B01J3/006

HIGH-LOAD VACUUM CHAMBER MOTION FEEDTHROUGH SYSTEM AND METHODS

A feedthrough for use in a vacuum chamber is provided and includes a hollow tube having a length, an inner circumference, and a first recess located within the inner circumference. The feedthrough also includes a first O-ring captured by the first recess within the hollow tube. The feedthrough further includes a rod extending through an entirety of the length of the hollow tube. An outer circumference of the rod is configured to contact an entirety of an inner circumference of the first O-ring, and a vacuum fitting is fixedly secured to the hollow tube.

Pressure-regulated multi-reactor system
10913048 · 2021-02-09 · ·

A device and a method are provided for reacting a starting material in at least two reactors connected to each other, including the reacting of the starting material in a first reactor to a first product, removing the first product from the first reactor using a jet pump, wherein a negative pressure zone of the jet pump is operationally connected to the first reactor, so that the first product of the first reactor moves through the negative pressure zone in a propulsion jet of a propulsion medium of the jet pump, conducting the propulsion medium having the first product into a second reactor, wherein the first product is allowed to react into a second product, separating the second product from the propulsion medium and discharging the separated second product.

Method for manufacturing elementary metal including metal precursor pressurization dosing operation

A pressurization type method for manufacturing elementary metal may include a metal precursor gas pressurization dosing operation of, in a state where an outlet of a chamber having a substrate is closed, increasing a pressure in the chamber by providing a metal precursor gas consisting of metal precursors, thereby adsorbing the metal precursors onto the substrate, a main purging operation of purging a gas after the metal precursor gas pressurization dosing operation, a reaction gas dosing operation of providing a reaction gas to reduce the metal precursors adsorbed on the substrate to elementary metal, after the main purging operation, and a main purging operation of purging a gas after the reaction gas dosing operation.

INTEGRATED DEVICE FOR PREPARING MAGNESIUM HYDRIDE POWDER AND METHOD FOR PREPARING MAGNESIUM HYDRIDE POWDER
20210046550 · 2021-02-18 ·

Provided is an integrated device for preparing magnesium hydride powder and a method for preparing magnesium hydride powder. The device comprises a heating chamber for heating a magnesium-based metal material to produce metal droplets; a powder-making chamber comprising an atomizing means used for atomizing the metal droplets which are then cooled to form a metal powder; and a reaction chamber used for performing a hydrogenation reaction on the metal powder to form the magnesium hydride powder. The device is an integrated structure monolithic with a simple structure and a convenient operation; and the entire process of preparing magnesium hydride powder can be completed in this single device and can realize automated control. The preparation method is simple and easy to operate and produces a product that has a moderate size, uniform particles, and excellent performance.

METHOD FOR PREPARING CALCIUM OXIDE USING A MULTISTAGE SUSPENSION PREHEATER KILN
20210078869 · 2021-03-18 ·

The disclosure discloses a method for preparing calcium oxide using multistage suspension preheater kiln. The steps of the method are: (1) the limestone powder is fed to the multistage suspension preheater kiln for preheating to 800 C. to 900 C.; (2) A preheated material is fed to a decomposition furnace, and calcined at 900 C. to 1100 C. for 25 s to 35 s; (3) A calcined material is fed to a rotary kiln, and calcined at 1100 C. to 1300 C. for 25 to 35 minutes, and finally cooled to obtain calcium oxide.

Preparation method of trifluoroamine oxide

The present invention relates to a preparation method of trifluoroamine oxide comprising the steps of producing an intermediate product by reacting nitrogen trifluoride and nitrous oxide in the presence of a reaction catalyst; and producing trifluoroamine oxide by reacting the intermediate product with sodium fluoride in vacuum condition up to 100 mmHg.

High-load vacuum chamber motion feedthrough systems and methods

A feedthrough for use in a vacuum chamber including a hollow tube, a first O-ring, and rod, and a vacuum fitting. The hollow tube having a first recess located along an entirety of an inner circumference. The first O-ring captured by the first recess. The rod carried by the hollow tube wherein an outer circumference of the rod is configured to contact an entirety of an inner circumference of the first O-ring. The vacuum fitting fixedly secured to the hollow tube.

PRODUCTION METHODS FOR IRON FULVATE SOLUTION, IRON HYDROXIDE FULVATE SOLUTION AND POLYSILICA-IRON FULVATE SOLUTION
20210070794 · 2021-03-11 ·

An iron fulvate solution production method capable of producing an iron fulvate solution efficiently within a short period of time is provided. The method comprises: preparing a processing apparatus which comprises: a hermetic container internally having a closeable processing space; a steam jetting device operable to jet high-temperature and high-pressure steam into the hermetic container; a supply section for supplying a raw material into the hermetic container; and a discharge section for discharging, to the outside, a processed liquid produced through processing of the raw material by the steam; inputting a raw material from the supply section into the processing space of the hermetic container of the processing apparatus, wherein the raw material comprises a woody plant material (and/or a herbaceous plant material) and an iron material, as main sub-raw materials; subjecting the raw material to a subcritical water reaction processing, under stirring, while introducing steam having a temperature of 120 to 250 C. and a pressure of 5 to 35 atm for a woody plant material, or steam having a temperature of 100 to 200 C. and a pressure of 2 to 25 atm for a herbaceous plant material, into the processing space in which the raw material is input, to obtain a mixed solution containing iron fulvate; and separating the iron fulvate from the obtained mixed solution to take out an iron fulvate solution.

Method and Apparatus for Curing Plant-Based Extracts

Equipment and processes for curing and decarboxylating botanical oils, and in particular oils such as cannabidiol (CBD) and tetrahydrocannabinol (THC) from plants of the genus Cannabis (including both THC-lacking industrial hemp and THC-bearing varieties) are described. Lower temperatures, extended cure cycles and inert-gas processing improve product quality and reduce undesired oxidation, resulting in clear, homogenous oils with less tendency to crystallize.

Method for cooling and detoxifying biomass
20210207185 · 2021-07-08 ·

The present invention relates to an improved method and device for treating biomass in which thermally treated biomass is discharged from a pressurized reactor and introduced into a blow tank, wherein the absolute pressure in the blow tank is maintained below atmospheric pressure. The slurry of biomass separated in the blow tank is then enzymatically treated.