G01N33/0052

Real time ozone layer monitoring using ion mobility spectrometry
09910022 · 2018-03-06 · ·

The present invention provides a capability of Ion Mobility Spectrometry/Atmospheric Pressure Ionization Mass Spectrometry (IMS/MS) in the negative ion mode for Ozone detection and methods for ozone layer depletion monitoring in laboratory environment. Ammonium hydroxide vapors, as a dopant chemical, introduced to the inlet system of the IMS/MS interfaced with the reaction sphere enables ozone ionized to be O.sub.3.sup.. The data obtainable from proposed methods show how ozone is depleted and which compound affect the most for O.sub.3 destruction among the O.sub.3 depletion substances of Chloro Fluoro Carbons (CFCs), Hydro Fluoro Carbons (HFCs), Hydro Chloro Fluoro Carbons (HCFCs), Hydro Chloro Bromo Carbons (HCBCs), and Hydro Chloro lodo Carbons (HClCs). Based on the results obtainable, more likely the IMS alone system without coupling with the mass spectrometer (IMS/MS) will rather be selected to develop as a spatial real time ozone layer depletion monitor. Real time monitoring device of ozone concentration in ambient atmospheric conditions can also be developed with this technique.

Systems and methods for sanitizing pool and spa water

Systems and methods for sanitizing pool and spa water are provided. An electrolytic chlorinator is provided which includes a combined flow, temperature, and salt concentration sensor. The electrolytic chlorinator could include an acid tank for in-situ cleaning of the electrolytic chlorinator or acidification of pool/spa water where needed. A delayed polarity reversal technique is provided for de-scaling and managing passivation of the blades of an electrolytic chlorinator. The electrolytic chlorinator could include a sacrificial anode for protecting components of the chlorinator as well as other pool/spa components. The electrolytic chlorinator could include an integral, electrically-controlled acid generator, a brine tank for periodically superchlorinating and/or shocking pool/spa water, and/or a plurality of chemical tanks/feeds for periodically injecting chemicals into the chlorinator. A combined ultraviolet (UV)/Ozone and salt (electrolytic) chlorine generator is provided, as well as: filters having integral UV sanitizers; reflective linings for UV sanitization systems; means for injecting bubbles into pool/spa water; and a system for acquiring and analyzing samples of pool/spa water using an unmanned aircraft (drone).

Innovative and safe method to conduct high temperature halogenation of metallic alloys

The present invention discloses a method and system for conducting high temperature corrosion tests on metallic alloys without the need for extensive laboratory equipment and attendant safety measures through the use of a two-compartment ampoule where a vestibule connects these two compartments. A pre-selected mixture of salts is placed in one compartment in order to generate a specific partial pressure of halogen gas; and a metallic alloy is placed in the other compartment. The ampoule is then heated to a pre-determined temperature and held at this temperature for a pre-determined time period. A halogen gas of a specific partial pressure is thereby generated from the mixture of salts which comes into contact with the metallic alloy. Because the ampoule creates a sealed environment, the metallic alloy is under constant halogenation during the pre-determined time period. The metallic alloy is removed for examination when the pre-determined time period expires.

FUSE FOR DETECTING FAILURE OF GAS TRAP
20170089877 · 2017-03-30 ·

A gas detection fuse is provided, comprising a thin strip or sheet of a conductive material, such as a metal, connecting two electrodes for detecting a gas of interest. The metal is selected to be reactive with the gas of interest, and has a relatively large surface area, such that when the gas of interest contacts the metal, the electrical connection between the electrodes is broken (e.g., due to the metal losing physical integrity, or becoming non-conductive, as a result of the reaction with the gas). The gas of interest may be chlorine, and the conducting material may be tin. When the tin is exposed to chlorine the tin becomes oxidized to produce liquid tin tetrachloride, thus breaking the electrical connection.

