Disclosed are effective methods for activating, washing, specifically extracting and purifying cannabinoids from Cannabis plant tissues using heat activation, washing impurities away with a polar solvent, optionally modified with an organic acid, base, surfactant or inorganic salt, extracting the activated non-polar cannabinoids with a potable selective solvent such as ethanol. The extracted active ingredients may be purified by chromatography and detected and quantified by mass spectrometry with external or isotopic or otherwise labelled standards.

A method of separating and purifying a mixed stream of contaminated reclaimed polyethylene and contaminated reclaimed polypropylene is provided. The method comprises the steps of extraction, dissolution, settling, purification, and solvent separation to produce separate streams of purified recycled polyethylene and purified recycled polypropylene. Both separate streams are produced in the same production plant operating in swing mode, and have virgin-like optical properties.

Embodiments of the inventive technology may be described as a plant biomass extraction apparatus for production of liquid extract from plant biomass, using carbon dioxide, including one or more of: carbon dioxide chiller, extraction chamber, extract collection chamber, at least one valve, and fluid conveyance componentry, configured to define a closed loop for passive, pump-free extract production. Certain embodiments may avoid saturation of the extractant, and the resultant compromise of process effectiveness that may be seen in those apparatus relying on mechanical pump(s) for flow and/or may present a tabletop, closed loop liquid carbon dioxide extraction apparatus for the production of an extract from plant biomass or other matrix.

A cryogenic solid-liquid extractor comprises a reboiler for evaporating an extraction solvent; a cryogenic heat exchanger for condensing the vaporized extraction solvent to a liquid extraction solvent by passing the vaporized extraction solvent through a container cooled by a cryogenic cooling agent comprising a mixture of a cryogenic solvent and a compressed, liquified or solidified gas to cool the extraction solvent to a temperature below the freezing point of water and above the freezing point of the extraction solvent; a cryogenic extractor for passing the condensed liquid extraction solvent through a solid organic material to extract solvent-soluble material, but not water-soluble material, from the solid organic material, wherein the cryogenic solid-liquid extractor returns the condensed liquid extraction solvent containing extracted material to the reboiler to repeat the vaporization and condensation cycle.

This invention relates to the extraction of psychoactive compounds from psilocybin fungus for use in medicine. Raw psilocybin fungus is dried and ground. The solvent used for extraction is a lower aliphatic alcohol, water, a hydro-alcohol mixture, an acidic hydro-alcohol mixture, or an alkaline hydro-alcohol mixture. The extraction slurry is filtered and pH-adjusted if necessary. The solvent is then partially evaporated, or completely evaporated with water added back, to form a concentrated slurry. The concentrated slurry is then standardized to provide a known concentration of the psychoactive alkaloids that have been extracted. The standardized slurry may then be dried to result in a powdered psilocybin mushroom extract with a precisely defined purity.

A method for forming self-assembled inorganic nanostructures. The method includes forming a mixture by adding a plurality of inorganic nanostructures to an aqueous solution under atmospheric pressure. Forming the mixture includes adding a first plurality of inorganic nanostructures to the aqueous solution and adding a second plurality of inorganic nanostructures to the aqueous solution. The first plurality of inorganic nanostructures has a first plurality of superficial sites with an opposite-signed surface zeta potential respective to a surface zeta potential of a second plurality of superficial sites of the second plurality of inorganic nanostructures.

Systems and methods for extracting a compound of interest from plant material, such as a cannabidiol (CBD) from cannabis, are provided. Particularly, the disclosed systems and methods utilize a crude oil to separate water and impurities including fats, sugars, resin glues, chlorophyll, and proteins prior to preparation of a CBD distillate. The systems and methods are operable to remove the impurities from the crude oil with a brine solution and at least one acid prior to distillation. The systems and methods are operable with conventional solvents containing between about 5 wt % and about 8 wt % water.

A device and method for preparing a sample for solid-liquid or liquid-liquid extraction are provided. In one embodiment, a device includes a sealed container including an opening for receiving a solid sample and a reservoir. The reservoir includes a solvent or is adapted to receive a solvent. The solid sample and the solvent are mixed in the reservoir and to concentrate at least one component of the sample into the solvent within the reservoir. The concentrate is settled into a solvent layer within the container. The solvent layer is sampled via a port. A method includes introducing a solid sample to a solvent; creating a solution by mixing the solid sample with the solvent; allowing the solvent solution to settle into at least one layer; and sampling within at least one layer.

Devices and methods for the high-pressure treatment of bulk material by extraction and/or impregnation. The bulk material is arranged in the interior volume of a pressure vessel device and is treated at a high pressure while sealed off from the surroundings. The high-pressure treatment is performed batchwise in a closed system in the pressure vessel device in a pressure-tight fashion. The bulk material is fed batchwise to the interior volume with the pressure vessel device closed and being arranged on at least one treatment level and, after the high-pressure treatment has occurred, being discharged batchwise from the interior volume with the pressure vessel device closed. The invention furthermore relates to the use of a supporting tray module with at least one treatment level for the high-pressure treatment in a closed system.

A process for extracting a target compound from a biomass includes: extracting a compound from a biomass charge using supercritical or subcritical CO.sub.2 as a solvent, at a first pressure and a first temperature, to yield a compound-laden solvent stream, the compound-laden solvent stream including the solvent, a solubilized target compound, and a solubilized byproduct compound; changing the temperature while maintaining the first pressure of the compound-laden solvent stream to desolubilize the byproduct compound from the compound-laden solvent stream to yield a resultant stream containing the solvent, the solubilized target compound, and a desolubilized byproduct compound; passing the resultant stream through a filter medium to separate the desolubilized byproduct compound from the solubilized target compound; and collecting the solubilized target compound.