F25J3/04054

METHOD FOR CRYOGENIC SEPARATION OF AIR, AND AIR SEPARATION PLANT
20190321772 · 2019-10-24 · ·

A method for cryogenic separation of air uses an air separation plant, wherein, in a mass transfer column, a liquid first fluid and a gaseous second fluid are subjected to mass transfer with one another. A gaseous third fluid is removed from the column and is at least partly discharged from the air separation plant. A liquid fourth fluid is removed from the column and is at least partly fed into a low-pressure column. The first fluid is formed using at least a part of an oxygen-rich liquid removed from the low-pressure column. The second fluid is formed using an oxygen-enriched liquid removed from a high-pressure column. The oxygen-enriched liquid removed from the high-pressure column and bottom liquid of the mass transfer column are mixed and partly evaporated in a condenser-evaporator. A liquid fifth fluid is removed from the mass transfer column between a feed point for the first fluid and a feed point for the oxygen-enriched liquid, and is at least partly fed into the low-pressure column. The fifth fluid or a fraction thereof is fed into the low-pressure column below the fourth fluid or a fraction thereof.

Method and apparatus for air separation by cryogenic distillation

A method for separating air by cryogenic distillation in a system of columns comprising a first column and a second column operating at a lower pressure than the first column, comprising the steps of compressing all of the feed air in a first compressor to a first output pressure of at least 1 bar greater than the pressure of the first column, sending a first portion of the air under the first output pressure to the second compressor, and compressing the air to a second output pressure, cooling and condensing at least a portion of the air under the second output pressure in a heat exchanger, withdrawal of a liquid from a column of the system of columns, pressurising the liquid and evaporating the liquid by heat exchange in the heat exchanger, and pressure reduction of a portion of the compressed air to a second output pressure, at least partially evaporating said air in the heat exchanger, optionally additional heating of said air in the heat exchanger, and sending at least a portion of this air to the second compressor.

METHOD AND PLANT FOR LOW TEMPERATURE FRACTIONATION OF AIR
20240183610 · 2024-06-06 ·

A SPECTRA process for low-temperature fractionation of air is proposed, in which bottoms liquid from an additional second rectification column used to obtain oxygen is evaporated in a second condenser evaporator arrangement. In this second condenser evaporator arrangement, gas that has been evaporated beforehand in a first condenser evaporator arrangement, which is used for condensation of tops gas from a first rectification column, is partially condensed after recompression. The invention also relates to a corresponding plant.

Method and device for the low-temperature separation of air at variable energy consumption
10215489 · 2019-02-26 · ·

A method and a device used to variably obtain a compressed-gas product by means of the low-temperature separation of air in a distillation column system. In a first operating mode, a first amount of first compressed-gas product is obtained, and, in a second operating mode, a second, smaller amount is obtained. In the first operating mode, a first amount of high-pressure column nitrogen is compressed in a nitrogen compressor and in the second operating mode, a second, larger amount is compressed in the nitrogen compressor.

APPARATUS AND METHOD FOR SEPARATION OF AIR BY CRYOGENIC DISTILLATION

An apparatus for separation of air by cryogenic distillation comprising: a system of columns; a first turbine; a warm compressor coupled to the first turbine; a second turbine; a cold compressor coupled to the second turbine; a heat exchanger; means for sending air cooled in the heat exchanger at an intermediate temperature of the heat exchanger to the cold compressor; means for sending expanded air from the second turbine to the system of columns; means for sending air compressed in the cold compressor to an intermediate point of the heat exchanger and then at least in part to the system of columns via a first valve; means for sending air compressed in the cold compressor to the inlet of the first turbine via a second valve without passing through the heat exchanger, wherein the means for sending air compressed in the cold compressor to the inlet of the first turbine via the second valve without passing through the heat exchanger is also connected to the inlet of the first turbine; means for sending a fraction of air cooled in the heat exchanger to an intermediate temperature of the latter to the first turbine; means for sending expanded air from the first turbine to the system of columns; and a bypass line provided with an expansion valve configured to send air from the cold compressor to the system of columns without passing through the heat exchanger.

METHOD FOR DE-ICING A DEVICE FOR SEPARATING AIR BY CRYOGENIC DISTILLATION AND DEVICE ADAPTED TO BE DE-ICED USING THIS METHOD

Method for separating air by cryogenic distillation in an air separation device comprising a system of columns, a first turbine and a second turbine, wherein, in de-icing operation, a common duct bringing air from the two turbines to a column is closed by means of an isolation valve, a purge gas is sent to the turbines at a temperature above 0 C. in order to de-ice them, but purge gas is not sent to the system of columns.

DEVICE AND METHOD FOR SEPARATING AIR BY CRYOGENIC DISTILLATION

Method for separating air by cryogenic distillation, wherein at least part of the air to be distilled is boosted in an air booster, compressed air is allowed to expand in at least one expansion turbine and, if the pressure drop between two points of the booster passes under a threshold and/or a flow of the booster passes under a minimum flow of the booster, part of the air boosted in the booster is allowed to expand without having been cooled between the booster and the expansion turbine and the boosted expanded air is sent upstream or downstream of the at least one turbine, without having been cooled in the heat exchanger, after having been boosted.

METHOD AND DEVICE FOR SEPARATING AIR BY CRYOGENIC DISTILLATION

Method for separating air by cryogenic distillation, wherein air is compressed in a compressor and is subsequently sent to a heat exchanger, with the air cooled in the exchanger being sent to a check valve downstream of the heat exchanger and subsequently to a turbine, the valve being positioned so that air from a short-circuiting duct cannot return to the exchanger from the compressor.

Process and apparatus for the low-temperature fractionation of air
10161676 · 2018-12-25 · ·

The process and the apparatus serve for the low-temperature fractionation of air in a distillation column system, which has at least one separating column. Feed air is compressed in a main air compressor. Compressed feed air is cooled in a main heat exchanger. Cooled feed air is introduced into the distillation column system. At least one product stream is drawn off from the distillation column system, heated in the main heat exchanger and drawn off as a gaseous end product. At least one process parameter is set by a basic controller. The control of the process parameter is set by a combination of an ALC control and an MPC controller. This involves the ALC control outputting a first target value to the MPC controller.

Method for starting up a cryogenic air separation unit and associated air separation unit

In a process for starting up an air separation unit, which is at a temperature of above 0? C., the air separation unit comprising a main air compressor for compressing the feed air, a booster driven by a turbine and a venting conduit connected downstream of the booster and upstream of the main heat exchanger wherein in order to start up the air separation unit, once the turbine is operating at said given speed, the venting conduit is opened to send at least part of the air compressed in the booster from the booster outlet to the atmosphere.