas, and heating and gasifying the liquid supply gas; a process gas recovery line that is connected to the lower part of the distillation column and recovers the liquid process gas discharged from the distillation column; and a supply gas recovery line that is connected to the upper part of the distillation column and recovers the gaseous supply gas discharged from the distillation column.

A method and system for liquefying a natural gas feed stream and removing nitrogen therefrom.