G01N30/7206

METHOD OF QUANTITATIVELY ANALYZING 11 AMIDE ALKALOIDS IN TOBACCO LEAVES USING GAS CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY
20230152284 · 2023-05-18 ·

A method for quantitatively analyzing 11 amide alkaloids in tobacco leaves using gas chromatography-tandem mass spectrometry, comprises: soaking with a sodium hydroxide solution so as to free amide alkaloids from a tobacco powder sample matrix, transferring target compounds into an ether layer through extraction with methyl tertiary butyl ether, concentrating methyl tertiary butyl ether extraction liquids for analysis with gas chromatography-tandem mass spectrometry, inputting chromatographic peak areas obtained by an instrument into standard calibration curve fitting equations of the corresponding amide alkaloids to obtain the concentrations of the corresponding target compounds, and converting the concentrations to obtain the contents of the corresponding amide alkaloids in the tobacco leaves. The method can quantitatively analyze the 11 amide alkaloids at the same time, and has the advantages of simpleness, rapidness, stability and the like.

SYSTEM AND METHOD FOR ANALYZING LIGHT N-ALKANE COMPONENTS AND CARBON ISOTOPES IN DEEP AND ULTRA-DEEP SOURCE ROCK
20230152285 · 2023-05-18 ·

A method for analyzing light n-alkane components and carbon isotopes in deep and ultra-deep source rocks includes: (S1) subjecting a 5A molecular sieve column to aging; (S2) pyrolyzing a source rock; and allowing a pyrolysis product to enter the 5A molecular sieve column; where n-alkanes are adsorbed and retained by the 5A molecular sieve column; allowing an outflow to pass through a fractionation plate and an empty column or a weak polarity column to be discharged; and (S3) performing programmed heating such that the n-alkanes adsorbed on the 5A molecular sieve column are successively desorbed according to molecular weight, and then pass through the fractionation plate and the HP-5 or DB-5 column to enter a mass spectrometer for composition analysis or isotopic analysis. An analysis system is further provided.

METHOD FOR MULTI-INFORMATION FUSION OF GAS SENSITIVITY AND CHROMATOGRAPHY AND ON-SITE DETECTION AND ANALYSIS OF FLAVOR SUBSTANCES BASED ON ELECTRONIC NOSE INSTRUMENT

Provided is a method for multi-information fusion of gas sensitivity and chromatography and on-site detection and analysis of flavor substances using an electronic nose instrument. The electronic nose instrument includes a gas sensor array module (I), a capillary gas chromatographic column module (II), an automatic headspace sampling module (III), a computer control and data analysis module (IV), an automatic lifter (V) for headspace sampling, a large-volume headspace vapor generation device (VI) and two auxiliary gas sources (VII-1, VII-2). The electronic nose instrument detects a large number of odorous samples to establish a big odor data. On this basis, the normalization fusion preprocessing is done, and the cascade machine learning model realizes both an on-site recognition of many foods, condiments, fragrances and flavors, and petroleum waxes and a real-time quantitative prediction of their odor quality grades and many key component concentrations.

MASS SPECTROMETER
20230147319 · 2023-05-11 · ·

A door 4 includes a closing portion 41 that closes an opening 302 in a closed state, and a holding portion 42 that holds the closing portion 41 and is connected to a hinge portion 5. The closing portion 41 is connected to the holding portion 42 on the side opposite to the hinge portion 5 side, and is configured to be separable from the holding portion 42 on the hinge portion 5 side. In a case where the door 4 is rotated from an open state to a closed state, the closing portion 41 is configured to be in contact with a peripheral edge portion of the opening 302 on the side opposite to the hinge portion 5 side before the closing portion 41 comes into contact with a peripheral edge portion of the opening 302 on the hinge portion 5 side.

