B01D11/0492

Method for the preparation of controlled porosity supports for chromatographic separation

Disclosed herein are extraction chromatographic supports comprising a porous support, an inert filler, and metal ion binding extractant that may be used for chromatographic separation of metal ions. Also disclosed herein are methods for preparing and using the extraction chromatographic supports.

Method of converting delta9-THC to delta10-THC and the purification of the delta10-THC by crystallization
11542243 · 2023-01-03 ·

A method of isomerizing Δ9-tetrahydrocannabinol (“Δ9-THC”) to Δ10-tetrahydrocannabinol (“Δ10-THC”). The method includes the steps of: extracting Δ9-THC from cannabis biomass, which optionally contains one or more of the components found in fire retardant such as PHOS-CHEK®; dewaxing of crude extracts by winterization; pH-adjusting extracts by washing the extracts in heptane solution with aqueous solutions of: citric acid, sodium bicarbonate, and brine; isomerizing Δ9-THC to Δ10-THC by exposure to suitable conditions and in the presence of a catalyst based on the components of fire retardant; vacuum distillation of Δ10-THC at a predetermined temperature range and vacuum level; collecting the distillate and redistilling it up to three times to acquire distillate containing less than 60% Δ10-THC; and purification of the MO-THC to a purity of 99% or greater by crystallization from n-pentane solution.

LIQUID-LIQUID EXTRACTION OF VACUUM RESID-CONTAINING FLUID

Methods comprising contacting a residue comprising paraffinic, olefinic, and aromatic hydrocarbons with a polar solvent under conditions effective to extract at least a portion of the aromatic hydrocarbons from the residue into the polar solvent, thereby generating: an extract phase comprising the portion of aromatic hydrocarbons and the polar solvent; and, a raffinate phase comprising a majority of the paraffinic and olefinic hydrocarbons.

Levulinic acid purification

The present invention refers to a process for the purification of levulinic acid, an aqueous solution comprising levulinic acid and a process for the production of levulinic acid.

Method and System for Directly Cracking Crude Oil to Prepare Olefin

A method for cracking crude oil includes delivering the crude oil to a first tube group of a convection section of a cracking furnace for preheating and then performing vaporization to obtain a first gas phase and a first liquid phase; performing high-pressure extraction on the first liquid phase to obtain a non-asphalt oil and an asphalt; and mixing the first gas phase and the non-asphalt oil with water vapor respectively, or mixing the first gas phase with the non-asphalt oil prior to mixing with water vapor, then delivering the same to a second tube group of the convection section of the cracking furnace for heating, followed by delivering same to a radiation section of the cracking furnace for cracking to obtain a cracked product, and separating the cracked product to obtain low-carbon olefins.

METHOD FOR MICROFLUIDIC EXTRACTION FROM VEGETABLE OIL
20220395766 · 2022-12-15 · ·

A process for the microfluidic extraction of molecules of interest from a vegetable oil, which utilizes a microfluidic chip with a double-Y-channel circuit, two inlets, two outlets, and a main channel, a first vessel including vegetable oil and a second vessel including ethanol for extraction, a pressure controller for pressurizing the vegetable oil and the ethanol, a first collector for the triglycerides-enriched vegetable oil and a second collector for molecules of interest-enriched ethanol. The extraction process includes: controlling the pressures to subject each of the vegetable oil and the ethanol to a pressure, so the interface between the two fluids is positioned at the junction point of inlets, bringing the vegetable oil and ethanol into contact with each other in the main channel for a time to enable extraction of the molecules of interest, collecting the molecules of interest-enriched ethanol, optionally, evaporating the ethanol, collecting the triglycerides-enriched vegetable oil.

A PROCESS FOR WORKING UP WATER CONTAINING 4,4'-DICHLORODIPHENYL SULFOXIDE AND/OR 4,4'-DICHLORODIPHENYL SULFONE AS IMPURITIES

The invention relates to a process for working up water containing 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone as impurities, comprising: (a) mixing the water containing 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone as impurities with an organic solvent in which 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone have a solubility of at least 0.5 wt % based on the amount of 4,4′-dichlorodiphenyl sulfoxide and/or 4, 4′-dichlorodiphenyl sulfone and organic solvent at 20° C., which forms a two-phase system with water and which can be stripped from water with a stripping gas and subsequently separating the obtained mixture into an aqueous phase and an organic phase, and (b) stripping the organic solvent from the aqueous phase with a stripping gas.

Method for the production of cannabinoids from types of industrial hemp

The present invention describes a process for the production of (−)-cannabidiol (CBD) from industrial hemp by means of an extraction followed by two alternative working processes: a process A which provides extraction with solvents first to an alkaline pH and then to acidic pH to isolate the carboxyl form of the CBD which is then subjected to decarboxylation and a process B which provides the elimination of waxes and pitches and then purification by chromatography. At the end of both alternative working processes the CBD is crystallized obtained in high purity crystalline form.

Methods and apparatus for transmitting RACH in wireless communication system

The present disclosure relates to a pre-5.sup.th-Generation (5G) or 5G communication system to be provided for supporting higher data rates Beyond 4.sup.th-Generation (4G) communication system such as Long Term Evolution (LTE). A method for operating a terminal in a wireless communication system includes receiving configuration information regarding a random access channel (RACH) from a base station, and transmitting a RACH preamble based on the configuration information. The configuration information includes information indicating the number of RACH transmission occasions in a frequency axis. A terminal includes a processor configured to receive configuration information regarding a RACH from a base station, and transmit a RACH preamble according to the configuration information, wherein the configuration information includes information indicating the number of RACH transmission occasions in a frequency axis.

Porous liquid and methods of making and using the same

The present disclosure relates to a porous liquid or a porous liquid enzyme that includes a high surface area solid and a liquid film substantially covering the high surface area solid. The porous liquid or porous liquid enzyme may be contacted with a fluid that is immiscible with the liquid film such that a liquid-fluid interface is formed. The liquid film may facilitate mass transfer of a substance or substrate across the liquid-fluid interface. The present disclosure also provides methods of performing liquid-based extractions and enzymatic reactions utilizing the porous liquid or porous liquid enzyme of the present disclosure.