A method for manufacturing FeNi ordered alloy having a L1.sub.0 type order structure is provided. After a nitrification process for nitriding a powder sample of a FeNi disordered alloy arranged in a tube furnace is performed using a NH.sub.3 gas, a de-nitrification process for removing a nitrogen from the FeNi disordered alloy which is processed by the nitrification process is performed using a H.sub.2 gas. Thus, the L1.sub.0 type FeNi ordered alloy with a regularity defined by S equal to or higher than 0.5 is obtained.

A cubic boron nitride sintered material comprises 30% by volume or more and 99.9% by volume or less of cubic boron nitride grains and 0.1% by volume or more and 70% by volume or less of a binder phase, the cubic boron nitride grain having a carbon content of 0.08% by mass or less, the cubic boron nitride sintered material being free of free carbon.

A cubic boron nitride sintered material comprises 30% by volume or more and 99.9% by volume or less of cubic boron nitride grains and 0.1% by volume or more and 70% by volume or less of a binder phase, the cubic boron nitride grain having a carbon content of 0.08% by mass or less, the cubic boron nitride sintered material being free of free carbon.

A powder cleaning system can include a fluidized bed reactor configured to retain powder and fluidize the powder to remove adsorbate and/or other contaminants from the powder, and one or more gas sources configured to be in selective fluid communication with the fluidized bed reactor via at least one inlet line to selectively provide an inlet flow having one or more gases to the fluidized bed reactor to fluidize the powder with the one or more gases within the fluidized bed reactor. The system can include at least one outlet line in fluid communication with the fluidized bed reactor and configured to allow removal of outlet flow which comprises the adsorbate and/or other contaminants from the fluidized bed reactor.

The present disclosure relates to a method of preparing a nano-porous powder material. The method includes: firstly removing A in the alloy A.sub.xT.sub.y by using an ultrasonically-assisted de-alloying method to prepare a nano-porous T coarse powder, and then, allowing the nano-porous T coarse powder to perform M-ization reaction with a gas reactant containing M to obtain a nano-porous T-M coarse powder, and finally, further crushing the nano-porous T-M coarse powder using a jet mill to obtain a nano-porous T-M fine powder. The method can achieve low-cost mass production of the nano-porous T-M fine powder, bringing broad application prospects.

The present disclosure relates to a method of preparing a nano-porous powder material. The method includes: firstly removing A in the alloy A.sub.xT.sub.y by using an ultrasonically-assisted de-alloying method to prepare a nano-porous T coarse powder, and then, allowing the nano-porous T coarse powder to perform M-ization reaction with a gas reactant containing M to obtain a nano-porous T-M coarse powder, and finally, further crushing the nano-porous T-M coarse powder using a jet mill to obtain a nano-porous T-M fine powder. The method can achieve low-cost mass production of the nano-porous T-M fine powder, bringing broad application prospects.

Metal powder is compacted in a die to produce a preform having a preselected porosity with the metal powder containing iron and having a plurality of particles having a preselected particle sizes. The preform is carburized to produce a high carbon solution in the metal powder. The preform is contacted with an ammonia gas distillation solution to inject nitrogen therein. The preform is heat treated for a predetermined period of time at a predetermined temperature and at a predetermined pressure. The preform is quenched to form a metal part.

Metal powder is compacted in a die to produce a preform having a preselected porosity with the metal powder containing iron and having a plurality of particles having a preselected particle sizes. The preform is carburized to produce a high carbon solution in the metal powder. The preform is contacted with an ammonia gas distillation solution to inject nitrogen therein. The preform is heat treated for a predetermined period of time at a predetermined temperature and at a predetermined pressure. The preform is quenched to form a metal part.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one α″-Fe.sub.16N.sub.2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one α″-Fe.sub.16N.sub.2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one α″-Fe.sub.16N.sub.2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one α″-Fe.sub.16N.sub.2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.