A liquor distillation system, comprising one or more channeled loops fluidly couplable to a boiler and a condenser, the condenser adapted to condense alcoholic vapors from a heated liquor wherein the one more channeled loops include an entrance point, an exit point, a split point, and a recombination point such that the heated liquor enters the one or more channeled loops from the entrance point, to the split point where the heated liquor is split into two separate opposite subchannels and recombined at the recombination point; one or more connection pipes adapted to connect the one or more channeled loops to another channeled ring; one or more drain valves; and a liquor outlet.

A distillation head for distilling a distillate from a vaporous distilland. The distillation head including a headspace chamber within a condenser surface. An inlet port having an extended portion below and to but not into the headspace, to receive the vaporous distilland and pass it into the headspace. A collection surface below the headspace to collect the distillate. And an outlet port, to receive the distillate from the collection surface and pass it out of the distillation head.

The invention refers to a distillation apparatus (100) for extraction of volatile components from biological material (50), especially from plants, comprising a housing (10) defining a sample chamber (S), a drum (30) arranged in the sample chamber (S), the drum (30) defining a receiving chamber (R) for receiving the biological material (50), and at least one microwave generator (70) for irradiating the biological material (50) with microwave radiation when received in the drum (30); wherein the drum (30) is rotatably arranged in the sample chamber (S) about a rotation axis (H) which is oriented substantially horizontally.

A distillation head for distilling a distillate from a vaporous distilland. The distillation head including a headspace chamber within a condenser surface. An inlet port having an extended portion below and to but not into the headspace, to receive the vaporous distilland and pass it into the headspace. A collection surface below the headspace to collect the distillate. And an outlet port, to receive the distillate from the collection surface and pass it out of the distillation head.

The present disclosure relates to the determination of analytes in a sample using chromatography. The present disclosure provides methods of separating an analyte from a sample. A mobile phase is flowed through a chromatography column. The mobile phase includes about 0.005% (v/v) to about 2.50% (v/v) difluoroacetic acid and less than about 100 ppb of any individual impurity, especially metal impurities. A sample including the analyte is injected into the mobile phase. The analyte is separated from the sample.

The present disclosure relates to the determination of analytes in a sample using chromatography. The present disclosure provides methods of separating an analyte from a sample. A mobile phase is flowed through a chromatography column. The mobile phase includes about 0.005% (v/v) to about 2.50% (v/v) difluoroacetic acid and less than about 100 ppb of any individual impurity, especially metal impurities. A sample including the analyte is injected into the mobile phase. The analyte is separated from the sample.

A distillation column including a plurality of alternating plates and spacers stacked in a z-direction is provided. The plates include a respective liquid channeling network on a top surface thereof, a respective vapor opening, and a respective descending ramp. The respective descending ramps abut a respective liquid feed location of the plate immediately below to form a continuous liquid channeling network. The respective vapor openings of adjacent plates are located on opposite sides of the distillation column and form a continuous S-shaped vapor channel defined by the plurality of alternating plates and spacers, and the respective vapor openings. Systems including such distillation columns and processes of distilling a fluid mixture are also provided.

A distillation column including a plurality of alternating plates and spacers stacked in a z-direction is provided. The plates include a respective liquid channeling network on a top surface thereof, a respective vapor opening, and a respective descending ramp. The respective descending ramps abut a respective liquid feed location of the plate immediately below to form a continuous liquid channeling network. The respective vapor openings of adjacent plates are located on opposite sides of the distillation column and form a continuous S-shaped vapor channel defined by the plurality of alternating plates and spacers, and the respective vapor openings. Systems including such distillation columns and processes of distilling a fluid mixture are also provided.

A remediation plant for remediating drilling mud, cuttings, and fluids. The preferred plant includes a reboiler that is adapted to provide heat to the drilling mud, cuttings, and fluid, a mud drum that is operatively connected to the reboiler, a distillation column that is operatively connected to the reboiler, a heat exchanger that is operatively connected to the reboiler, a condenser that is operatively connected to the distillation column, a condenser tank that is operatively connected to the condenser, an oil-water separator that is operatively connected to the condenser tank, and a pump that is operatively connected to the oil-water separator. The preferred remediation plant is adapted to remove synthetic drilling fluid from drilling mud, cuttings, and fluids. A method for remediating drilling mud, cuttings, and fluid.

A remediation plant for remediating drilling mud, cuttings, and fluids. The preferred plant includes a reboiler that is adapted to provide heat to the drilling mud, cuttings, and fluid, a mud drum that is operatively connected to the reboiler, a distillation column that is operatively connected to the reboiler, a heat exchanger that is operatively connected to the reboiler, a condenser that is operatively connected to the distillation column, a condenser tank that is operatively connected to the condenser, an oil-water separator that is operatively connected to the condenser tank, and a pump that is operatively connected to the oil-water separator. The preferred remediation plant is adapted to remove synthetic drilling fluid from drilling mud, cuttings, and fluids. A method for remediating drilling mud, cuttings, and fluid.