The present invention relates to apparatus for measuring fuel thermal stability, deposit formation rate, and in-situ reactivity via optical methods and as well as methods of making and using same. Applicants' apparatus can deliver the rate and amount of degradation as well as the quantifying and qualifying the chemical species in the fuel on a real time basis during a test. As a result, Applicants' apparatus provides significantly improved performance over the current apparatuses.

An oil degradation meter and a method for evaluating oil degradation are provided, in which a user is enabled to arbitrarily set a degradation of oil/fat using an acid value (AV value) as an index, and capable of learning a replacement time of oil/fat easily with a stable reproducibility, even in a case where a condition such as a moisture amount in food (deep-fried food) is different. In a setup procedure, an acid value (AV.sub.0) of unused oil/fat is set to 0, a dielectric constant (D.sub.0) at that time is measured and recorded, a dielectric constant (D.sub.100) of oil/fat at a replacement time under a specific oil/fat usage condition is measured, and it is recorded along with an acid value (AV.sub.100) at that time, and in a measurement procedure, a dielectric constant (D.sub.n) of the sample oil/fat is measured, and an acid value (AV.sub.n) of said sample oil/fat is calculated based on the dielectric constants (D.sub.0, D.sub.100) and the acid value (AV.sub.100) recorded in said setup procedure, according to a calculation formula of [AV.sub.n=AV.sub.100{(D.sub.nD.sub.0)/(D.sub.100D.sub.0)}].

Apparatus includes a pivotable, cradling framework that can hold a rotatable bomb instrument, which can include a hollow cylinder and a grease rack. This may be employed to effect a significantly improved version of the ASTM D942 Test Method. The same is useful in measurement of grease oxidation.

A method of evaluating formation of fouling material in a petroleum feed involves illuminating a sample with cross-polarized light while subjecting the sample to temperature and pressure conditions relevant to an industrial process to induce chemical and/or physical changes; collecting images of the treated sample; and analyzing the images to evaluate fouling formation based on heterogeneity of the images in terms of brightness and/or color, where an increase in heterogeneity is indicative of initiation of fouling formation. The method is conducted using a cross-polarized microscopy system including a hot stage reactor assembly capable of withstanding operation within a temperature between about 20 C. to 450 C. or higher, and a pressure between about 0.1 MPa to 16 MPa or higher.

A sensor for monitoring the quality of oil in mechanical machinery is provided. The sensor includes a portion that is sealed from the oil which contains electric circuitry to process signals received from the sensing elements. Another portion of the sensor is exposed to the oil and contains one or more sensing elements to sense one or more properties of the oil. The sensed properties may include electrical properties, temperature properties and/or optical properties.

Machine for testing thermal resistance of plastic materials, comprising a tank configured, in use, to be filled for example with a heat-transfer fluid; a heating coil for heating the heat-transfer fluid; a temperature sensor generating a temperature signal of the heat-transfer fluid; and a control unit calculating a degradation index of the heat-transfer fluid on the basis of the temperature signal. In particular, the degradation index is calculated by determining the temperature range associated with the temperature signal, updating the corresponding partial heating time, and calculating the weighted sum of the partial heating times previously saved in memory and pertaining to different temperature ranges. Upon reaching one or more thresholds, signals are generated which indicate the need to replace the heat-transfer fluid.

Jet fuels' thermal oxidation characteristics are evaluated via the Standard Test Method for Thermal Stability of Aviation Turbine Fuels. This test method mimics the thermal stress conditions encountered by jet fuel in operation and is often carried out by laboratory devices, known as rigs. The rigs include a test section having a sleeve and a heater tube arranged therein. A pair of bus bars secure the test section to the rig and apply a current to the heater tube. The applied current heats the heater tube and subjects the sample jet fuels that are flowing in the volume between the sleeve and heater tube to high temperatures, which may produce thermal oxidation deposits on the heater tube. Heater tubes are difficult to install, however, and a gauge may be used to ensure accurate placement of the heater tube within the sleeve. In addition, the fuel sample must be prepared via an aeration process, and systems are disclosed for automating the aeration process such that the sample is prepared precisely according to the test standard. Moreover, the rig includes a pump system that moves the fuel sample through the test section, and a pump system is provided in a double syringe arrangement that optimizes fuel flow through the test section without fluctuation. Finally, the rigs include cooling systems for cooling the bus bars and maintaining an appropriate thermal profile within the heater tube, and cooling systems may be provided that independently control the temperature of each bus bar.

Elevated temperature liquid testing apparatus and methodology in which a thin film of test liquid and a reactant/control gas are provided about the top of a depositor member that is surrounded by a special mantle, for example, a substantially cylindrically walled glass mantle. As an oxidative engine oil test, it may mimic turbocharger conditions of a modern internal combustion engine. For example, employing moist air, the apparatus can test a thin film of engine oil for oxidation deposits at a predetermined temperature, say, 285 C., 290 C., or cycled between 285 C. or 290 C. and 320 C. or 330 C.

A foam testing apparatus with a closed loop air circulation along a sample cylinder which maintains a lubrication oil sample at a desired temperature during a test procedure. The apparatus may include a digital camera adjacent to the sample cylinder for observation and recording of foam characteristics during the test procedure.

Apparatus includes a pivotable, cradling framework that can hold a rotatable bomb instrument, which can include a hollow cylinder and a grease rack. This may be employed to effect a significantly improved version of the ASTM D942 Test Method. The same is useful in measurement of grease oxidation.