Disclosed is a method for manufacturing a metal part made from titanium, by sintering a powder, the method comprising a step of mixing a spherical titanium powder and a dendritic titanium powder in order to form a mixture, a step of agglomerating the mixture of titanium powders by compaction with a ram moving at a speed of more than 2 m.Math.s.sup.−1, the mixture of titanium powders being free of binders, in particular organic binders, forming a green body or agglomerate suitable for sintering having a density above 78%, and preferably 80%, of the density of the solid metal, and a step of sintering.

Certain aspects of the technology disclosed herein include an apparatus and method for programming a crystal lattice structure of a nanoparticle. A particle programming apparatus can include an input channel connected a particle sampling system. The particle sampling system can direct freshly milled nanoparticles to the particle programming apparatus if the nanoparticles are determined to be below a threshold size. The particle programming apparatus can include one or more programming devices configured to alter a crystal lattice of the received nanoparticles including an ultrasonic sound generator, a magnetic pulse generator, and a voltage generator. The one or more programming devices applies any of a sound, magnetic pulse, and voltage to the received nanoparticles within a time threshold of receiving the nanoparticles from the mill core.

Certain aspects of the technology disclosed herein include an apparatus and method for programming a crystal lattice structure of a nanoparticle. A particle programming apparatus can include an input channel connected a particle sampling system. The particle sampling system can direct freshly milled nanoparticles to the particle programming apparatus if the nanoparticles are determined to be below a threshold size. The particle programming apparatus can include one or more programming devices configured to alter a crystal lattice of the received nanoparticles including an ultrasonic sound generator, a magnetic pulse generator, and a voltage generator. The one or more programming devices applies any of a sound, magnetic pulse, and voltage to the received nanoparticles within a time threshold of receiving the nanoparticles from the mill core.

The present disclosure refers to a preparation method for improving the coercive force of a sintered Nd—Fe—B magnet and comprises: preparing Nd—Fe—B alloy flakes by a strip casting process, followed by hydrogen decrepitation of the Nd—Fe—B alloy flakes and jet milling to obtain an Nd—Fe—B powder; mixing Nd—Fe—B powder and an amount of 0.1 to 5 wt. % of a nanoparticulate powder in a powder mixing machine to obtain a powder mixture; modification of the powder mixture obtained in step B) under inert conditions in a mechanical mixing equipment such that the particles of the Nd—Fe—B powder are rounded and the nanoparticulate powder adheres to the particle surface of the Nd—Fe—B powder; mixing in a lubricant to the modified Nd—Fe—B powder in a powder mixing machine; and align pressing the modified Nd—Fe—B powder into a green body, sintering the green body, and aging of the obtained sintered Nd—Fe—B magnet.

A sintered Nd—Fe—B magnet comprising at least one light rare earth element having a weight content between 31 wt. % and 35 wt. %, at least one heavy rare earth element having a weight content of no more than 0.2 wt. %, B having a weight content between 0.95 wt. % and 1.2 wt. %, at least one additive including Ti and having a weight content between 1.31 wt. % and 7.2 wt. %, Fe as a balance, and impurities including C, O, and N. Ti has a weight content between 0.3 wt. % and 1 wt. % and forms a Titanium-Iron-Boron phase with Fe and Boron B and being present in the sintered Nd—Fe—B magnet between 0.86 vol. % and 2.85 vol. %. The C, O, and N satisfy 630 ppm≤1.2C+0.6O+N≤3680 ppm. The sintered Nd—Fe—B magnet has a squareness factor of at least 0.95.

A sintered Nd—Fe—B magnet comprising at least one light rare earth element having a weight content between 31 wt. % and 35 wt. %, at least one heavy rare earth element having a weight content of no more than 0.2 wt. %, B having a weight content between 0.95 wt. % and 1.2 wt. %, at least one additive including Ti and having a weight content between 1.31 wt. % and 7.2 wt. %, Fe as a balance, and impurities including C, O, and N. Ti has a weight content between 0.3 wt. % and 1 wt. % and forms a Titanium-Iron-Boron phase with Fe and Boron B and being present in the sintered Nd—Fe—B magnet between 0.86 vol. % and 2.85 vol. %. The C, O, and N satisfy 630 ppm≤1.2C+0.6O+N≤3680 ppm. The sintered Nd—Fe—B magnet has a squareness factor of at least 0.95.

The present disclosure relates generally to a method for improving the performance of sintered NdFeB magnet. A method of preparing a sintered NdFeB magnet therefore comprises the steps of: a) preparing alloy flakes from a raw material of the NdFeB magnet by a strip casting process; and b) preparing a coarse alloy powder from the alloy flakes by a hydrogen decrepitation process, the hydrogen decrepitation process including treatment of the alloy flakes under a hydrogen pressure of 0.10 MPa to 0.25 MPa for a duration of 1 to 3.5 hours, then degassing the hydrogen at a predetermined temperature between 300° C. to 400° C. for a duration time of 0.5 to 5 hours, and then mixing the resulting coarse alloy powder with a lubricant.

The present disclosure relates generally to a method for improving the performance of sintered NdFeB magnet. A method of preparing a sintered NdFeB magnet therefore comprises the steps of: a) preparing alloy flakes from a raw material of the NdFeB magnet by a strip casting process; and b) preparing a coarse alloy powder from the alloy flakes by a hydrogen decrepitation process, the hydrogen decrepitation process including treatment of the alloy flakes under a hydrogen pressure of 0.10 MPa to 0.25 MPa for a duration of 1 to 3.5 hours, then degassing the hydrogen at a predetermined temperature between 300° C. to 400° C. for a duration time of 0.5 to 5 hours, and then mixing the resulting coarse alloy powder with a lubricant.

A method of manufacturing a permanent magnet comprises a solution heat treatment. The solution heat treatment includes: performing a heat treatment at a temperature T.sub.ST; placing a cooling member including a first layer and a second layer on the first layer between the heater and the treatment object so that the first layer faces the treatment object; and transferring the treatment object together with the cooling member to the outside of a heating chamber, and cooling the treatment object until a temperature of the treatment object becomes a temperature lower than a temperature T.sub.ST200 C. In the step of cooling the treatment object, a cooling rate until the temperature of the treatment object becomes the temperature T.sub.ST200 C. is 5 C./s or more.

A method of manufacturing a permanent magnet comprises a solution heat treatment. The solution heat treatment includes: performing a heat treatment at a temperature T.sub.ST; placing a cooling member including a first layer and a second layer on the first layer between the heater and the treatment object so that the first layer faces the treatment object; and transferring the treatment object together with the cooling member to the outside of a heating chamber, and cooling the treatment object until a temperature of the treatment object becomes a temperature lower than a temperature T.sub.ST200 C. In the step of cooling the treatment object, a cooling rate until the temperature of the treatment object becomes the temperature T.sub.ST200 C. is 5 C./s or more.