B01D3/34

Multi-Stage Device and Process for Production of a Low Sulfur Heavy Marine Fuel Oil

A multi-stage process for the production of an ISO 8217 compliant Product Heavy Marine Fuel Oil from ISO 8217 compliant Feedstock Heavy Marine Fuel Oil involving a Reaction System composed of one or more reactor vessels selected from a group reactor wherein said one or more reactor vessels contains one or more reaction sections configured to promote the transformation of the Feedstock Heavy Marine Fuel Oil to the Product Heavy Marine Fuel Oil. The Product Heavy Marine Fuel Oil has a Environmental Contaminate level has a maximum sulfur content (ISO 14596 or ISO 8754) between the range of 0.05 mass % to 1.0 mass. A process plant for conducting the process for conducting the process is disclosed that can utilize a modular reactor vessel.

System and method to reboil a process stream in a distillation system by mixing the stream with a heating medium

A system and method to reboil a process or feed water stream in a distillation system does so in a liquid pool zone of a vessel as the stream is removed from a distillation column and comes into contact with a heating medium that is immiscible with and less volatile than the process stream. To keep the pool hot, the heating medium can be recirculated through a heater of a pump-around loop or a heater can be placed in the liquid pool. As the process stream is partially vaporized, any solids present in the process stream together with the unvaporized process or feed water stream move into the heating medium. These solids and unvaporized liquids may be further removed from the heating medium in the pool or in the pump-around loop. The vaporized stream is returned to the distillation column.

System and method to reboil a process stream in a distillation system by mixing the stream with a heating medium

A system and method to reboil a process or feed water stream in a distillation system does so in a liquid pool zone of a vessel as the stream is removed from a distillation column and comes into contact with a heating medium that is immiscible with and less volatile than the process stream. To keep the pool hot, the heating medium can be recirculated through a heater of a pump-around loop or a heater can be placed in the liquid pool. As the process stream is partially vaporized, any solids present in the process stream together with the unvaporized process or feed water stream move into the heating medium. These solids and unvaporized liquids may be further removed from the heating medium in the pool or in the pump-around loop. The vaporized stream is returned to the distillation column.

Process for recovering close boiling products

The disclosure is directed to a method for recovering products from a fermentation broth. The disclosure relates to the use of extractive distillation and/or dehydration to recover products which have close boiling points, such as ethanol and isopropanol, from a fermentation broth. In an embodiment, the recovery of product is completed in a manner that minimizes stress on the microbial biomass, such that it remains viable, at least in part, and may be recycled and reused in the fermentation process, which may result in increased efficiency in the fermentation process. The extractive distillation vessel and/or dehydration reactor may be used downstream of a distillation vessel. To minimize stress on the microbial biomass the distillation vessel may be under vacuum. The extractive distillation vessel may be used alongside a separation vessel such that the separation vessel is capable of recycling extractive distillation agent.

PRODUCTION APPARATUS AND PRODUCTION METHOD OF SUCROSE-6-ESTER

A production apparatus and a production method of sucrose-6-ester are provided. The production apparatus includes a tank, a rotary distillation device, and a condensation device, the tank includes a separation chamber and a reaction chamber; the condensation device is sheathed inside the rotary distillation device, and the rotary distillation device is slidably connected in the separation chamber; a turntable of the rotary distillation device is fixed on a top surface of a drum, and a first heating device is provided on an outer wall of the turntable; the condensation device includes a condenser pipe, a water receiving plate, and a condensate water box that are connected sequentially from top to bottom; the condensation device is sheathed inside the drum of the rotary distillation device in a non-contact manner, and the condenser pipe is arranged to penetrate through the turntable and contacts a top surface of the tank.

PRODUCTION APPARATUS AND PRODUCTION METHOD OF SUCROSE-6-ESTER

A production apparatus and a production method of sucrose-6-ester are provided. The production apparatus includes a tank, a rotary distillation device, and a condensation device, the tank includes a separation chamber and a reaction chamber; the condensation device is sheathed inside the rotary distillation device, and the rotary distillation device is slidably connected in the separation chamber; a turntable of the rotary distillation device is fixed on a top surface of a drum, and a first heating device is provided on an outer wall of the turntable; the condensation device includes a condenser pipe, a water receiving plate, and a condensate water box that are connected sequentially from top to bottom; the condensation device is sheathed inside the drum of the rotary distillation device in a non-contact manner, and the condenser pipe is arranged to penetrate through the turntable and contacts a top surface of the tank.

Process water distillation plant and method for operating a process water distillation plant
20230398467 · 2023-12-14 ·

A process water distillation system (10) comprises an evaporator (18), a condenser (34), a compressor (28) configured to generate a desired pressure in at least a region of the process water distillation system (10) and to convey steam from the evaporator (18) to the condenser (34) during operation of the process water distillation system (10), an inert gas source (40) configured to supply inert gas to the process water distillation system (10), and a control device (48) configured to control the supply of inert gas from the inert gas source (40) to the process water distillation system (10) in such a way that, at least in certain operating phases of the process water distillation system (10), an oxygen concentration in the process water distillation system (10) does not exceed a permissible maximum value.

Method and apparatus for extracting plant oils using ethanol water
11040295 · 2021-06-22 ·

The invention provides a method and apparatus for continuous extraction of plant oils from plant tissue using an advantageous azeotrope of ethanol and water and employing the differing solubility of plant oils in ethanol and water to drive formation of a non-toxic oil tincture.

Method for obtaining pure 1,3-butadiene
11034631 · 2021-06-15 · ·

Process for isolating pure 1,3-butadiene from a crude C.sub.4 fraction by extractive distillation using a selective solvent, wherein (a) the crude C.sub.4 fraction is introduced into a predistillation column, a first low boiler fraction comprising C.sub.3-hydrocarbons is taken off as overhead stream, a gaseous C.sub.4 fraction is taken off as side stream and a first high boiler fraction is taken off as bottom stream, (b) the gaseous C.sub.4 fraction is brought into contact with a selective solvent in at least one extraction column, giving an overhead fraction comprising butanes and butenes and a bottom fraction comprising 1,3-butadiene and selective solvent, (c) crude 1,3-butadiene is desorbed from the bottom fraction in at least one stripping column, with a stripped selective solvent being obtained and the stripped selective solvent being recirculated to the extraction column, and (d) at least part of the crude 1-3-butadiene is fed to a pure distillation column and a second high boiler fraction is separated off and a gaseous purge stream is taken off. Gaseous purge streams from the columns which are necessary in order to keep the concentration of molecular oxygen below a predetermined concentration limit are consolidated with output streams which are in any case provided for discharging other components in the process. The recirculation of the second high boiler fraction to a lower section of the predistillation column creates a further degree of freedom in operation of the pure distillation column.

Process for removing volatile contaminants

A process for cleansing a liquid of volatile contaminants can be accomplished by cross flowing a liquid through a contactor vessel. As the liquid cross flows through the horizontal contactor vessel, a radial flow pattern is induced in the liquid and the liquid is contacted with a cleansing gas. As the liquid moves through the contactor vessel, contaminants enter the cleansing cross current gas percolating through the liquid. The cross current gas may then be collected and cleansed of the contaminants it collected. The cleaned cleansing gas may then be recycled back into the contactor vessel.