An apparatus for analysis of metals is provided. The apparatus includes a molding cavity for receiving a sample of a molten metal, a gating system for allowing the molten metal to be poured, and a vent for allowing gases to escape from the apparatus when the molten metal is poured. The apparatus further includes at least one chill plate, adjacent to the molding cavity, for enabling faster cooling and solidification of the sample of the molten metal. The apparatus also includes a longitudinal slot, extending from the molding cavity, for allowing a sensor element to be introduced into the sample of the molten metal, the sensor element is a thermocouple wire that is used to monitor a cooling curve of the molten metal, while the molten metal solidifies.

The present invention relates to a sampler for taking samples from a molten metal bath, particularly a molten iron, the sampler comprising: a carrier tube having an immersion end; and a sample chamber assembly arranged on the immersion end of the carrier tube, the sample chamber assembly comprising a cover plate and a housing, wherein the housing comprises: an immersion end having a first opening for an inflow conduit and an opposing end having a second opening for a gas coupler, a first face extending between the immersion end and the opposing end, the first face having a first depression proximate the immersion end and a second depression, the first depression being an analysis zone and the second depression being a ventilation zone, a portion of the analysis zone overlying a distribution zone which is in direct flow communication with the first opening and configured to receive the molten steel from the inflow conduit, wherein the first depression having a cross sectional circle segment profile along a central longitudinal axis that is concavely or triangularly shaped, wherein the cover plate and the housing are configured to be assembled together to form a sample cavity including the distribution zone, the analysis zone and the ventilation zone, such that an analysis surface of a solidified steel sample formed within the sample cavity lies in a first plane, and wherein the first and second openings are spaced apart from the first plane. The invention also relates to a sampler for taking samples from a molten metal bath, particularly a molten iron.

This invention relates to nonferrous metallurgy, in particular to a device and method for electrolyte composition analysis based on differential thermal measurements for aluminum electrolysis control. The device is comprised of a metal body including a reference material and an electrolyte sample receptacle, temperature sensors immersed into the reference material and in an electrolyte sample, a system for registration, data processing, and visualization of obtained results. A method includes immersing a metal body into an electrolyte; filling a receptacles with the molten electrolyte; removing and cooling down the metal body having the filled receptacle above a crust on the molten electrolyte surface; drawing and analyzing differential-thermal curves based on which the liquidus temperature, electrolyte superheating and phase and blend compositions of electrolyte solid samples are determined taking into account all crystallizing phases the content of which in the electrolyte sample is no less than 3 wt %.

An apparatus for producing metal bars and ingots with quality monitoring, includes at least one mold essentially constituted by a body that forms at least one cavity for forming an ingot or a bar and by at least one cover that is detachably associated with the body in order to upwardly close the cavity. The apparatus has at least one passage, provided on the body of the mold, on the cover or on both, for connecting the inside of the cavity to the outside even when the cover is associated with the body in order to upwardly close the cavity. The apparatus according to the invention also has the particularity that it includes a means for taking a sample of the melted material contained in a mold, constituted essentially by a body that forms at least one cavity for forming an ingot or a bar and by at least one cover that is detachably associated with the body in order to upwardly close the cavity. The present invention also relates to a plant and a method for producing metal bars and ingots with quality monitoring.

A method of analyzing a phase transformation process of a material comprises providing a spherical sample of the material, measuring and recording a first data series of core temperature at the sample's center of gravity, measuring and recording a respective second data series of temperature at the sample's periphery, measuring and recording a respective third data series of radial displacements at the sample's periphery, and calculating a change in pressure in the sample at a plurality of points in time based on first, second and third said data series.

An immersion sensor is configured to determine the content of a chemical element in molten metal. The immersion sensor has an auxiliary electrochemical cell extending from an interior surface into the internal volume of a sampling chamber. The sampling chamber can be integrally-formed in a sensor head or in a separate refractory structure. The immersion sensor may be configured for the flow of molten metal into the internal volume of the sampling chamber and into contact with the auxiliary electrochemical cell.

The present invention relates to an apparatus for demolding and analyzing a direct analysis sample formed from a molten metal material contained within a sample chamber assembly, wherein the sample chamber assembly comprises at least a sample housing, a cover plate and closing means, comprising: a cabinet defining an interior and comprising at least one opening for the sample housing to enter the cabinet, and analyzing means located inside the cabinet for analyzing an analysis surface of the sample; demolding means adapted to remove at least the closing means to expose at least part of the analysis surface of the sample; and transporting means adapted to hold and transport the sample housing at least between a sample demolding position, where the closing means is removed by the demolding means, and a sample analysis position, where the analysis surface of the sample is analyzed by the analyzing means, and wherein the sample demolding position and the sample analysis position are different from each other.

The invention also relates to a system and method for demolding and analyzing a direct analysis sample.

An apparatus for producing metal bars and ingots with quality monitoring, includes at least one mold essentially constituted by a body that forms at least one cavity for forming an ingot or a bar and by at least one cover that is detachably associated with the body in order to upwardly close the cavity. The apparatus has at least one passage, provided on the body of the mold, on the cover or on both, for connecting the inside of the cavity to the outside even when the cover is associated with the body in order to upwardly close the cavity. The apparatus according to the invention also has the particularity that it includes a means for taking a sample of the melted material contained in a mold, constituted essentially by a body that forms at least one cavity for forming an ingot or a bar and by at least one cover that is detachably associated with the body in order to upwardly close the cavity. The present invention also relates to a plant and a method for producing metal bars and ingots with quality monitoring.

This invention relates to nonferrous metallurgy, in particular to a device and method for electrolyte composition analysis based on differential thermal measurements for aluminum electrolysis control. The device is comprised of a metal body including a reference material and an electrolyte sample receptacle, temperature sensors immersed into the reference material and in an electrolyte sample, a system for registration, data processing, and visualization of obtained results. A method includes immersing a metal body into an electrolyte; filling a receptacles with the molten electrolyte; removing and cooling down the metal body having the filled receptacle above a crust on the molten electrolyte surface; drawing and analyzing differential-thermal curves based on which the liquidus temperature, electrolyte superheating and phase and blend compositions of electrolyte solid samples are determined taking into account all crystallizing phases the content of which in the electrolyte sample is no less than 3 wt %.

Disclosed is a disc-shaped sample chamber for collecting molten metal, the chamber comprising: a chamber body having a left body and a right body bonded to each other to define a disc-shaped sample space therebetween; an inlet extending upward from the chamber body and connecting the sample space with the outside; and a welded bonding portion disposed on at least one lateral face of the chamber body for bonding the left body and the right body to each other. Further, a probe having the chamber is disclosed.