The invention relates to a process for preparing dimeric and/or trimeric silanes by conversion of monosilane in a plasma and to a plant for performance of the process.

The invention relates to a process for preparing dimeric and/or trimeric silanes by conversion of monosilane in a plasma and to a plant for performance of the process.

Methods for generating a purified catalyst are provided. The method includes performing a reaction in a reaction vessel to generate a liquid catalyst and reaction products, purging the reaction products using an inert gas to form a purged catalyst, freezing the purged catalyst in the reaction vessel, and applying a vacuum to the reaction vessel while the purged catalyst thaws, wherein the vacuum removes residual reaction products to form a purified catalyst. Systems for generating a purified catalyst and a purified catalyst are also provided.

Disclosed is a method for the continuous impregnation of wood elements, such as wood chips. The method comprises the subsequent steps of subjecting the wood elements to vacuum, to contact with acetylation fluid, and to impregnation pressure. Preferably, the process is conducted in a plant having conveyors, such as transportation screws, in suitable positions between the zones in which the subsequent process steps are conducted. The impregnation method is used in connection with the acetylation of the wood elements, and preferably is followed by a continuous acetylation process conducted in an acetylation reaction zone downstream of the zone where the impregnation is conducted.

Disclosed are methods and apparatuses for producing heavy water. In one embodiment, a catalyst is treated with high purity air or a mixture of gaseous nitrogen and oxygen with gaseous deuterium all together flowing over the catalyst to produce the heavy water. In an alternate embodiment, the deuterium is combusted to form the heavy water. In an alternate embodiment, gaseous deuterium and gaseous oxygen is flowed into a fuel cell to produce the heavy water. In various embodiments, the deuterium may be produced by a thermal decomposition and distillation process that involves heating solid lithium deuteride to form liquid lithium deuteride and then extracting the gaseous deuterium from the liquid lithium deuteride.

A vacuum chamber (2) for a direct air capture process and enclosing an interior space (13) for housing an adsorber structure (1) is given comprising a contiguous circumferential wall structure (115) along an axis (15), which circumferential wall structure (115) in an axial direction is closed by an inlet and an outlet axial wall (116), respectively, both axial walls (116) comprising at least one closing stainless steel lid (6) allowing for, in an open position, gas to be circulated through the vacuum chamber (2) for passing an adsorber structure (1), and, in a closed position, to close the interior space (13) and to allow evacuation of the interior space (13) down to pressure of 500 mbar.sub.abs or less.

This invention relates to an apparatus and method for separating a solvent in a metallocene catalyst-based solution polymerization process for preparing a polyolefin, suitable for use in removing a solvent from a reaction mixture resulting from a polymerization step during a solution polymerization process for preparing a polyolefin polymer using a metallocene catalyst, wherein volatile matter including a solvent and an unreacted monomer is primarily removed from the reaction mixture using a flash drum, after which residual volatile matter including the solvent, which is left behind in the reaction mixture after the primary removal process, is secondarily removed in a high vacuum using a thin-film evaporator. The polymer thus obtained has a volatile matter content of 100 ppm or less and is thus an environmentally friendly product.

The present invention provides a highly effective method of removal of gases from the chemical reactor (01) by use of a suction unit employed near the inlet, outlet or both ends of the chemical reactor. The suction of entrapped air from the reaction mixture helps avoid fluctuation in the temperature or pressure requirement or formation of other by-products in the reaction mixture.

The present invention relates to a method for treating waste comprising at least one organic phase, said method comprising the following consecutive steps: a) preparation of an oil-in-water emulsion with controlled TOD using waste to be treated comprising at least one organic phase, by mixing said waste with an aqueous phase in a mixer, preferably with high shear; b) possible adjustment of the TOD of the emulsion obtained in step a); and c) hydrothermal oxidation, under subcritical or supercritical starting conditions, of the emulsion thus obtained. The present invention also relates to a facility suitable for implementing the method for treating waste comprising at least one organic phase according to the invention.

Systems for manufacturing bulked continuous carpet filament from polymer, where the systems are configured for: (1) passing polymer flakes through a crystalliers; (2) melting the polymer to create a first single stream of polymer melt; (3) separating the first single stream of polymer melt into multiple streams of polymer melt; (4) exposing the multiple streams of polymer melt to a pressure of between about 0 millibars and about 25 millibars in a chamber; (5) recombining the multiple streams of polymer melt into a second single stream of polymer melt; and (6) providing the second single stream of polymer melt to one or more spinning machines that are configured to form the second single stream of polymer melt into bulked continuous carpet filament.