An X-ray fluorescence analyzer comprises an X-ray tube for emitting incident X-rays in the direction of a first optical axis. A slurry handling unit is configured to maintain a constant distance between a sample of slurry and the X-ray tube. A first crystal diffractor is located in a first direction from the slurry handling unit, and configured to separate a predefined first wavelength range from fluorescent X-rays that propagate into the first direction. It is configured to direct the fluorescent X-rays in the separated predefined first wavelength range to a first radiation detector. The input power rating of said X-ray tube is at least 400 watts. The first crystal diffractor comprises a pyrolytic graphite crystal. The optical path between said X-ray tube and the slurry handling unit is direct with no diffractor therebetween.

Systems and methods are provided for determining an exposure temperature in an engine. One or more particles filtered from lubrication fluid of an engine may be analyzed. The chemical composition of filtered particles may be compared to reference data which includes a relationship between chemical composition and exposure temperature. An estimate of the exposure temperature may be determined. An output may be generated based on the exposure temperature.

A method of analysing granular material in a slurry, the method comprising: compacting the granular material in the slurry to form one or more pucks; irradiating said pucks with X-Ray radiation and detecting X-ray energy transmitted through said one or more irradiated pucks; irradiating a reference material with X-Ray radiation, said reference material having known material characteristics and detecting X-ray energy transmitted through said reference material; comparing X-ray energy transmission through said one or more pucks with the reference material to compute, using a processing unit, one or more particle characteristics of the granular material in the one or more pucks.

An X-ray diffraction method measures crystallite size distribution in a polycrystalline sample using an X-ray diffractometer with a two-dimensional detector. The diffraction pattern collected contains several spotty diffraction rings. The spottiness of the diffraction rings is related to the size, size distribution and orientation distribution of the crystallites as well as the diffractometer condition. The invention allows obtaining of the diffraction intensities of all measured crystallites at perfect Bragg condition so that the crystallite size distribution can be measured based on the 2D diffraction patterns.

Chemical components in a mixture are analysed using scattering data representing the results of a diffraction experiment performed on the mixture. Using non-negative matrix factorisation or another optimisation technique, the scattering data is deconvolved into non-negative basis components that represent contributions to the scattering data from each chemical component and fitting coefficients are derived in respect of the basis components that represent the proportions of chemical components in the mixture.

The invention relates to a method for calibrating a radiometric apparatus for determining and/or monitoring density of a medium (6) located in a container (1). The method includes method steps as follows: determining the mass attenuation coefficient .sub.C of the empty container (1) with application of the half value thickness N/N.sub.0=0.5 of the radioactive radiation upon passage through the empty container (1) according to the formula: N/N.sub.0I/I.sub.0=e.sup..sup.C.sup.1D, with .sub.C: mass attenuation coefficient, 1: density of the material of the wall of the container, D: distance traveled by the radiation, or inner diameter of the container (1), I: intensity the measured radiation, I.sub.0 intensity of the transmitted radiation, N measured counting rate, N.sub.0 counting rate of the transmitted radiation, determining the mass attenuation coefficient (.sub.M) based on the measured intensity, or the counting rate, of the radioactive radiation after passage through the container (1), when a calibration medium of known density (2) is located in the container (1), ascertaining the dependence of the linear absorption coefficient () on the geometric dimensions of the container (1) based on the two mass attenuation coefficients, calculating a calibration curve, which shows the dependence of the density of the medium on the count of measured radiation intensity after passage through the container (1).

Fluidic and electrofluidic devices comprising carbon nanotubes and methods of making and using the same are provided. The carbon nanotubes may be densely bundled to span an aperture in a substrate. A polymeric coating over the substrate may contain reservoir(s) etched therein, the reservoir(s) in fluid connectivity with the carbon nanotubes. X-rays may be directed through the aperture and fluid-filled carbon nanotubes with x-ray analysis providing data on fluid structure and dynamics inside the carbon nanotubes.

An X-ray spectrometer is provided with: an excitation source configured to irradiate excitation rays onto an irradiation area of a sample, a diffraction member provided to face the irradiation area; a slit member provided between the irradiation area and the diffraction member, the slit member having a slit extending parallel to the irradiation area and a prescribed surface of the diffraction member; an X-ray linear sensor having a light-incident surface in which a plurality of detection elements are arranged in a direction perpendicular to a longitudinal direction of the slit; a first moving mechanism configured to change an angle between the sample surface and the prescribed surface, and/or a distance between the sample surface and the prescribed surface by moving the diffraction member within a plane perpendicular to the longitudinal direction; and a second moving mechanism configured to position the X-ray linear sensor on a path of characteristic X-rays passed through the slit and diffracted by the prescribed surface by moving the X-ray linear sensor within a plane perpendicular to the longitudinal direction.

A measurement head for making X-ray measurements on drilling fluid includes an inner pipe (30) having a outlet (32) and an outer pipe (34) around the inner pipe. Drilling fluid is pumped through the outlet refreshing the fluid at the outlet. The pump is then stopped. A height sensor (42) is then used to measuring the height of a meniscus of drilling fluid at the outlet (32). An X-ray head (50) including an X-ray source (52) and an X-ray detector (54) is then moved into a reproducible position above the meniscus of fluid above the outlet. The height sensor (42) may be fixed to a movable cover (40), to the X-ray head (50) or to some other part of the measurement head.

A method for use in measuring a composition of a multiphase fluid which includes flowing a multiphase fluid through a fluid flow path defined by a wall of a fluid conduit is disclosed. The wall includes an electrically non-conductive material. The method includes establishing an electromagnetic field which extends through the electrically non-conductive material of the wall of the fluid conduit into the fluid and measuring a property of the electromagnetic field over a measurement time period. The method also includes transmitting additional energy through the fluid over the measurement time period independently of the electromagnetic field and measuring the additional energy transmitted through the fluid over the measurement time period. The method may be used to unambiguously determine a composition of a multiphase fluid which has different components.