Provided is a method of fabricating a micro/nanowire having a nanometer- to micrometer-sized diameter at predetermined positions on an object. The method comprises: preparing a micro/nanopipette having a tip with an inner diameter (d.sub.pt) which is substantially the same as the diameter of the micro/nanowire to be fabricated; filling the micro/nanopipette with a solution containing a micro/nanowire-forming material; bringing the solution into contact with the object through the tip of the micro/nanopipette; and pulling the micro/nanopipette apart from the object at a pulling speed lower than or equal to a predetermined critical pulling speed (v.sub.c) to fabricate a micro/nanowire having substantially the same diameter as the inner diameter of the micro/nanopipette tip (d.sub.pt). The critical pulling speed (v.sub.c) is defined by a maximum limit of the pulling speed at which the micro/nanowire to be fabricated has the same diameter as the inner diameter of the micro/nanopipette tip (d.sub.pt).

In a method of manufacturing a highly stretchable three-dimensional (3D) percolated conductive nano-network structure, a 3D nano-structured porous elastomer including patterns distributed in a periodic network is formed. A surface of the 3D nano-structured porous elastomer is changed to a hydrophilic state. A polymeric material is conformally adhered on the surface of the 3D nano-structured porous elastomer. The surface of the 3D nano-structured porous elastomer is wet by infiltrating a conductive solution in which a conductive material is dispersed. A 3D percolated conductive nano-network coupled with the 3D nano-structured porous elastomer is formed by evaporating a solvent of the conductive solution and removing the polymeric material.

The present invention relates to a method of fabricating a nanowire connected to an optical fiber, the method comprising the steps of: a) filling a micropipette with a material solution to form a nanowire; b) coaxially aligning the micropipette with the optical fiber at one end of the optical fiber such that a longitudinal axis of the optical fiber and a longitudinal axis of the micropipette are aligned in a line; c) forming a meniscus of the material solution to form the nanowire in the coaxially aligned state; and d) fabricating the nanowire by evaporating a solvent from the material solution to form the nanowire while lifting the micropipette in a state in which the meniscus is formed, in a direction away from the optical fiber. The method further comprises a step of a step of controlling a shape of the distal end of the nanowire by irradiating a laser to the nanowire fabricated.

A method for surface writing is disclosed. The method includes fabricating a plurality of nanomotors, forming a secondary solution by adding the plurality of nanomotors to a primary solution placed on a substrate, guiding the plurality of nanomotors along a path in the secondary solution, and forming a sol-gel film along the path on a surface of the substrate. Wherein, the primary solution includes a monomer and hydrogen peroxide (H.sub.2O.sub.2). Fabricating the plurality of nanomotors includes preparing a mesoporous silica template, forming the plurality of nanomotors within the mesoporous silica template, and separating the plurality of nanomotors from the mesoporous silica template. The mesoporous silica template includes a plurality of channels, wherein each channel of the plurality of channels has a diameter less than about 50 nm and a length of less than about 100 nm, and each nanomotor of the plurality of nanomotors is formed within a channel of the plurality of channels.

A new technique, referred to as PSBEE, is disclosed and enables fabrication of freestanding nanomembranes. The PSBEE technique enables fabrication and synthesis of nanomembranes comprising 2D high entropy alloys and 2D metallic glasses and may be extended to ceramics and semiconductors, thereby enabling the fabrication of large-scale freestanding nanomembranes across a wide range of materials, including those deemed to have a great potential for future functional and structural use. To form nanomembranes using PSBEE, a plurality of membranes may be prepared and subjected to thermoplastic compression. Afterwards, one of the membranes may be removed and the remaining membranes may undergo additional thermoplastic compression in the presence of a Si substrate. Once a threshold level of smoothness is achieved, a coating or film may be applied and then separated from the final plate.

Methods of manufacturing well-controlled nanopores using directed self-assembly and methods of manufacturing free-standing membranes using selective etching are disclosed. In one aspect, one or more nanopores are formed by directed self-assembly with block co-polymers to shrink the critical dimension of a feature which is then transferred to a thin film. In another aspect, a method includes providing a substrate having a thin film over a highly etchable layer thereof, forming one or more nanopores through the thin film over the highly etchable layer, for example, by a pore diameter reduction process, and then selectively removing a portion of the highly etchable layer under the one or more nanopores to form a thin, free-standing membrane.

A method for manufacturing a metallic nanospring includes preparing a nanotemplate having a nanopore and including a working electrode disposed on its one surface, preparing a first metal precursor mixture including ascorbic acid (C.sub.6H.sub.8O.sub.6), vanadium (IV) oxide sulfate (VOSO.sub.4.xH.sub.2O), and a metal precursor solution including a metal desired to be deposited, preparing a second metal precursor mixture by mixing the first metal precursor mixture with nitric acid (HNO.sub.3), depositing a metallic nanospring into the nanopore using electrodeposition by dipping the nanotemplate into the second metal precursor mixture and applying current between a counter electrode inserted into the second metal precursor mixture and the working electrode, and selectively removing the working electrode on the nanotemplate with the deposited metallic nanospring and the nanotemplate.

The present invention relates to a method of fabricating a nanowire connected to an optical fiber, the method comprising the steps of: a) filling a micropipette with a material solution to form a nanowire; b) coaxially aligning the micropipette with the optical fiber at one end of the optical fiber such that a longitudinal axis of the optical fiber and a longitudinal axis of the micropipette are aligned in a line; c) forming a meniscus of the material solution to form the nanowire in the coaxially aligned state; and d) fabricating the nanowire by evaporating a solvent from the material solution to form the nanowire while lifting the micropipette in a state in which the meniscus is formed, in a direction away from the optical fiber. The method further comprises a step of a step of controlling a shape of the distal end of the nanowire by irradiating a laser to the nanowire fabricated.

The present invention discloses a flexible graphene film and a preparation method thereof. The preparation method includes steps of placing a liquid graphene oxide film in a poor solvent, performing gelation, and drying a graphene oxide gel film. The graphene film has an excellent flexibility, a crystallinity of lower than 60% and an elongation at break of 15-50%, wherein no crease is remained after the flexible graphene film is repeatedly folded more than 100,000 times. The preparation method of the graphene film provided by the present invention controls the macroscopic properties of the graphene film by microscopically controlling the morphology of the graphene monolith, and can significantly improve the flexibility of the graphene film. It can significantly improve the flexibility of the graphene film. The process is simple and easy to be popularized, and has potential applications in flexible electronic devices and the like.

This present disclosure provides methods for utilizing such forces in when generating nanofibrillar constructs with engineered morphology from the nano- to macro-scales. Using for example, a biopolymer silk fibroin as a base material, patterns an intermediate hydrogel were generated within a deformable mold. Subsequently, mechanical tension was introduced via either hydrogel contraction or mold deformation, and finally a material is reentrapped in this transformed shape via beta-sheet crystallization and critical point drying. Topdown engineered anchorages, cables, and shapes act in concert to mediate precision changes in nanofiber alignment/orientation and a macroscale form of provided nanofibrillar structure. An ability of this technique to engineer large gradients of nano- and micro-scale order, manipulate mechanical properties (such as plasticity and thermal transport), and the in-situ generation of 2D and 3D, multi-tiered and doped, nanofibrillar constructs was demonstrated.