B01J13/0095

Methods and systems for the synthesis of nanoparticles including strained nanoparticles
10544046 · 2020-01-28 · ·

A method for synthesizing nanoparticles includes aerosolizing a precursor solution in the presence of a flowing carrier gas to yield a reactant stream, the precursor solution comprising a volatile solvent and a nanoparticle precursor. The method further includes heating the reactant stream to a temperature above a boiling point of the volatile solvent to form a product stream comprising a plurality of nanoparticles, cooling the product stream, and passing the product stream through a collection liquid to collect the nanoparticles from the product stream.

Process for the hydrophobization of porous silica

A process for the hydrophobization of a porous silica based compound involves the steps of providing a composition (I) containing a porous silica based compound, treating the composition (I) with a composition (II) containing hexamethyldisiloxane or its hydrolyzed form, and removing the treated silica based compound. The porous silica based compound obtained by the process is useful. A porous silica based compound obtained or obtainable by the process can be used for medical and pharmaceutical applications, as adsorbents, for cosmetic applications, as an additive for food, as a catalyst support, for the preparation of sensors, or for thermal insulation.

Nanoparticulate-aerosol generator and method for continuously generating aerosols, associated with said generator

The object of the present invention relates to a nanoparticulate aerosol generator comprising a compressed gas reservoir (1) connected to a nanoparticulate material receptacle (2) through an operational valve (8), wherein said receptacle (2) comprises an outlet hole (3) for the aerosol. Advantageously, the outlet of said nanoparticulate material receptacle (2) is connected to or inserted into a pressurized aerosol distribution chamber (4) equipped with a hole (9) for the exit of said aerosol out of the chamber (4). The invention provides the possibility of using different types of nanoparticles with sizes less than 100 nanometers continuously over time during long production periods of more than three hours. The invention also relates to a method for continuously generating nanoparticulate aerosols associated with the mentioned generator.

DEVICE FOR AEROSOL GENERATION AND USE OF A DEVICE FOR AEROSOL GENERATION

The invention relates to devices for aerosol generation comprising a container holding a liquid, an aerosol generator having a supply container holding the liquid, and an apparatus for conditioning the aerosol of the aerosol generator, said apparatus having a collection container for liquid and an outlet for the aerosol, in a series connection, wherein the aerosol generator is connected to a pressurized gas generator. The invention also relates to uses of such devices. Said devices and uses are characterized in particular by interruption-free operation. For this purpose, the collection container is connected to the aerosol generator via a first non-return valve in the passage direction and via a first jet pump, wherein the opening pressure of the first non-return valve is smaller than the pressure that can be achieved by the first jet pump. Furthermore, the container is connected to the aerosol generator via a second non-return valve in the passage direction and via a second jet pump, wherein the opening pressure of the second non-return valve is greater than the pressure difference between the supply container of the aerosol generator and the surroundings of the device for aerosol generation and smaller than the pressure that can be achieved by the second jet pump.

NANOPARTICULATE-AEROSOL GENERATOR AND METHOD FOR CONTINUOUSLY GENERATING AEROSOLS, ASSOCIATED WITH SAID GENERATOR

The object of the present invention relates to a nanoparticulate aerosol generator comprising a compressed gas reservoir (1) connected to a nanoparticulate material receptacle (2) through an operational valve (8), wherein said receptacle (2) comprises an outlet hole (3) for the aerosol. Advantageously, the outlet of said nanoparticulate material receptacle (2) is connected to or inserted into a pressurized aerosol distribution chamber (4) equipped with a hole (9) for the exit of said aerosol out of the chamber (4). The invention provides the possibility of using different types of nanoparticles with sizes less than 100 nanometers continuously over time during long production periods of more than three hours. The invention also relates to a method for continuously generating nanoparticulate aerosols associated with the mentioned generator.

Central fed roller for filament extension atomizer

A roller has an outer cylindrical surface having an array of holes, a central feed channel inside the roller, and vanes connecting the channel to the holes, forming a path for liquid between the channel and the holes. An atomization system having a fluid reservoir; a pair of rollers, at least one of the rollers having: a central feed channel, the channel fluidically connected to the fluid reservoir, an array of holes on a surface of the roller, and vanes connecting the channels to the holes, a nip formed between the rollers, and a receiving surface positioned to receive droplets formed when liquid exits the holes, stretches between the rollers as they counterrotate to form filaments and the filaments break into droplets.

Dryer for preparation of dry nanoparticles

A system for producing dry nanoparticles from a liquid includes a closed tubing system which incorporates a mister, heater and an electrostatic collector therein. The system is able to produce dry nanoparticles from liquid-suspensions and from solvent solutions.

METHODS AND SYSTEMS FOR COLLECTING DROPLETS OF STRAIN HARDENING VISCOELASTIC FLUIDS IN A SPRAY

An aerosol creation system can include a pair of counter-rotating rollers configured to be positioned adjacent each other and define a nip between each other, a fluid source configured to provide a fluid to the nip, a driving element configured to drive the pair of counter-rotating rollers to rotate in counter rotation with respect to each other and cause the fluid to be drawn through the nip, and a collection shell configured to be positioned substantially around the pair of counter-rotating rollers, the collection shell having a nozzle configured to allow passage of the fluid from the nip.

ARCHITECTED THREE DIMENSIONAL GRAPHENE VIA ADDITIVE MANUFACTURING

Disclosed here is a method for making an architected three-dimensional aerogel, comprising providing a photoresin comprising a solvent, a photoinitiator, a crosslinkable polymer precursor, and a precursor for graphene, metal oxide or metal chalcogenide; curing the photoresin using projection microstereolithography layer-by-layer to produce a wet gel having a pre-designed three dimensional structure; drying the wet gel to produce a dry gel; and pyrolyzing the dry gel to produce an architected three-dimensional aerogel. Also disclosure is a photoresin for projection microstereolithography, comprising a solvent, a photoinitiator, a crosslinkable polymer precursor, and graphene oxide.

Passive Filter for Aerosol Printing

A passive filter for an aerosol printing system. The passive filter includes a housing having a fluid inlet port at a first end and a fluid outlet port at a second end, the fluid inlet and outlet ports being coaxial. A chamber is disposed within the housing and has a ceiling, a base, at least one wall between the ceiling and the base, a chamber entrance in the ceiling, and a chamber exit. The chamber entrance and exit being coaxial to the fluid inlet and outlet ports. The chamber exit is disposed within chamber between the chamber entrance and the base and defining a circumferential trough about the chamber exit.