A moderate pressure air separation unit and air separation cycle is disclosed that provides for up to about 96% recovery of argon and an overall nitrogen recovery of 98% or greater. The air separation is configured to produce a high purity oxygen enriched stream which is used as the refrigerant to condense the argon in the argon condenser, with the resulting vaporized oxygen stream used to regenerate the temperature swing adsorption prepurifier unit. Argon recovery is facilitated with the use of an argon superstaged column.

The method and the device arc used for the cryogenic decomposition of air in a distillation column system for separating nitrogen and oxygen, said system having a first high-pressure column (23), a low-pressure column (25, 26), and three condenser-evaporators, namely a high-pressure column head condenser (27), a low-pressure column bottom evaporator (28), and an auxiliary condenser (29; 228).

A method for controlling a coupled heat exchanger system having a first heat exchanger block and a second heat exchanger block. A first fluid stream is divided into a first partial current and a second partial current both flowing through the heat exchanger system. A second fluid stream flows through the first heat exchanger block counter to the first partial current. A third fluid stream flows through the second heat exchanger block counter to the second partial current. An intermediate temperature is measured on one of the heat exchanger blocks. The amount of the first partial current and the second partial current is controlled based on the current value of the intermediate temperature. This control reduces the strain on the heat exchangers by changing loads while keeping fluctuations of the intermediate temperature low.

A method and plant for discharging components that are less volatile than oxygen from an air separation plant that contains a main heat exchanger a side condenser and a two-column distillation column system for nitrogen-oxygen separation. The side condenser is constructed as a condenser-evaporator and is arranged in a vessel. A part of the feed air is cooled in the main heat exchanger and liquefied at least in part in the side condenser. A first oxygen fraction is withdrawn in the liquid state from the low-pressure column, introduced into the vessel of the side condenser and in part vaporized. A purge stream is taken off from the bottom of the vessel in the liquid state and discharged or withdrawn as end product. The vessel has a mass transfer section above the side condenser, which mass transfer section corresponds to more than one theoretical plate and fewer than 10 theoretical plates.

A SPECTRA process for low-temperature fractionation of air is proposed, in which bottoms liquid from an additional second rectification column used to obtain oxygen is evaporated in a second condenser evaporator arrangement. In this second condenser evaporator arrangement, gas that has been evaporated beforehand in a first condenser evaporator arrangement, which is used for condensation of tops gas from a first rectification column, is partially condensed after recompression. The invention also relates to a corresponding plant.

The invention relates to a method and device for generating two purified partial air streams under different pressures. A total air stream (1) is compressed to a first total air pressure. The compressed total air stream (5) is cooled with cooling water under the first total air pressure by way of heat exchange (4, 6). The heat exchange with cooling water for cooling the total air stream (5) is carried out as a direct heat exchange in a first direct contact cooler (6), at least in part. The cooled total air stream (9) is divided into a first partial air stream (10) and a second partial air stream (11). The first partial air stream (10) is purified in a first purification device (18) under the first total air pressure, generating the first purified partial air stream (19). The second partial air stream (11) is re-compressed to a higher pressure (12), which is higher than the first total air pressure. The re-compressed second partial air stream (14) is cooled with cooling water in a second direct contact cooler (15) by way of direct heat exchange (13, 15). The cooled second partial air stream (17) is purified under the higher pressure in a second purification device (30), thus generating the second purified partial air stream (31).

An apparatus for separation of air by cryogenic distillation comprising: a system of columns; a first turbine; a warm compressor coupled to the first turbine; a second turbine; a cold compressor coupled to the second turbine; a heat exchanger; means for sending air cooled in the heat exchanger at an intermediate temperature of the heat exchanger to the cold compressor; means for sending expanded air from the second turbine to the system of columns; means for sending air compressed in the cold compressor to an intermediate point of the heat exchanger and then at least in part to the system of columns via a first valve; means for sending air compressed in the cold compressor to the inlet of the first turbine via a second valve without passing through the heat exchanger, wherein the means for sending air compressed in the cold compressor to the inlet of the first turbine via the second valve without passing through the heat exchanger is also connected to the inlet of the first turbine; means for sending a fraction of air cooled in the heat exchanger to an intermediate temperature of the latter to the first turbine; means for sending expanded air from the first turbine to the system of columns; and a bypass line provided with an expansion valve configured to send air from the cold compressor to the system of columns without passing through the heat exchanger.

Method for separating air by cryogenic distillation in an air separation device comprising a system of columns, a first turbine and a second turbine, wherein, in de-icing operation, a common duct bringing air from the two turbines to a column is closed by means of an isolation valve, a purge gas is sent to the turbines at a temperature above 0 C. in order to de-ice them, but purge gas is not sent to the system of columns.

Method for separating air by cryogenic distillation, wherein at least part of the air to be distilled is boosted in an air booster, compressed air is allowed to expand in at least one expansion turbine and, if the pressure drop between two points of the booster passes under a threshold and/or a flow of the booster passes under a minimum flow of the booster, part of the air boosted in the booster is allowed to expand without having been cooled between the booster and the expansion turbine and the boosted expanded air is sent upstream or downstream of the at least one turbine, without having been cooled in the heat exchanger, after having been boosted.

Method for separating air by cryogenic distillation, wherein air is compressed in a compressor and is subsequently sent to a heat exchanger, with the air cooled in the exchanger being sent to a check valve downstream of the heat exchanger and subsequently to a turbine, the valve being positioned so that air from a short-circuiting duct cannot return to the exchanger from the compressor.