A calorimeter and method is also provided, including a sample cell, a reference cell, a thermostat in thermal communication with the sample cell and the reference cell, a first conductive wire, the first conductive wire having a first end connected to the thermostat and a second end connected to the sample cell, and a second conductive wire, the second conductive wire having a first end connected to the thermostat and a second end connected to the reference cell.

A calorimeter and method is also provided, including a sample cell, a reference cell, a thermostat in thermal communication with the sample cell and the reference cell, a first conductive wire, the first conductive wire having a first end connected to the thermostat and a second end connected to the sample cell, and a second conductive wire, the second conductive wire having a first end connected to the thermostat and a second end connected to the reference cell.

A heat flow rate measurement method for use with a differential scanning calorimeter sensor is provided. The method includes calculating a heat exchange between a plurality of sample containers and a reference container placed on a plurality of sample calorimeter units and a reference calorimeter unit, respectively, and determining a heat flow rate of samples within the sample containers using the calculated heat exchange between the plurality of sample containers and the reference container. A multiple sample differential scanning calorimeter sensor and calorimeter system are also provided.

In association with a method and a device for sensory measurement of a material sample, a measurement curve is used to detect deviations from the regular measuring characteristics of the device. A corresponding file can be made available to a service technician for evaluation.

In association with a method and a device for sensory measurement of a material sample, a measurement curve is used to detect deviations from the regular measuring characteristics of the device. A corresponding file can be made available to a service technician for evaluation.

A method for measuring the oil content of a lithium battery separator by using DSC includes the following steps: taking 5-10 mg of an oil-containing separator sample from the lithium battery separator, and taking 5-10 mg of an oil-free separator sample from an oil-free separator; performing an enthalpy test on the oil-free separator sample at room temperature by using a differential scanning calorimeter to obtain a first enthalpy value, and performing an enthalpy test on the oil-containing separator sample by using the differential scanning calorimeter to obtain a second enthalpy value; subtracting the second enthalpy value from the first enthalpy value to obtain a difference, and then dividing the difference by the first enthalpy value to obtain the oil content of the oil-containing separator sample.

Described is a calorimeter that includes a thermal column, a sample container, a reference container, a thermal shield, a diffusion-bonded block and a thermal plate. One or more heat flux sensors are disposed between the thermal column and the sample container and between the thermal column and the reference container. The thermal shield is in thermal communication with the thermal column and is separated from and substantially encloses the sample container, reference container and thermal column. The diffusion-bonded block includes a first metallic layer having a first thermal conductivity, a second metallic layer having a second thermal conductivity and a third metallic layer having a third thermal conductivity. The second thermal conductivity is different from the first and third thermal conductivities. The first metallic layer is in thermal communication with the base of the thermal column and the third metallic layer is in thermal communication with the thermal plate.

Described is a calorimeter that includes a thermal column, a sample container, a reference container, a thermal shield, a diffusion-bonded block and a thermal plate. One or more heat flux sensors are disposed between the thermal column and the sample container and between the thermal column and the reference container. The thermal shield is in thermal communication with the thermal column and is separated from and substantially encloses the sample container, reference container and thermal column. The diffusion-bonded block includes a first metallic layer having a first thermal conductivity, a second metallic layer having a second thermal conductivity and a third metallic layer having a third thermal conductivity. The second thermal conductivity is different from the first and third thermal conductivities. The first metallic layer is in thermal communication with the base of the thermal column and the third metallic layer is in thermal communication with the thermal plate.

A method for measuring the oil content of a lithium battery separator by using DSC includes the following steps: taking 5-10 mg of an oil-containing separator sample from the lithium battery separator, and taking 5-10 mg of an oil-free separator sample from an oil-free separator; performing an enthalpy test on the oil-free separator sample at room temperature by using a differential scanning calorimeter to obtain a first enthalpy value, and performing an enthalpy test on the oil-containing separator sample by using the differential scanning calorimeter to obtain a second enthalpy value; subtracting the second enthalpy value from the first enthalpy value to obtain a difference, and then dividing the difference by the first enthalpy value to obtain the oil content of the oil-containing separator sample.

Disclosed are systems and methods for providing an adiabatic power compensation differential scanning calorimeter to minimize a temperature difference between a sample and a reference. For instance, methods can include providing ramp-up heating power to heat a sample container and a reference container based on a preprogrammed temperature ramp rate; minimizing a temperature difference among the sample container, the reference container, and at least one furnace; providing compensating heat to the sample container and the reference container when a self-heating activity of the sample material is detected; providing container-only compensating heat to the sample container to block heat transfer from the sample material to the sample container once the self-heating activity of the sample material is detected; and providing compensating heat to the reference container to facilitate container-only compensating heat calculation and control.