Improvements in extraction techniques are described. The improved extraction is provided by an outlet flow controller nut which enhances the efficiency of the collection of compounds as they are extracted from supercritical CO.sub.2. An improved extraction apparatus which includes precise computer controls based on the properties of supercritical CO.sub.2 is also described. The extraction apparatus enables a human operator to extract compounds from organic material with a minimum of intervention and with greater precision that conventional extraction apparatus, which often requires frequent adjustment and yields imprecise results.

Polymorphic forms of tetrahydro-N,N-dimethyl-2,2-diphenyl-3-furanmethanamine hydrochloride (ANAVEX2-73) and a metabolite of tetrahydro-N,N-dimethyl-2,2-diphenyl-3-furanmethanamine hydrochloride (ANAVEX2-73) are disclosed and characterized. Compositions and method for treatment of Alzheimer's disease that includes the polymorphic forms and metabolite of tetrahydro-N,N-dimethyl-2,2-diphenyl-3-furanmethanamine hydrochloride (ANAVEX2-73).

The present invention provides a portable extraction device for extracting at least one constituent from a substance by an extraction fluid. The extraction device comprises at least one pump, an extractor, an evaporator, and a condenser. The substance and the extraction fluid are placed and mixed in the extractor. The extraction fluid is a subcritical fluid. The constituent in the substance will be dissolved in the extraction fluid under a predetermined pressure and temperature. The evaporator receives the extraction fluid including the constituent from the extractor, and heats the extraction fluid including the constituent to gasify the extraction fluid and separate the constituent from the gasified extraction fluid. The condenser receives the gasified extraction fluid via a first pipe, liquefies the gasified extraction fluid, and transmits the liquefied extraction fluid to the extractor via a second pipe. The extractor, the evaporator, and the condenser are operated under constant pressure.

A plurality of collection surfaces for use in an aqueous slurry has a polymeric coating to provide a compliant and sticky surface. The polymer coating has a chemical to render the surface hydrophobic so as to attract hydrophobic or hydrophobized mineral particles in the slurry. The substrate can take the form of a conveyor belt, a bead, a mesh, an impeller, a filter or a flat surface. The substrate can also be an open-cell foam. The collection surfaces having the mineral particles attached thereon are caused to interact with liquid and supercritical carbon dioxide so that the mineral particles can be stripped from the collection surfaces.

The present application provides systems and methods for upgrading an oil stream. The system includes a reactor, a phase separator, an expansion device, a cooling unit, and two separation units. The reactor receives the oil stream, ammonia, and supercritical water. The supercritical water upgrades the oil stream, and the ammonia reacts with sulfur initially present in the oil stream to produce ammonia-sulfur compounds. The phase separator receives a mixture stream comprising the upgraded oil stream, supercritical water, and the ammonia-sulfur compounds, and separates out non-dissolved components. The expansion device reduces the pressure of the mixture stream below a water critical pressure. The cooling unit reduces the temperature of the mixture stream. A first separation unit separates the mixture stream it into a hydrocarbon-rich gaseous phase, a water stream containing ammonia-sulfur compounds, and a treated oil stream. A second separation unit separates the ammonia-sulfur compounds from the water stream.

A system, process and method for remediating contaminated soil and solvent recovery. A solvent mixture including a polar and a non-polar solvent is mixed with contaminated soil in mixing vessels, allowing the solvent mixture to extract contaminates from the soil. The solvent mixture is separated from the soil using bicanting units to form a solvent stream and a soil stream. The soil stream goes through air sparging in a dryer to remove residual solvent vapor. Water and/or micro-fines are extracted from the solvent stream using a centrifuge. The solvent stream undergoes distillation in a distillation unit to remove the containments from the solvent stream, while recovering separately the solvent mixture and a product. The recovered solvent mixture can be recycled back to the mixing vessels. The contaminates can be BTEX or F1-F4 hydrocarbons, and the product can be oil or other hydrocarbons. The system can be mobile.

A process and system for producing deasphalting and demetallized oil from an initial feed such as a heavy feed is provided. The feed is contacted with an effective quantity of solvent to promote phase separation, to produce an asphalt phase and a reduced asphalt content phase. The reduced asphalt content phase is contacted with an effective amount of solid adsorbent to remove undesirable metal compounds to produce an oil phase substantially-free of asphalt and substantially-free of metal. The oil phase that is substantially-free of asphalt and substantially-free of metal is subjected to flash separation to produce a solvent fraction for recycle and an oil phase effluent substantially-free of asphalt and substantially-free of metal for recovery as the desired product.

A crystalline pigment or colorant composition having high color intensity and/or low sugar content, and methods and processes of preparation. The composition may comprise purified fruit and/or vegetable color juices.

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C. to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.