H01M10/54

METHOD FOR REUSING ACTIVE MATERIAL BY USING POSITIVE ELECTRODE SCRAP
20230041348 · 2023-02-09 ·

There is provided a method for collecting and reusing an active material from positive electrode scrap. The method for reusing a positive electrode active material of the present disclosure includes (a) thermally treating positive electrode scrap comprising an active material layer on a current collector in air for thermal decomposition of a binder and a conductive material in the active material layer, to separate the current collector from the active material layer, and collecting an active material in the active material layer, (b-1) washing the active material collected from the step (a) with a lithium compound solution which is basic in an aqueous solution, (b-2) mixing the active material washed from the step (b-1) with a lithium precursor aqueous solution and spray drying, and (c) annealing the active material spray dried from the step (b-2) to obtain a reusable active material.

METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
20230045467 · 2023-02-09 ·

There is provided a method for collecting and reusing an active material from positive electrode scrap. The positive electrode active material reuse method of the present disclosure includes (a) thermally treating positive electrode scrap comprising an active material layer on a current collector in air for thermal decomposition of a binder and a conductive material in the active material layer, to separate the current collector from the active material layer, and collecting an active material in the active material layer, (b) washing the collected active material using a lithium precursor aqueous solution which is basic in an aqueous solution and drying, and (c) annealing the washed active material to obtain a reusable active material.

METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
20230045467 · 2023-02-09 ·

There is provided a method for collecting and reusing an active material from positive electrode scrap. The positive electrode active material reuse method of the present disclosure includes (a) thermally treating positive electrode scrap comprising an active material layer on a current collector in air for thermal decomposition of a binder and a conductive material in the active material layer, to separate the current collector from the active material layer, and collecting an active material in the active material layer, (b) washing the collected active material using a lithium precursor aqueous solution which is basic in an aqueous solution and drying, and (c) annealing the washed active material to obtain a reusable active material.

System and method for separating battery components
11557813 · 2023-01-17 · ·

A system and method for separating battery components provides for the separation of batteries into their individual layers of anodes, cathodes, first polymer separator layers, and second polymer separator layers. A battery casing of a battery is cut to uncover a battery cell core, which is then washed to remove an electrolyte therefrom. An outer wrapping layer of the washed battery cell core is cut to form an open loose end, and the open loose end is engaged by first and second rollers to unroll a laminate therefrom. The laminate includes a cathode layer, an anode layer, a first polymer separator layer, and a second polymer separator layer. The laminate is then separated into the cathode layer, the anode layer, the first polymer separator layer, and the second polymer separator layer with the first roller, the second roller, a third roller, and a fourth roller. Each layer is then collected.

System and method for separating battery components
11557813 · 2023-01-17 · ·

A system and method for separating battery components provides for the separation of batteries into their individual layers of anodes, cathodes, first polymer separator layers, and second polymer separator layers. A battery casing of a battery is cut to uncover a battery cell core, which is then washed to remove an electrolyte therefrom. An outer wrapping layer of the washed battery cell core is cut to form an open loose end, and the open loose end is engaged by first and second rollers to unroll a laminate therefrom. The laminate includes a cathode layer, an anode layer, a first polymer separator layer, and a second polymer separator layer. The laminate is then separated into the cathode layer, the anode layer, the first polymer separator layer, and the second polymer separator layer with the first roller, the second roller, a third roller, and a fourth roller. Each layer is then collected.

Recycling Li-ion batteries using green chemicals and processes

A process for extracting, recovering and recycling metals and materials from spent lithium ion batteries (LIB) that comprises the contacting battery waste products with a deep eutectic solvent, and leaching the metal from the battery waste product and extracting the metal into the deep eutectic solvent with heat and agitation. After the leaching and extracting, the process further includes recovering the dissolved metals ions from the deep eutectic solvent solution, followed by a step of regeneration of cathode materials.

Recycling Li-ion batteries using green chemicals and processes

A process for extracting, recovering and recycling metals and materials from spent lithium ion batteries (LIB) that comprises the contacting battery waste products with a deep eutectic solvent, and leaching the metal from the battery waste product and extracting the metal into the deep eutectic solvent with heat and agitation. After the leaching and extracting, the process further includes recovering the dissolved metals ions from the deep eutectic solvent solution, followed by a step of regeneration of cathode materials.

METHOD FOR RECYCLING LITHIUM-ION BATTERY
20180013181 · 2018-01-11 · ·

Provided herein is a method for recycling lithium-ion batteries in a polar solvent such as an aqueous media or water. The method disclosed herein isolates a mixture of anode and cathode materials from waste lithium-ion batteries. The separated electrode materials can easily be collected with high recovery rate, providing a rapid, efficient and low-cost method for recycling electrode materials from waste lithium-ion batteries.

METHOD FOR RECYCLING LITHIUM-ION BATTERY
20180013181 · 2018-01-11 · ·

Provided herein is a method for recycling lithium-ion batteries in a polar solvent such as an aqueous media or water. The method disclosed herein isolates a mixture of anode and cathode materials from waste lithium-ion batteries. The separated electrode materials can easily be collected with high recovery rate, providing a rapid, efficient and low-cost method for recycling electrode materials from waste lithium-ion batteries.

Recycling of cobalt and nickel from lithium-ion batteries

A process for recovering a nickel cobalt manganese hydroxide from recycled lithium-ion battery (LIB) material such as black mass, black powder, filter cake, or the like. The recycled LIB material is mixed with water and either sulfuric acid or hydrochloric acid at a pH less than 2. Cobalt, nickel, and manganese oxides from the recycled lithium-ion battery material dissolve into the acidic water with the reductive assistance of gaseous sulfur dioxide. Anode carbon is filtered from the acidic water, leaving the dissolved cobalt, nickel, and manganese oxides in a filtrate. The filtrate is mixed with aqueous sodium hydroxide at a pH greater than 8. Nickel cobalt manganese hydroxide precipitates from the filtrate. The nickel cobalt manganese hydroxide is filtered from the filtrate and dried. The filtrate may be treated ammonium fluoride or ammonium bifluoride to precipitate lithium fluoride from the filtrate. The composition ratio of nickel to cobalt to manganese in the acid filtrate may be adjusted to a desired ratio. The anode carbon is recovered and purified for reuse.