A device and method for headspace sampling is disclosed herein. The headspace sampling device comprises a sample holding device configured to be sealed in a vial. The sample holding device has a pair of electrodes gap spaced from one another and a basket extending between the electrodes configured to hold a sample. The basket is configured to heat a sample held therewith and volatize at least a portion of the sample upon an electrical current being passed through the electrodes and the basket.

The invention relates to a device for determining a volume of gas in a sample contained in a vessel, the device comprising: a frame configured to attach the vessel; a needle having a longitudinal axis, comprising a proximal part and a distal part, the distal part being configured to pierce the vessel and the proximal part comprising a lumen; and an analysis compartment comprising a cell in fluid communication with the lumen of the proximal part of the needle. The invention also relates to a method for determining a volume of gas in a sample contained in a vessel.

The invention provides a method for verifying the age of an animal providing meat using volatile profiles that comprises the step of providing a sample of animal meat. The method uses one or more chemical analyses to obtain a profile of a set of volatile organic compounds from a sample of meat from an animal. The profile is fit to a mathematically discriminating function resulting. The data obtained is analyzed in order to establish a correlation between the age of the animal (tooth development) and volatiles exuded by meat.

A system and method calibrate efficiency of a gas extraction system in extracting hydrocarbons from mud flowing in a drilling operation. A background reading of a hydrocarbon is extracted from the mud flowing in the drilling operation with the gas extraction system and is checked for stability. An injection operation injects a known concentration of the hydrocarbon into mud, and a subject reading of the hydrocarbon is obtained with the gas extraction system during the injection operation. A correction factor of the hydrocarbon is determined for the gas extraction system by comparing the subject reading against its corresponding known concentration. Then, at least one operational reading of the hydrocarbon extracted from the mud with the gas extraction system can be corrected using the determined correction factor.

A sample extraction device and a desorption device for use in gas chromatography (GC), gas chromatography-mass spectrometry (GCMS), liquid chromatography (LC), and/or liquid chromatography-mass spectrometry (LCMS) are disclosed. In some examples, the sample extraction device includes a lower chamber holding a sorbent. The sample extraction device can extract sample headspace gas from a sample vial by placing the sorbent inside the vial and creating a vacuum to increase recovery of low volatility compounds, for example. Once the sample has been collected, the sample extraction device can be inserted into a desorption device. The desorption device can control the flow of a carrier fluid (e.g., a liquid or a gas) through the sorbent containing the sample and into a pre-column and/or a primary column of a chemical analysis device for performing GC, GCMS, LC, LCMS, and/or some other chemical analysis process.

A gas analysis system for engaging a sealed container to withdraw and analyze gas from the sealed container, the system comprising: a penetration implement configured to create an opening to permit withdrawal of gas from the container; a chamber operatively coupled to the penetration implement for receiving gas from the container; a gas analyzer; a seal configured to engage the container to enable the system to maintain an enclosed volume comprising the chamber and an interior of the container after the penetration implement has created an opening in the container; and a mechanism to effect flow of gas from the container to the chamber, and thereafter from the chamber to the gas analyzer, the mechanism comprising a first valve operatively coupled to the penetration implement, and a connection pipe configured to connect with the gas analyzer; wherein the first valve is movable between a first position in which it permits flow of gas from the container to the chamber, and prevents gas from escaping from the enclosed volume or being contaminated, and a second position in which it permits flow of gas from the chamber to the connection pipe and the gas analyzer.

The present invention provides a method for determining hydrogen sulfide (H.sub.2S) by headspace single-drop liquid phase microextraction and intelligent device colorimetry, which comprises: taking a silver-gold core-shell triangular nanosheet (Ag@Au TNS) as a nanodetection probe, in combination with an analysis method of headspace single-drop microextraction (HS-SDME), specifically extracting H.sub.2S volatilized from a sample to be detected by the nanodetection probe, and detecting H.sub.2S in the extracted sample with the help of the photographing function of an intelligent device and a color picking software. Compared with the prior art, the present invention adopts intelligent device colorimetry, with the limit of detection of about 65 nM and the linear range of 0.1-100 μM, and the established method can be applied to the determination of H.sub.2S in actual samples such as egg white, milk and other opaque samples, and has the advantages of few procedures, simple operation, high detection efficiency and the like.

A device determines an oxygen content of a headspace gas in a liquid-filled container. The device contains a piercer, a sampling tube, a piercing head on which the piercer and the sampling tube are disposed, a pump, a ring line, and a sensor unit disposed within the ring line and used to determine the oxygen content and/or an oxygen partial pressure of the headspace gas of the liquid-filled container. The ring line is configured such that the headspace gas of the liquid-filled container can be sampled via the piercer or the piercing head by use of the pump and can be returned into the headspace of the liquid-filled container via the sampling tube.

A headspace extraction and analysis method for volatile compounds can be performed in automatic mode in a HS-ITEX apparatus adapted to be additionally connectable to a vacuum source. The method includes extracting the headspace by sucking volatile compounds into a sorbent-containing trap followed by desorption into the injector of a GC-MS analyzer.

Beverage processing system for filling a beverage into containers with a filler with several filling valves for filling the beverage into the containers, where the filling valves are each configured having a filling device for filling at least two components of the beverage into one of the containers, a capper for closing the container filled with the beverage, and with a conveyor for transporting the containers at least from the filler to the capper, characterised in that the beverage processing system comprises at least one gas analysis device for quality control of the mixed beverage filled into the containers, and in that the at least one gas analysis device each comprises a gas suctioning device for suctioning gas from a head region of the containers filled with the beverage and an analyzer for analyzing the suctioned gas.