QUANTITATIVE ANALYSIS METHOD AND QUANTITATIVE ANALYSIS APPARATUS
20230146444 · 2023-05-11 · ·

One mode of the present invention is a quantitative analysis method of quantifying a target compound contained in a sample derived from an organism, including: a category selection step of receiving selection by a user of one category containing a target sample from among categories determined in advance for the sample; a preprocessing step of performing a predetermined preprocessing including derivatization on the target sample; a measurement execution step of executing GC/MS analysis on the preprocessed target sample based on analysis condition information provided from a database storing the analysis condition information for the GC/MS analysis and calibration curve information for quantification by a standard addition method for each category; and a quantitative processing step of performing quantitative processing based on data obtained in the measurement execution step using the calibration curve information corresponding to the selected category, the calibration curve information being provided by the database.

MULTIFUNCTIONAL MAGNETIC TAGS FOR MUD LOGGING
20230141819 · 2023-05-11 ·

Compositions and methods for determining the origin location of a subterranean sample are provided. Compositions include a nanoparticle tag including a superparamagnetic iron oxide core, an intermediate layer including a fluorescent dye, and a polymer shell. The nanoparticles can be synthesized by functionalizing a superparamagnetic iron oxide nanoparticle core and covalently bonding a fluorescent dye to the functionalized nanoparticle core. In some implementations, a polymer is covalently bonded to the functionalized, fluorescent superparamagnetic iron oxide nanoparticle core. The nanoparticle tag can be used to determine the origin location of a subterranean sample by mixing the nanoparticle tag into a fluid, flowing the fluid into a subterranean formation, recovering subterranean samples from the subterranean formation, and separating tagged samples from untagged samples using a magnet. The origin location of the subterranean sample can be determined by analyzing the fluorescent signal of the nanoparticle tag.

METHODS FOR QUANTIFICATION OF COMPOUNDS IN CULTIVARS OF Cannabis sp.
20230138563 · 2023-05-04 ·

The disclosure provides a method for analyzing compounds extracted from Cannabis. The method comprises extracting cannabinoids or terpenes from a sample using a C.sub.1-C.sub.4 alcohol or C.sub.5-C.sub.8 solvent as an extraction solvent to produce a supernatant, drying the supernatant to produce a dried extract, and dissolving the dried extract in a second C.sub.1-C.sub.4 alcohol or C.sub.5-C.sub.8 solvent, separating the cannabinoids or terpenes by gas chromatography using a capillary column with hydrogen as a carrier gas; and detecting the cannabinoids or terpenes using a mass spectrometer. The disclosure also provides a method of determining an effect of one or more Cannabis-derived compounds on intracellular calcium concentration in a cell using a microfluidic device.

INTEGRATED VIEWER FOR MULTIPLE MEASUREMENTS, AND PROGRAM

An integrated viewer for multiple measurements according to a first aspect includes: a storage unit that stores, for each of a plurality of types of analyzers, a type of a feature amount obtained from a measurement result of the analyzer; a display control unit that displays types of feature amounts stored in the storage unit on a display screen in a selectable manner; and a registration unit that names and registers a set of types of feature amounts selected by an operator among the types of the feature amounts. The display control unit displays, side by side on the display screen, a first display region in which the type of the feature amount is displayed in a tab for each type of the analyzers and a second display region in which the set of types of the feature amounts selected by the operator is displayed.

METHOD FOR DETERMINING THE PREGNANCY STATE OF AN ANIMAL
20230200964 · 2023-06-29 ·

Disclosed herein is a method for determining a pregnancy state of an animal. The method comprises detecting an amount of one or more biomarkers in a breath sample from the animal, the amount of the or each biomarker being indicative of a pregnancy state of the animal.

LOW THERMAL MASS GC MODULE

A system and method for performing field-portable GC/MS measurements for the rapid sampling and measurement of high temperature boiling semi-volatile organic compounds in environmental samples, wherein other column bundles have cold spots that may prevent high temperature boiling semi-volatile components from eluting the GC column, this new design may eliminate those cold spots on the GC column.