B01J19/0053

New Industrial Process for Manufacturing of Perfluoro (Methyl Vinyl Ether)(PFMVE) and of 1,1,2,2-Tetrafluoro-1-(Trifluoromethoxy)ethane (TFTFME)
20220185756 · 2022-06-16 · ·

The invention relates to a new industrial process for manufacturing of perfluoro(methylvinylether) (PFMVE), and of 1,1,2,2-tetrafluoro-1-(trifluoromethoxy)ethane (TFTFME) (E 227), involving reactions in liquid phase and performing reactions, for example, in a (closed) column reactor or in a microreactor, respectively. The invention also relates to a new industrial process for manufacturing of perfluoro(methyl vinyl ether) (PFMVE) by HF-elimination from the compound 1,1,2,2-tetrafluoro-1-(trifluoromethoxy)ethane (TFTFME) (E 227). The invention also relates to a new industrial process for manufacturing of the compound 1,1,2,2-tetrafluoro-1-(trifluoromethoxy)ethane (TFTFME) (E 227) by selective fluorination of the compound HFE-254 (1,1,2,2-tetrafluoro-1-(methoxy)ethane), i.e., perfluorination of only the CH.sub.3O-group (i.e., methoxy-group) of the compound HFE-254 is selectively fluorinated to a CF.sub.3O-group (i.e., trifluoromethoxy-group).

MULTI-REFLECTOR PHOTOREACTOR FOR CONTROLLED IRRADIATION OF FLUID
20220176336 · 2022-06-09 ·

A UV reactor comprises a main chamber extending in a generally longitudinal direction. The main chamber may comprise a UV-LED and a reflective wall located at opposing longitudinal ends of the main chamber. Fluid enters main chamber through a fluid inlet and exits main chamber through a fluid outlet. The fluid inlet may be located at the reflective wall end of the main chamber. The fluid outlet may be located at the UV-LED end of the main chamber.

PROCESS AND SYSTEM FOR PRODUCING BIODIESEL
20220162518 · 2022-05-26 ·

A method of producing biodiesel using a conduit contactor in fluid communication with a collection vessel includes: introducing a first stream including an alcohol proximate a plurality of fibers positioned within the conduit contactor and extending proximate to the collection vessel; introducing a second stream including an oil into the conduit contactor proximate to the plurality of fibers, wherein the second stream is in contact with the first stream; reacting the oil and the alcohol to for a single phase; receiving the single phase in the collection vessel; and separating biodiesel from the single phase.

REACTOR FOR SYNTHESIS OF METHANOL OR OTHER PRODUCTS
20230271152 · 2023-08-31 ·

An improved reactor comprising a shell and at least one reactor internal component. The reactor internal component includes a tube bundle comprising a plurality of tubes attached by at least one tube support plate comprising at least one radial strut and at least one bracket configured to secure to at least one tube of the tube bundle. The tubes are arranged in concentric bands about a longitudinal axis of the reactor. The reactor can also include a gas inlet plate, a catalyst support plate, and a top plate. The reactor shell can include a domed head portion with a startup nozzle connected to a reducing flange, providing a manhole access opening into the shell. Sliding strips that slide relative to the tube support plates can facilitate easier assembly, and support rings for the tubes adjacent the plates can accommodate variable thermal expansion of the tubes received in the plates.

Continuous flow processes for making bicyclic compounds

Processes for making bicyclic compounds and precursors thereof, and particularly for making [1.1.1]propellane and bicyclo[1.1.1]pentane and derivatives thereof, utilize continuous flow reaction methods and conditions. A continuous process for making [1.1.1]propellane can be conducted under reaction conditions that advantageously minimize clogging of a continuous flow reactor. A continuous flow process can be used to make precursors of [1.1.1]propellane.

METHODS AND APPARATUS FOR INSTALLATION AND REMOVAL OF CATALYST CARRIERS

A method of installing catalyst carriers into a first selected reactor tube of a tubular reactor. The method comprising the steps of: i) providing an installation tool, the installation tool comprising: a) an installation frame; b) a movable ram mounted to the installation frame and configured for pushing one or more catalyst carriers into the first selected reactor tube; and c) one or more anchors for releasably attaching the installation frame to the tubular reactor; ii) attaching the installation tool to the tubular reactor by engaging the one or more anchors in one or more reactor tubes located alongside the first selected reactor tube so as to align the movable ram with the first selected reactor tube; and iii) actuating the movable ram to push the one or more catalyst carriers into the first selected reactor tube.

CATALYTIC REACTOR WITH IMPROVED PROPERTIES

The invention is in the field of catalysis. In particular, the invention is directed to a catalytic reactor body, a method for the production of a catalytic reactor body and a use of a catalytic reactor body.

The invention provides a catalytic reactor body, comprising a circumferential reactor wall extending in a main fluid flow direction of the reactor body between a reactor inlet and a reactor outlet thereby forming a channel for conducting a fluid; and a reactor bed arranged in the channel and being integrally formed with the circumferential reactor wall, wherein the reactor bed forms a plurality of sub-channels for guiding the fluid from the reactor inlet to the reactor outlet, each sub-channel defining a predetermined fluid path between the reactor inlet and the reactor outlet and being configured for directing the fluid in a direction at least partly transverse to the main flow direction.

SAFE PYROLYTIC EXTRACTION OF DISINFECTING AGENTS FROM OILS
20220151243 · 2022-05-19 ·

Described herein are methods for producing multiple disinfecting agents from oils and reactors for producing multiple disinfecting agents from oils.

METHODS AND REACTORS FOR PRODUCING MULTIPLE DISINFECTING AGENTS FROM OILS
20220151239 · 2022-05-19 ·

Described herein are methods for producing multiple disinfecting agents from oils, including waste oils, and reactors for producing multiple disinfecting agents from the oils.

METHODS OF HIGH THROUGHPUT HYDROCOLLOID BEAD PRODUCTION AND APPARATUSES THEREOF
20230249146 · 2023-08-10 ·

A method of creating hydrocolloid beads includes forcing a hydrocolloid gel suspension through a plurality of nozzles, wherefrom the hydrocolloid gel forms into a plurality of gel drops and fall into a reactant bath. The drops are exposed to the reactant bath for a predetermined period of time, wherein the drops form firm or semi-firm beads as they remain in the reactant bath. The firm or semi-firm beads are removed from the reactant bath, rinsed, and dried.