This disclosure provides techniques for extending useful life of a reference electrode, as well as a novel voltametric system and measurement cell design and related chemistries. An automated, repeatable-use system features a reference electrode that directly immerses a metallic conductor into an analyte, with electrolytes (e.g., chlorides) used for measurement being separately added and removed for each measurement cycles; the metallic conductor can optionally be left exposed to clean dry air in between measurements. In one implementation, the system can be restricted to application with specific analytes (e.g., ground water) that are known in advance to be free of substances that could degrade reference electrode use or lifetime. Cleaning solutions can optionally be used that would not be practical with conventional (insulated) reference electrode designs. In another embodiment, a measurement cell can be configured to receive separated electrode modules, permitting independent cleaning/removal of the working electrode (or other electrodes).

A qualitative and quantitative heavy metal analysis device and, more particularly, a qualitative and quantitative heavy metal analysis device implemented by a rotary platform are provided. The rotary platform device includes a main injection part which is positioned near a rotating shaft of a rotary platform, wherein the main injection part is configured to receive a fluid sample containing heavy metals, a pH adjusting part configured to adjust pH of the fluid sample, a detecting part coated with a chelating agent configured to initiate a color reaction with heavy metals in the fluid sample by spreading the pH-adjusted fluid sample into the detecting part, and a ruler for measuring a spreading distance of the color reaction, wherein the fluid sample moves from the main injection part through the pH adjusting part to the detecting part by a rotation of the rotary platform device.

A qualitative and quantitative heavy metal analysis device and, more particularly, a qualitative and quantitative heavy metal analysis device implemented by a rotary platform are provided. The rotary platform device includes a main injection part which is positioned near a rotating shaft of a rotary platform, wherein the main injection part is configured to receive a fluid sample containing heavy metals, a pH adjusting part configured to adjust pH of the fluid sample, a detecting part coated with a chelating agent configured to initiate a color reaction with heavy metals in the fluid sample by spreading the pH-adjusted fluid sample into the detecting part, and a ruler for measuring a spreading distance of the color reaction, wherein the fluid sample moves from the main injection part through the pH adjusting part to the detecting part by a rotation of the rotary platform device.

Provided herein is a method for measuring a concentration of a metal ion in an electrodeposition solution. The method of the present disclosure can substantially reduce the interference of organic additives and different electrode conditions on voltammetric metal ion concentration measurements.

Disclosed is a method for estimating deterioration of a steel support structure (180) supporting an offshore wind turbine (181). The steel support structure (180) being made of a first type of steel, the method comprising the steps of: (a) providing a first sensor (111) having one or more sensor elements, wherein a first sensor element of the one or more sensor elements is made of a type of steel corresponding to the first type of steel; (b) arranging the first sensor (111) in connection with said steel support structure (180); (c) inducing an electrical current through at least one of the one or more sensor elements; (d) monitoring the deterioration of a part of the first sensor (111) by in a first time interval measuring electrical properties of the first sensor (111) and storing the measurements as first data; (e) estimating the deterioration of the steel support structure (180) from the first data.

Disclosed is a method for estimating deterioration of a steel support structure (180) supporting an offshore wind turbine (181). The steel support structure (180) being made of a first type of steel, the method comprising the steps of: (a) providing a first sensor (111) having one or more sensor elements, wherein a first sensor element of the one or more sensor elements is made of a type of steel corresponding to the first type of steel; (b) arranging the first sensor (111) in connection with said steel support structure (180); (c) inducing an electrical current through at least one of the one or more sensor elements; (d) monitoring the deterioration of a part of the first sensor (111) by in a first time interval measuring electrical properties of the first sensor (111) and storing the measurements as first data; (e) estimating the deterioration of the steel support structure (180) from the first data.

This disclosure provides techniques for extending useful life of a reference electrode, as well as a novel voltametric system and measurement cell design and related chemistries. An automated, repeatable-use system features a reference electrode that directly immerses a metallic conductor into an analyte, with electrolytes (e.g., chlorides) used for measurement being separately added and removed for each measurement cycles; the metallic conductor can optionally be left exposed to clean dry air in between measurements. In one implementation, the system can be restricted to application with specific analytes (e.g., ground water) that are known in advance to be free of substances that could degrade reference electrode use or lifetime. Cleaning solutions can optionally be used that would not be practical with conventional (insulated) reference electrode designs. In another embodiment, a measurement cell can be configured to receive separated electrode modules, permitting independent cleaning/removal of the working electrode (or other electrodes).

Disclosed are methods that, by not physically touching a material being measured, can measure the material's differential response quite accurately. A collimated light shines on the material under test is reflected off it, and is then captured by a device that records the position where the reflected light is captured. This process is done both before and after the material is processed in some way (e.g., by applying a coat of paint). The change in position where the reflected light is captured is used in calculating the deflection of the material as induced by the process. This measured induced deflection is then used to accurately determinate the stress introduced into the material by the process. Other characteristics of the material under test, such as aspects of the material composition of a bi-metallic strip, for example, may also be determined from a deflection measurement.

Provided herein is a method for measuring a concentration of a metal ion in an electrodeposition solution. The method of the present disclosure can substantially reduce the interference of organic additives and different electrode conditions on voltammetric metal ion concentration measurements.

The present disclosure provides techniques for determining plating conditions by numerically analyzing a film-thickness distribution. The disclosed techniques comprise performing electrochemical measurement in an electroplating apparatus; determining electrochemical parameters based on a result of the electrochemical measurement; receiving initial plating conditions for performing a plating process; based on the electrochemical parameters and the initial plating conditions, determining a current density distribution on a surface of a substrate based on a function formula which comprises a variable which represents a position on the substrate; based on the current density distribution, calculating a thickness of a film to be plated on the substrate; and performing the plating process based on final plating conditions corresponding to a calculated film-thickness distribution satisfying a desired film-thickness distribution.