An air separation plant for obtaining product containing argon by low temperature separation of compressed, cooled feed air. The air separation plant comprises a high-pressure column, a multi-part low-pressure column having a base segment and a head segment and a multi-part crude argon column having a base segment and a head segment. An oxygen-enriched flow is obtained from part of the feed air in the high pressure column, an argon-enriched flow is obtained from part of the oxygen-enriched flow in the low-pressure column, and an argon-rich flow is obtained from part of the argon-enriched flow in the crude argon column. Liquid flow is transferred from a lower region of the head segment of the low-pressure column and from a lower region of the base segment of the crude argon column into an upper region of the base segment of the low-pressure column.

An enclosure for a column for low-temperature distillation comprises a distillation column, which has a circular cross section and is to be thermally insulated, the column containing liquid during use, at least one pipe attached to the column for transporting a liquid, a parallelepipedal casing enclosing the column in a sealed manner, pulverulent thermal insulation filling the space between the column or columns and the casing, a liquid-retaining tank, which has a flat bottom and four side walls, defining a liquid-retaining space, the tank being arranged inside the casing below the column in order to collect liquid that has leaked from the column, the tank being made from stainless steel or from aluminium and the casing being made from carbon steel, the column resting on the bottom of the tank through a skirt, the skirt being a cylinder made from stainless steel and having the same diameter as the column, the liquid-retaining space containing pulverulent thermal insulation.

The invention relates to a column for separating air by means of cryogenic distillation, said column comprising a shell and at least four distillation segments, including at least a first intermediate distillation segment of the low-pressure column, which is surrounded by an auxiliary shell around which a space is defined that is divided into a lower section and an upper section along the radius of the column, the intermediate segment(s) being located in an intermediate part of the low-pressure column, the capacity of the first intermediate segment being greater than that of at least one adjacent segment, and an opening being disposed in the shell between two adjacent segments, which opening can be sealed if the column is to form part of an argon production device.

Disclosed herein is a modular process plant structural system which includes numerous modules, all ISO-certified under ISO 1496 and capable of holding within the entire module at least one chemical (or non-chemical) production plant piece of equipment, capable of individually being shipped or transported. The modules can be stacked vertically, horizontally, or mixed (both vertical and horizontal arrangement). The modules are pre-fabricated offsite, built with the desired equipment within the module, pre-plumbed with piping, instrumentation, and electrical wiring, and then the multiple modules are shipped multimodally as ISO 1496 containers to the desired location and assembled to form a plant. Generally, two or more modules are connected together to form a complete plant. The plant can be of any type, e.g., chemical, mechanical/production, thermal, and the like, or of any size, e.g., production, small, micro, or pilot plant scale. When no longer needed, the plant may be disassembled and reused at another site or facility.

Process and apparatus for producing pressurized gaseous nitrogen by cryogenic separation of air. The distillation column system includes a high pressure column, a medium pressure column, a main condenser and top condenser both being condenser-evaporators. Compressed and purified feed air is cooled in a heat exchanger and introduced to the distillation system. A gaseous nitrogen stream from the high pressure column is condensed in the main condenser. Bottom liquid of the medium pressure column is evaporated and gaseous nitrogen from the medium pressure column is condensed in the top condenser. Liquid nitrogen from the medium pressure column is pressurized and introduced to the high pressure column. A second gaseous nitrogen stream from the high pressure column is recovered as pressurized gaseous nitrogen product. A portion of the compressed and purified feed air is work-expanded and then warmed in the main heat exchanger.

The invention relates to a method for constructing or altering a matter- and/or heat-exchange device, said mass- and/or heat-exchange device comprising an assembly of at least one first and one second stackable modular elements (A, B, C, D, E, F, G, H, I, J, K, L), in which the first element is secured over the second element or the second element is secured below the first element in a sealed manner, such that a fluid can flow from the body of the first element to the body of the second element and/or from the body of the second element to the body of the first element.

A method for low temperature separation of air using an air separating installation having a distillation column system which has a first, a second, a third and a fourth separating unit. Compressed and cooled air is fed into the first separating unit. An oxygen-enriched, nitrogen-depleted, argon-containing first sump liquid and a nitrogen-enriched, oxygen-depleted first head gas are formed by means of the first separating unit. An oxygen-rich second sump liquid and an argon-enriched second head gas are formed by means of the second separating unit. A liquid return to the second separating unit is provided by means of the third separating unit. A fourth sump liquid and a fourth head gas are formed by means of the fourth separating unit, and the fourth sump liquid is at least partially returned to the second separating unit.

A stackable modular element comprises a parallelepipedal caisson, the caisson comprising at least one layer of thermal insulation of thickness less than one-third of the width of the caisson, the layer of insulation covering at least the lateral and frontal faces of the caisson and surrounding at least one chamber having a parallelepipedal volume within the caisson, the chamber containing at least one body of material that permits the exchange of mass and/or of heat, the body being parallelepipedal in shape and filling at least part of the chamber, the chamber having an opening on the upper face and/or an opening on the lower face to allow fluid to be transferred to the body from outside the element and/or from the body to outside the element.

A method for obtaining an air product from an air separation plant having a distillation column system and a tank system. The tank system includes a first tank and a second tank. Cryogenic liquid is withdrawn from the distillation column system, stored in the tank system, and used as the air product. The cryogenic liquid is supplied to the first tank and withdrawn from the second tank during a first period, and is supplied to the second tank and withdrawn from the first tank during a second period. The tank system has a third tank to which cryogenic liquid withdrawn from the first tank and the second tank is transferred unheated. The air product is withdrawn from the third tank in liquid state, vaporized and discharged. Alternatively, the cryogenic liquid can be withdrawn from the third tank and stored in the liquid state in a fourth tank.

A liquefier device which may be a retrofit to an air separation plant or utilized as part of a new design. The flow needed for the liquefier comes from an air separation plant running in a maxim oxygen state, in a stable mode. The three gas flows are low pressure oxygen, low pressure nitrogen, and higher pressure nitrogen. All of the flows are found on the side of the main heat exchanger with a temperature of about 37 degrees Fahrenheit. All of the gasses put into the liquefier come out as a subcooled liquid, for storage or return to the air separation plant. This new liquefier does not include a front end electrical compressor, and will take a self produced liquid nitrogen, pump it up to a runnable 420 psig pressure, and with the use of turbines, condensers, flash pots, and multi pass heat exchangers. The liquefier will make liquid from a planned amount of any pure gas oxygen or nitrogen an air separation plant can produce.