B01D11/0492

Mass spectrometry compatible salt formation for ionic liquid sample preparation

Reagents and methods for obtaining a metabolite solution comprising a mass spectrometry compatible volatile salt or volatile compound.

METHOD FOR PURIFYING MAGNESIUM CHLORIDE SOLUTIONS
20230059919 · 2023-02-23 · ·

A process for removing lactic acid from an aqueous lactic acid-containing magnesium chloride solution, the weight ratio of magnesium chloride to lactic acid in the aqueous lactic acid-containing magnesium chloride solution being at least 1:1, the process including the steps of subjecting the aqueous lactic acid-containing magnesium chloride solution to an evaporation step, resulting in the formation of a slurry of MgC12.MgL2.4H2O in an aqueous magnesium chloride solution, then subjecting the slurry to a solid-liquid separation step, to separate the solid MgC12.MgL2.4H2O from the aqueous magnesium chloride solution, resulting in the removal of lactic acid from the aqueous lactic acid-containing magnesium chloride solution in the form of MgC12.MgL2.4H2O. The process makes it possible to efficiently remove lactic acid from aqueous lactic acid-containing magnesium chloride solutions, resulting in magnesium chloride solutions with a low lactic acid content which can be further processed as desired.

Ammonium Sulphate Production on Industrial Scale

The invention provides a process for the production of crystalline ammonium sulfate, wherein the process comprises performing a Beckmann rearrangement reaction, neutralizing the Beckmann rearrangement reaction mixture, separating a first aqueous ammonium sulfate phase and an aqueous ε-caprolactam phase, charging the first ammonium sulfate phase to a first evaporative type crystallization section wherein crystalline ammonium sulfate is obtained, discharging from the first evaporative type crystallization section mother liquor enriched in organic components, extracting the aqueous ε-caprolactam phase to obtain an extracted ε-caprolactam phase and a second aqueous ammonium sulfate phase, discharging the mother liquor that is discharged from the first evaporative type crystallization section and/or the second aqueous ammonium sulfate phase to a second evaporative type crystallization section wherein evaporative type crystallization is performed so that a three-phase system occurs. At least a liquid oily phase is recovered from the three-phase system. The invention further provides a plant suitable to carry out the process of the invention, crystalline ammonium sulfate and a liquid oily phase obtained by the process of the invention.

Method for Isolation of Cytisine

A method for isolating cytisine from plant material includes dissolving the plant material in an alcohol to form a liquid mixture and acidifying the liquid mixture by addition of an acid. The method also includes concentrating the liquid mixture to form a concentrated aqueous solution and extracting the concentrated aqueous solution with a first extractant to form a purified aqueous concentrate. The method includes alkalizing the purified aqueous concentrate with an alkalizing agent to form an alkaline aqueous concentrate. The method further includes extracting the alkaline aqueous concentrate with a second extractant and removing the second extractant to obtain cytisine.

ANTI-OBESITY COMPOSITION INCLUDING GEUMHWAGYU EXTRACT AS ACTIVE INGREDIENT

Proposed is a Geumhwagyu extract as an active ingredient. The Geumhwagyu extract of the present disclosure inhibits the differentiation of pre-adipocytes by inducing the degradation of CEBP-α and inhibits the expression of CEBP-α, PPARγ, Perilipin-1, Adiponectin, FABP4, etc., to suppress the accumulation of lipids in adipocytes. It can be easily used as a composition for preventing or managing obesity by inhibiting it and lowering the content of TG (Triacylglycerol) to show anti-obesity activity.

Method of Separating and Purifying a Mixed Stream of Contaminated Reclaimed Polyethylene and Polypropylene

A method of separating and purifying a mixed stream of contaminated reclaimed polyethylene and contaminated reclaimed polypropylene is provided. The method comprises the steps of extraction, dissolution, settling, purification, and solvent separation to produce separate streams of purified recycled polyethylene and purified recycled polypropylene. Both separate streams are produced in the same production plant operating in swing mode, and have virgin-like optical properties.

MOLECULARLY IMPRINTED POLYMERS FOR EXTRACTION OF CANNABINOIDS AND USES THEREOF
20230100363 · 2023-03-30 ·

The present disclosure relates to molecularly imprinted polymers that target cannabinoid(s), including THC and CBD, as well as methods of making molecularly imprinted polymers that target cannabinoid(s), including THC and CBD and uses thereof.

Method and apparatus for producing specific substances by extraction and separation in a liquid-liquid system

A new system in which a forward extraction part, a scrubbing part, and a backward extraction part operate together and synchronously to produce specific substances by extraction and separation in a liquid-liquid system. The aqueous phase is circulated independently only in the forward extraction part one or more times, and the organic phase is circulated from the forward extraction part through the scrubbing part and the backward extraction part to the forward extraction part again in synchronization with the liquid circulation of the aqueous phase.

Extracting apparatus, and extracting-unit manufacturing method
11612832 · 2023-03-28 · ·

An extracting apparatus includes: a first phase transition section that causes a phase transition of an extraction solvent from a gas to a liquid; a second phase transition section that causes a phase transition of the extraction solvent from a liquid to a gas; a treatment tank that stores a treated material, and receives an inflow of the extraction solvent that has been liquefied in the first phase transition section; a first valve that is provided between the second phase transition section and the treatment tank; and a second valve that is provided between the first phase transition section and the treatment tank. The second phase transition section is connected with a recovery valve.

Method of separating solid electrolyte and cathode active material which are contained in slurry
11484812 · 2022-11-01 · ·

A method of easily separating a solid electrolyte and a cathode active material which are contained in a slurry is disclosed. The method of separating a solid electrolyte and a cathode active material which are contained in a slurry includes: adding a fluorine-based solvent to the slurry containing the solid electrolyte and the cathode active material, the cathode active material containing at least one selected from nickel, cobalt and manganese as a constituent element.