G01N31/10

Catalyst testing process and apparatus
11260356 · 2022-03-01 · ·

A method for analyzing a catalyst in a catalytic reactor that operates under non-isothermal conditions includes the steps of: positioning a catalyst basket within a catalyst bed within the catalytic reactor, the catalyst basket containing catalyst material the forms the catalyst bed; operating the catalytic reactor, the catalyst basket having dimensions such that a temperature difference (ΔT) along an axial direction (height) of the catalyst basket is non-isothermal; and analyzing the catalyst material contained within the catalyst basket. The temperature difference (ΔT) is, in one embodiment, within a range of 1° C. to 40° C. and preferably, within a range of 5° C. to 25° C.

Catalyst failure detection based combined ammonia to NOx ratios, conversion inefficiency values and ammonia slip values
09790835 · 2017-10-17 · ·

Implementations of systems and methods for detecting the failure of an selective catalytic reduction (SCR) catalyst may include a controller or one or more circuits for acquiring an ammonia to NOx ratio (ANR) value for exhaust gas flowing through an exhaust system, acquiring a conversion inefficiency value indicative of a conversion inefficiency of the SCR catalyst, acquire an NH.sub.3 slip value indicative of an amount of NH.sub.3 slip through the exhaust system downstream of the SCR catalyst, calculate a combined ANR/conversion inefficiency/NH3 slip (ACN) value based on the ANR value, conversion inefficiency value, and NH.sub.3 slip value, and indicating a failure of the SCR catalyst responsive to the calculated ACN value exceeding a predetermined threshold value.

Hydrogen sensor and method for manufacturing the same

A hydrogen sensor and a method for manufacturing the same are provided. The hydrogen sensor includes a metal oxide layer formed over a substrate, and a catalytic pattern that is formed over the metal oxide layer. Further, a protective layer is formed over the catalytic pattern.

Hydrogen sensor and method for manufacturing the same

A hydrogen sensor and a method for manufacturing the same are provided. The hydrogen sensor includes a metal oxide layer formed over a substrate, and a catalytic pattern that is formed over the metal oxide layer. Further, a protective layer is formed over the catalytic pattern.

REACTOR AND MULTIFUNCTIONAL RISER AND DOWNER SIMULATOR INCORPORATING THE SAME
20170320036 · 2017-11-09 ·

A reactor comprises a reactor vessel defining a confined reactor volume, a support assembly extending about a periphery of the confined reactor volume, a basket positioned within the reactor vessel and supported by the support assembly, the basket having an interior surface and an exterior surface, a downflow zone being defined between the exterior surface of the basket and an interior surface of the confined reactor volume, an inlet screen positioned adjacent to one end of the interior surface and an outlet screen positioned adjacent to an opposite end of the interior surface, an upflow zone defined between the inlet screen and outlet screen, the inlet screen and the outlet screen containing a quantity of particulate catalyst, and a circulating device positioned above said upflow zone and configured to continuously circulate fluid upwardly though said upflow zone and downwardly through said downflow zone, the support assembly and the basket configured to promote the formation of a fluid vortex within a portion of the downflow zone.

DISTANCE MEASURING DEVICE AND METHOD FOR MEASURING DISTANCE
20220236241 · 2022-07-28 ·

A distance measuring device includes a measuring member holding a length measuring instrument and at least one rail member (base member) on which the measuring member is movably disposed. When a straight line parallel to a direction in which the measuring member disposed on the base member moves is defined as a reference line, an angle formed by a straight line parallel to an axial length direction of a reaction tube and the reference line, which are on an identical plane, is constant for the plurality of reaction tubes disposed side by side along the reference line. A measurement direction of the length measuring instrument is parallel to the axial length direction of the reaction tube in a state where the measuring member is disposed on the base member. The measuring member is disposed on the base member to be able to sequentially move.

DISTANCE MEASURING DEVICE AND METHOD FOR MEASURING DISTANCE
20220236241 · 2022-07-28 ·

A distance measuring device includes a measuring member holding a length measuring instrument and at least one rail member (base member) on which the measuring member is movably disposed. When a straight line parallel to a direction in which the measuring member disposed on the base member moves is defined as a reference line, an angle formed by a straight line parallel to an axial length direction of a reaction tube and the reference line, which are on an identical plane, is constant for the plurality of reaction tubes disposed side by side along the reference line. A measurement direction of the length measuring instrument is parallel to the axial length direction of the reaction tube in a state where the measuring member is disposed on the base member. The measuring member is disposed on the base member to be able to sequentially move.

Device and method for catalytically converting chemical substances at dwell times in the range of 0.1-10 seconds
11207652 · 2021-12-28 · ·

Disclosed herein is an apparatus and a method for catalytic conversion of chemical substances in the presence of pulverulent catalysts in a trickle bed reactor with residence times in the range of 0.1-10 seconds, wherein the apparatus includes a trickle bed reactor (2), the inlet side of which is functionally connected to a catalyst reservoir vessel (1) and a reactant feed, and the outlet side of which is functionally connected to a separator (3). The separator (3) has an exit conduit for leading off product stream, wherein the apparatus has the characteristic feature that the exit conduit disposed on the separator (3) for leading off product stream has a continuously acting valve connected via a controller to a pressure measurement sensor, wherein the continuously acting valve and the pressure measurement sensor form a pressure control circuit with a controller.

Method of determining a relative decrease in catalytic efficacy of a catalyst in a catalyst solution

The present disclosure provides a method of determining a relative decrease in catalytic efficacy of a catalyst in a test sample of a catalyst solution with unknown catalytic activity. The method includes (a) mixing the test sample with a test solvent to form a test mixture and (b) measuring the increase in the temperature of the test mixture at predetermined time intervals immediately after forming the test mixture. A predetermined feature is used to determine both a test value in the increase in temperature measured in (b) and a control value in a known increase in temperature of a control mixture of the test solvent with a control sample of a control catalyst solution. The relative decrease in catalytic efficacy of the catalyst in the test sample having the unknown catalytic activity is then determined from: Relative Decrease in Catalytic Efficacy=Control Value−Test Value/Control Value.

Multiple reactor system for parallel catalyst testing

A reactor system for conducting multiple continuous reactions in parallel may include a preheating unit that includes an outer preheater shell and a plurality of heating tubes disposed within the preheating shell and arranged in parallel. The reactor system may include a reactor unit downstream of the preheating unit, the reactor unit comprising a plurality of reactor tubes disposed within a reactor shell and an outer heating element disposed about the reactor shell. An inlet end of at least one of the reactor tubes may be fluidly coupled to at least one of the heating tubes of the preheating unit. The reactor unit may include a multi-chamber separator downstream of the reactor unit, the multi-chamber separator having a plurality of separation chambers. At least one of the separation chambers may be fluidly coupled to at least one of the reactor tubes.