ELECTROCHEMICAL GAS SENSOR

An electrochemical gas sensor (10) includes a housing (11) which has a number of electrodes (31, 32), i.e. at least one working electrode (31) and at least one counter electrode (32), in addition to a liquid electrolyte (60). At least one of said electrodes (31, 32) and/or the housing (11) are at least partially formed of an absorption agent composition. A method of detecting acid gases employs the electrochemical gas sensor (10).

Studies on Real Time Ozone Layer Depletion Monitoring using the Negative Ion Mode of Ion Mobility Spectrometry / Atmospheric Pressure Ionization Mass Spectrometry (NEG. MODE IMS/APIMS) in Upper and Lower Atmosphere
20170016868 · 2017-01-19 ·

The present invention provides a capability of Ion Mobility Spectrometry/Atmospheric Pressure Ionization Mass Spectrometry (IMS/MS) in the negative ion mode for Ozone detection and methods for ozone layer depletion monitoring in laboratory environment. Ammonium hydroxide vapors, as a dopant chemical, introduced to the inlet system of the IMS/MS interfaced with the reaction sphere enables ozone ionized to be O.sub.3.sup.. The data obtainable from proposed methods show how ozone is depleted and which compound affect the most for O.sub.3 destruction among the O.sub.3 depletion substances of Chloro Fluoro Carbons (CFCs), Hydro Fluoro Carbons (HFCs), Hydro Chloro Fluoro Carbons (HCFCs), Hydro Chloro Bromo Carbons (HCBCs), and Hydro Chloro lodo Carbons (HClCs). Based on the results obtainable, more likely the IMS alone system without coupling with the mass spectrometer (IMS/MS) will rather be selected to develop as a spatial real time ozone layer depletion monitor. Real time monitoring device of ozone concentration in ambient atmospheric conditions can also be developed with this technique.

Fuse for detecting failure of gas trap
12461082 · 2025-11-04 · ·

A gas detection fuse comprising a thin strip or sheet of a conductive material, such as a metal, connecting two electrodes for detecting a gas of interest. The metal is selected to be reactive with the gas of interest, and has a relatively large surface area, such that when the gas of interest contacts the metal, the electrical connection between the electrodes is broken (e.g., due to the metal losing physical integrity, or becoming non-conductive, as a result of the reaction with the gas). The gas of interest may be chlorine, and the conducting material may be tin. When the tin is exposed to chlorine the tin becomes oxidized to produce liquid tin tetrachloride, thus breaking the electrical connection.

SYSTEM AND METHOD FOR MEASURING A GAS CONCENTRATION IN ONE OR MORE REACTION CHAMBERS

A system for determining a concentration of a gas in one or more reaction chambers. The system comprises an energy source configured to provide a reaction energy to the one or more reaction chambers. A gas meter is capable of measuring a concentration of a gas in the one or more reaction chambers. A method for determining a concentration of a gaseous product in one or more reaction chambers is also disclosed, a test kit and a reaction chamber are also disclosed.

NOVEL TECHNIQUE TO QUANTIFY GASEOUS REACTIVE CHLORINE SPECIES BY LIQUID ION CHROMATOGRAPHY

An apparatus useful for the collection (and optionally measurement of) of an amount of a first fluid, including a vial comprising an opening and a septum covering the opening. The septum is pierced by a needle configured for coupling to a source suspected of outputting the fluid. The vial further comprises a second fluid capable of combining with (e.g., dissolving) the first fluid (e.g., gas) introduced into the vial via the needle, e.g., to form a solution. The apparatus further includes an incubator capable of chilling the vial and its contents to between 10 C. and 5 C. when the vial is positioned within the incubator such that the septum faces the ground or a bottom of the incubator. A liquid ion chromatography instrument can then be used to quantify the amount of moiety of the substance of the first fluid.

System, apparatus and method for landfill gas sensing

An apparatus including: a housing configured for installation in a landfill; a differential pressure sensor and at least one gas sensor in the housing; and a first valve configured to control landfill gas (LFG) flow to the at least one gas sensor, wherein the first valve is configured to open when the differential pressure sensor detects a selected pressure difference or pressure difference change between the atmospheric air pressure and the LFG pressure.